U.S. patent number 3,907,106 [Application Number 05/360,532] was granted by the patent office on 1975-09-23 for compounding vessel.
This patent grant is currently assigned to E S P E GmbH. Invention is credited to Rainer Grimm-Lenz, Peter Jochum, Robert Purrmann, Werner Schmitt.
United States Patent |
3,907,106 |
Purrmann , et al. |
September 23, 1975 |
**Please see images for:
( Certificate of Correction ) ** |
Compounding vessel
Abstract
A compounding vessel for component substances which interact and
form ready-for-use dental preparations. The vessel has a main
chamber forming a mixing compartment (and adapted to contain a
first component), and a supplementary chamber (adapted to contain a
second component) separated by a membrane-closed opening from the
mixing compartment. Mixing is effected by rupturing the membrane by
pressure applied in a direction towards a wall of the main
chamber.
Inventors: |
Purrmann; Robert (Starnberg,
DT), Schmitt; Werner (Starnberg, DT),
Jochum; Peter (Hechendorf, DT), Grimm-Lenz;
Rainer (Seefeld, DT) |
Assignee: |
E S P E GmbH (Seefeld,
DT)
|
Family
ID: |
4334604 |
Appl.
No.: |
05/360,532 |
Filed: |
May 15, 1973 |
Foreign Application Priority Data
|
|
|
|
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May 31, 1972 [CH] |
|
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008066/72 |
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Current U.S.
Class: |
206/219; 222/80;
366/602 |
Current CPC
Class: |
A61C
5/64 (20170201); A61C 5/66 (20170201); Y10S
366/602 (20130101) |
Current International
Class: |
A61C
5/06 (20060101); A61C 5/00 (20060101); B65D
081/32 () |
Field of
Search: |
;259/72,27,47,48,49,54,57,60,70,71 ;206/47A,219,222 ;222/80 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Jenkins; Robert W.
Attorney, Agent or Firm: Bierman & Bierman
Claims
We claim:
1. An apparatus for mixing at least two components in precise
proportions comprising a main mixing chamber containing one
component of the mixture, at least one supplementary chamber
containing an additional component of the mixture, said chamber
being defined by a radially inwardly movable wall embracing in
movable relationship thereto, the outer wall of the main chamber,
said outer wall being cylindrical, the movable wall conforming to
the outer wall of the main chamber, the supplementary chamber
communicating with the main chamber through an opening in the wall
of the main chamber, the component in the supplementary chamber
being sealed from the main chamber by a rupturable bag containing
the additional component, said bag being placed over said hole,
whereupon said bag, upon substantially reducing the volume of the
supplementary chamber, abruptly ruptures to allow the additional
component to enter the main chamber, means for rupturing the bag
comprising external pressure applied in the direction of the wall
of the main chamber, whereby the bag is ruptured and the volume of
the supplementary chamber is reduced substantially to zero, and a
means for retaining the movable wall in a terminal position against
the main chamber, comprising axially disposed ribs which engage
corresponding notches provided in the movable wall.
2. The apparatus of claim 1 in which one end of the main chamber is
closed by an axially sliding plunger and the other end is provided
with an axially tapering end wall, said wall having an axially
outwardly projecting ejector nozzle.
3. An apparatus for mixing at least two components in precise
proportions comprising a main mixing chamber containing one
component of the mixture, at least one supplementary chamber
containing an additional component of the mixture, said chamber
being defined by a radially inwardly movable wall embracing in
movable relationship thereto, the outer wall of the main chamber,
said outer wall being cylindrical, the movable wall conforming to
the outer wall of the main chamber, the supplementary chamber
communicating with the main chamber through an opening in the wall
of the main chamber, the component in the supplementary chamber
being sealed from the main chamber by a rupturable bag containing
the additional component, said bag being placed over said hole,
whereupon said bag, upon substantially reducing the volume of the
supplementary chamber, abruptly ruptures to allow the additional
component to enter the main chamber, means for rupturing the
membrane comprising external pressure applied in the direction of
the wall of the main chamber, whereby the volume of the
supplementary chamber is reduced substantially to zero and the
membrane is ruptured, and a means for retaining the movable wall in
a terminal position against the main chamber outside wall, the
axial position of the movable wall being fixed by two flanges
projecting radially from the outside wall of the main chamber.
