U.S. patent number 3,905,423 [Application Number 05/465,977] was granted by the patent office on 1975-09-16 for method of protecting well apparatus against contamination during handling.
This patent grant is currently assigned to Continental Oil Company. Invention is credited to Clarence B. Kolb, Jr., Derry D. Sparlin.
United States Patent |
3,905,423 |
Sparlin , et al. |
September 16, 1975 |
Method of protecting well apparatus against contamination during
handling
Abstract
A method of protecting downhole well apparatus having openings
therein or movable parts during handling of such apparatus,
particularly during positioning thereof in a wellbore, comprising;
filling the openings or coating the movable parts with a blend of a
wax and a polymer, handling the so-treated apparatus such as
positioning the same in a wellbore, and removing the filling or
coating blend from the openings or movable parts.
Inventors: |
Sparlin; Derry D. (Ponca City,
OK), Kolb, Jr.; Clarence B. (Ponca City, OK) |
Assignee: |
Continental Oil Company (Ponca
City, OK)
|
Family
ID: |
23849946 |
Appl.
No.: |
05/465,977 |
Filed: |
May 1, 1974 |
Current U.S.
Class: |
166/296;
166/376 |
Current CPC
Class: |
C09K
8/92 (20130101) |
Current International
Class: |
C09K
8/92 (20060101); C09K 8/60 (20060101); E21B
043/10 () |
Field of
Search: |
;166/296,295,294,280 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Novosad; Stephen J.
Attorney, Agent or Firm: Collins; Richard W.
Claims
What is claimed is:
1. A method of placing a cavitycontaining well apparatus downhole
in a wellbore comprising:
a. blending together from 25 to 80 parts by weight of a paraffin
wax heated to a temperature above its melting point and from 75 to
20 parts by weight of a polymer selected from the class consisting
of polyterpenes, polyvinyl acetates, polyolefins, polyamides and
rosin esters to form a melted wax-polymer blend having a softening
point 10-15.degree.F below its melting point,
b. filling the cavity of the well apparatus with the melted
wax-polymer blend,
c. solidifying the wax-polymer blend,
d. positioning the so-treated well apparatus downhole in a
wellbore, and
e. removing the wax-polymer blend from the cavity.
2. The method of claim 1 wherein the cavity is filled by brushing
the melted blend into the cavity.
3. The method of claim 1 wherein the blend is solidified by
allowing the blend to cool to ambient temperature.
4. The method of claim 1 wherein the apparatus is a screen, slotted
liner or packer.
5. The method of claim 1 wherein the blend is removed from the
cavity by contacting the blend with a solvent selected from the
group consisting of crude oil, diesel fuel, kerosene or xylene.
Description
BACKGROUND OF THE INVENTION
Field of the Invention
This invention relates to apparatus and methods for completing
wells. More particularly, it relates to such apparatus and methods
wherein an apparatus having openings, holes, apertures or
perforations therethrough to provide fluid flow channels through
the apparatus or an apparatus having moving parts is positioned
downhole in a well.
2. Description of the Prior Art
In completing wells it is often desirable to position downhole some
type of apparatus through which fluids are passed between the
wellbore and the surrounding formation. Such apparatus include
perforated liners, screens, packers and the like. One
characteristic of such apparatus is that they have cavities or
recesses such as an opening or openings therethrough through which
the fluid passes. The size of the openings may vary considerably
depending on the exact nature and intended use of the apparatus.
Other apparatus have movable parts which must be activated once the
apparatus has been positioned downhole. Such apparatus include
packers which have jaws which, once the packer is positioned
downhole, must be moved out to contact and bite into the
surrounding casing or borehole wall. Such apparatus are handled
repeatedly from the time they are manufactured until they are in
position downhole in a well ready for use. Such handling includes
packaging, shipping, unpackaging, storing and positioning in a
well. The apparatus are positioned downhole in a well by lowering
the same through a borehole, such as via a wireline or as a part of
the tubing string, to the desired position downhole. The borehole
through which the apparatus is lowered may be an open hole or may
be cased. During its passage through the borehole the apparatus
necessarily contacts and passes through any fluid or detritus which
may be in the wellbore and can scrape against the sides of the
cased or open borehole, especially if the borehole deviates from
the vertical. Throughout the handling and positioning operations
there are many opportunities