4. The apparatus of claim 3 in which each flange is provided with a
notch, the notches being axially aligned; and the movable wall is
provided with projections which align with the notches and which
engage therein.
5. An apparatus for mixing at least two components in precise
proportions comprising a main mixing chamber containing one
component of the mixture, at least one supplementary chamber
containing an additional component of the mixture, the
supplementary chamber communicating with the main chamber through
an opening in the wall of the main chamber, the component in the
supplementary chamber being sealed from the main chamber by a
rupturable membrane which, upon substantially reducing the volume
of the supplementary chamber, abruptly ruptures to allow the
additional component to enter the main chamber, means for rupturing
the membrane comprising external pressure applied in the direction
of the wall of the main chamber, whereby the membrane is ruptured
and the volume of the supplementary chamber is reduced
substantially to zero, said supplementary chamber being
cylindrical, its axis being substantially normal to the axis of the
main chamber, the supplementary chamber being provided with a
slideable plunger which seals the end of its supplementary chamber
remote from the main chamber.
6. The apparatus of claim 5 in which there are two supplementary
chambers disposed coaxially opposite each other about the main
chamber.
7. The apparatus of claim 5 in which one end of the main chamber is
closed by an axially sliding plunger and the other end is provided
with an axially tapering end wall, said wall having an axially
outwardly projecting ejector nozzle.
8. An apparatus for mixing at least two components in precise
proportions comprising a main mixing chamber containing one
component of the mixture, at least one supplementary chamber
containing an additional component of the mixture, said chamber
being defined by a radially inwardly movable wall embracing in
movable relationship thereto, the outer wall of the main chamber,
said outer wall being cylindrical, the movable wall conforming to
the outer wall of the main chamber, the supplementary chamber
communicating with the main chamber through an opening in the wall
of the main chamber, the component in the supplementary chamber
being sealed from the main chamber by a rupturable membrane which,
upon substantially reducing the volume of the supplementary
chamber, abruptly ruptures to allow the additional component to
enter the main chamber, means for rupturing the membrane comprising
external pressure applied in the direction of the wall of the main
chamber, whereby the membrane is ruptured and the volume of the
supplementary chamber is reduced substantially to zero, said main
chamber being cylindrical, one end of which is closed by an axially
sliding plunger, and the other end of which is provided with an
axially tapering end wall, the end wall having an axially
projecting ejector nozzle.
9. An apparatus for mixing components in precise proportions
comprising a main mixing chamber containing one component of the
mixture, two supplementary chambers containing additional
components of the mixture, said supplementary chambers being
defined by a common radially inwardly movable wall embracing in
movable relationship thereto, the outer wall of the main chamber,
said outer wall being cylindrical, the movable wall conforming to
the outer wall of the main chamber, each of the supplementary
chambers communicating with the main chamber through an opening in
the wall of the main chamber, each of the components in the
supplementary chamber being sealed from the main chamber by a
rupturable bag containing an additional component, said bags being
placed over said holes, wherein said bags, upon substantially
reducing the volume of the supplementary chamber, abruptly rupture
to allow the additional components to enter the main chamber, means
for rupturing the bags comprising external pressure applied in the
direction of the wall of the main chamber, whereby the bags are
ruptured and the volume of the supplementary chambers is reduced
substantially to zero.
10. The apparatus of claim 9 in which one end of the main chamber
is closed by an axially sliding plunger and the other end is
provided with an axially tapering end wall, said wall having an
axially outwardly projecting ejector nozzle.
Description
The invention relates to a compounding vessel for component
substances which interact and form ready-for-use dental
preparation, comprising a main chamber forming a mixing compartment
and adapted to contain a first component, and at least one
supplementary chamber adapted to contain respectively, one or more
additional components and which adjoins a portion of the outside
wall containing an opening which communicates with the mixing
compartment, and which is closed by a membrane or bag which is
ruptured when for the purpose of combining the components the
capacity of the supplementary chamber is reduced.
Such a vessel has already been described in the published
specification of German application No. 1,910,885. In this vessel
the supplementary chamber which contains a foil bag is formed by
the external surface of the cylinder wall of the main chamber wall
and/or the inside surface of the cover deviate from a pure
concentric, axially symmetrical shape. By turning the cover in
relation to the main chamber the capacity of the supplementary
chamber can be reduced to the destruction of the foil bag which
discharges its contents through the opening into the mixing
chamber. In this vessel there is a risk of the rotary movement not
being continued far enough for the foil bag to be completely
discharged. When this happens the proportions of the components of
the mixture will vary and the finished dental preparation will fail
to have the expected optimum properties. Moreover, in the case of
this vessel, special steps must be taken to ensure that during the
twisting of the cover the foil bag will not be displaced from the
opening in the wall of the main chamber. This requirement creates
difficulties in the design or assembly of the several parts of the
vessel.
Furthermore, the published specification of German patent
application No. 1,939,316 describes a mixer vessel in which the
supplementary chamber, which again contains a foil bag, is disposed
between a piston that can be moved inside the main chamber and a
plunger which is movable in relation to the piston. The reduction
in capacity of the supplementary chamber for the destruction of the
foil bag and the discharge of its contents into the mixing
compartment of the main chamber is effected by displacing the
plunger in relation to the piston. When the components that have
thus been combined have been mixed the piston is displaced in the
cylindrical main chamber and expels the mixture through a delivery
nozzle in the other end wall of the main chamber. In other words,
in this vessel the movements for bringing the two components
together and for expelling the finished mixture proceed in the same
direction axially in the cylindrical main chamber. However, since
first only the plunger is moved in relation to the piston whilst
the latter remains stationary inside the main chamber, appropriate
arresting means or frictional resistances must be provided. These
call for an extremely precise manufacture of the several parts of
the vessel. The tolerances which must be observed are extremely
critical because the piston which is first kept stationary in the
main chamber must be capable of withstanding considerable pressure
by the plunger to ensure that the foil bag will be completely
discharged. Another difficulty inherent in this type of vessel is
that portions of the ruptured bag can enter the mixture during the
following violent shaking which is needed for satisfactory
commixture of the two components, and that the properties of the
preparation may thus be impaired.
The present invention seeks to provide a compounding vessel for the
production of dental preparation, which on the one hand enables the
desired preparation to be produced in precisely the required
mixture proportions without any risk of the inclusion of foreign
matter and, on the other hand, comprises simple, easily produced
elements that can be assembled without much trouble.
According to the invention, in a compounding vessel of the first
hereinabove specified kind the capacity of the supplementary
chamber is reduced by pressure applied in a radially inwards
direction towards the wall of the main chamber. Such a pressure can
be generated by a thrust-induced movement, which can be abruptly
produced, causing the capacity of the supplementary chamber to be
reduced essentially to zero and thus completely discharging the
component of the mixture in the bag. Moreover, the opening in the
cylindrical wall of the main chamber may be so disposed that a
plunger, which may be provided in the main chamber, can be
displaced to cover said opening after the supplementary chamber has
been emptied and before the mixture is shaken, so that on the one
hand portions of the ruptured bag cannot enter the mixing
compartment and, on the other hand, the mixture cannot leak back
into the possibly re-expanded supplementary chamber. For ejecting
the finished mixture, such a plunger can be designed to move easily
since it does not require the cooperation of arresting means and
need not overcome special frictional resistance. Another advantage
of the invention is that a compounding vessel based on the proposed
principle of construction can be readily designed to mix three or
more components by the provision of additional supplementary
chambers.
In a convenient embodiment of the invention the supplementary
chamber is constituted by a movable wall such as a partially
cylindrical clip containing the second component in a foil bag, the
internal diameter of said clip being substantially equal to the
external diameter of a cylindrical wall of the main chamber and
being held by engageable retaining elements in a position in which
the inner surface of the clip is spaced away from the external
surface of the cylindrical wall by a distance equal to the
thickness of the filled foil bag. The compounding vessel in this
arrangement is easy and cheap to produce and no strict tolerances
need be observed.
To prevent the supplementary chamber from resiliently re-expanding
after an abrupt capacity reduction and from thus drawing portions
of the mixture back again by suction effects, it is preferred to
provide further engageable elements for retaining the clip in a
position in which its inside surface presses the empty foil bag
tightly against the outside surface of the cylindrical wall.
If the compounding of the desired dental preparation requires the
combination of three components, then two foil bags may be located
either under a common, axially wider, clip, or one under each of
two different separate clips.
In another convenient embodiment of the invention the supplement
chamber is constituted by a cylindrical attachment disposed with
its axis normal to the axis of a cylindrical main chamber and
containing an axially slidably movable plunger which closes its
free open end. This embodiment is of particular utility when a
relatively large quantity of the second component is needed, more
than could be conveniently accommodated in a foil bag adapted to be
destroyed by shock thrust.
For mixing three components this latter embodiment can be provided
with an additional supplementary chamber which may resemble or be
identical with the first supplementary chamber, and which is
likewise attached to the main chamber, both supplementary chambers
being preferably coaxially disposed.
In an advantageous further development of the invention, one end of
the main chamber is closed by an axially tapering end wall from the
centre of which an ejector nozzle projects, whereas the other end
is closed by an axially slidably movable plunger. A mixer vessel
which is thus constructed permits a ready-mixed dental preparation
to be directly injected into the dental cavity that is to be
filled.
The invention will now be more particularly described by way of
example, with reference to the accompanying drawings, in which:
FIG. 1 is a first embodiment of a compounding vessel according to
the invention, in longitudinal section,
FIG. 2 is a cross section taken on the line II -- II in FIG. 1,
FIG. 3 is a second embodiment of a compounding vessel according to
the invention, likewise in longitudinal section, and,
FIG. 4 is a cross section taken on the line IV -- IV in FIG. 3,
FIG. 5 is an additional embodiment of the present invention in
longitudinal section.
Referring to the compounding vessel shown in FIGS. 1 and 2, this
comprises a generally cylindrical main chamber 10 of a circular
cross-section, containing a first substance (not shown) which may
be in the form of a powder. The lower end of the cylindrical main
chamber 10 is terminated by a hemispherically dome-shaped portion
11 which is formed with a delivery nozzle 12 projecting therefrom
coaxially with the longitudinal axis of the main chamber 10. The
mouth of the nozzle 12 is closed by a removable pin 13. The upper
end of the main chamber 10 is closed by a hollow plunger 14 which
has a hemispherically dome head facing the interior of the main
chamber, the radius of this dome head being equal to the radius of
the interior of the dome-shaped portion 11.
At axially spaced levels, the cylinder wall of the main chamber 10
is formed externally with two annular flanges 15 provided with
axially aligned gaps 16. These two annular flanges 15 serve for
axially locating a roughly semicylindrical clip 17 which embraces
the outside of the cylindrical wall of the main chamber 10. On
diametrically opposite sides of the external surface of the
cylindrical wall of the main chamber 10, ribs 18 are formed between
the two annular flanges 15. These ribs 18 are adapted to engage
notches 19 or 20 formed on the inwardly facing surfaces of the ends
of the clips 17. Moreover, in the middle, the clip 17 is provided
with a bulbous enlargement 21 which extends in the axial direction,
the length of this enlargement exceeding the distance between the
two annular flanges 15, its ends aligning with the gaps 16 in the
annular flanges.
Midway between the annular flanges 15 the cylindrical wall of the
main chamber 10 contains an opening 22 facing the clip 17. A bag 23
of rupturable material (e.g., metal foil), contains for instance a
liquid, is interposed between the clip 17 and that part of the
cylindrical wall of the main chamber 10 containing the opening 22.
The bag walls are of material of two different strengths, that
facing the opening 22 being weaker than the other.
When the compounding vessel illustrated in FIGS. 1 and 2 is to be
used, one component of the substance to be mixed is placed in the
chamber 10 and the other component is in the bag 23. When pressure
is applied to the clip 17, more particularly to the enlargement 21
thereof, the clip 17 is forced from the position shown in FIGS. 1
and 2 (in which the ribs 18 engage in outer notches 19) inwards
towards the wall of the main chamber 10 until the ribs 18 snap into
engagement with the inner notches 20. During this inward
displacement, the wall of the bag 23 facing the opening 22 will
burst and the substance contained in the bag will spill through the
opening 22 into the mixing compartment of the main chamber 10. The
ribs 18 which engage the notches 20 prevent the clip 17 after
pressure on the clip is released from being forced back by the
resiliency of the clip and possibly drawing some of the mixture, by
suction outwardly through the opening 22. Since the radius of the
inner wall of the clip 17 in the region holding the bag 23 is equal
to the radius of the external surface of the cylindrical wall of
the main chamber 10, the bag 23 is pressed completely flat and is
substantially completely empty when the ribs 18 snap into
engagement with the inner notches 20.
The vessel can then be shaken (e.g., in a mechanical shaker) for
thoroughly mixing the two combined substances. The pin 13 can be
pulled out of the nozzle 12 and the ready-mixed dental preparation
introduced directly into a cavity of a tooth by expelling the
compound through the nozzle 12 by means of the plunger 14. The
displacement of the plunger 14 inside the cylindrical main chamber
10 may possibly be effected by auxiliary means. The fact that the
internal wall of the portion 11 of the vessel and the facing
surface of the head of the plunger 14 are parts of spheres having
identical radii, substantially all the compounded preparation in
the chamber 10 can in practice be ejected.
In the compounding vessel illustrated in FIGS. 3 and 4 the main
vessel 10 is formed in the same way as in the previously described
embodiment with a part spherically domed portion 11 which is
centrally elongated into a delivery nozzle 12 which is closed by a
removable pin 13. The hollow plunger 14' in this embodiment is
extended rearwards beyond the end of the main chamber 10 and its
rear end is formed with a flange 30. The rear end of the main
chamber 10 is likewise formed with a flange 31. The internal wall
of the main chamber 10 is again of circular cylindrical shape,
whereas its external wall has a central portion which is square in
cross section, as can be seen in FIG. 4. In this region two
circularly cylindrical chambers 32 and 33 are attached to opposite
sides, their common axis extending centrally through holes 34 and
35 in each of the two corresponding side faces of the main chamber
wall. The two cylindrical accessory chambers are also formed with
flanges 36 at their free ends. The inner end of each accessory
chamber 32, 33 is closed by a destructible membrane 37 (e.g., of
foil) which also seals the corresponding holes 34 and 35 into the
main chamber 10. The other end of each accessory chamber is closed
by a slidably movable hollow plunger 38 which differs from plunger
14' in not having a hemispherical, but a flat inner face 39. The
accessory chamber 32, 33 may be affixed to the square side faces of
the main chamber 10 either with an adhesive, or they may be fused
or secured in some other convenient way. Flanges 41 provided on the
accessory chambers may be arranged to engage rails 42 formed on the
outside square faces of the main chamber 10.
The compounding vessel illustrated in FIGS. 3 and 4 is used by
first emptying the two accessory chambers 32 and 33 by pushing
their plungers 38 inwards, (possibly in a prescribed order
consecutively). If both chambers are emptied simultaneously
pressure can be applied to the terminal flanges 40 from both sides;
if each chamber is to be emptied separately, this can be done
manually by applying the thumb to one of the flanges, say 40, and
the index and second fingers to the other flange 36. Inward
displacement of the plunger 38 causes the membrane 37 to be
destroyed and the substance in the chamber, say a liquid, to be
forced through the appropriate hole 34 or 35 into the mixing
compartment of the main chamber 10. When all the substances have
been thoroughly mixed, possibly with the aid of a mechanical
shaker, the pin 13 is removed from the nozzle 12 and the finished
dental preparation can be ejected possibly directly into a dental
cavity by pressing the plunger 14' inwards.
Many of the features that have been described in connection with
each of the two above embodiments are interchangeable or applicable
in combination. For instance, the plunger 14 in the embodiment
according to FIGS. 1 and 2 may be rearwardly extended like the
plunger 14' and both plunger and main chamber may be provided with
terminal flanges. The compounding vessel according to FIGS. 3 and 4
may be fitted with only one accessory chamber. Conversely, the
vessel according to FIGS. 1 and 2 may be provided with two openings
22 and two bags 23 may be located either under a wider clip or
under two separate clips. When two separate clips are provided the
two bags can be emptied in succession. Instead of a single membrane
37 one or both the accessory chambers 32, 33 in the embodiment
according to FIGS. 3 and 4 may contain a destructible bag for the
reception of the substance in question FIG. 5 illustrates the
embodiment of the present invention in which more than one opening
is provided under a single clip. Hence, openings 22 and 24
correspond respectively to bags 23 and 25. The bags are positioned
over their respective openings, thereby permitting separate
components to be added to main chamber 10 without premixing. The
membranes or bags of the present invention can be of any suitable
material which has the characteristics of being compatable with the
components to be mixed, and which is easily rupturable upon
application of external pressure. For example, the material could
be metal foil, treated paper, cellophane and other materials within
the pen of a skilled artisan.
* * * * *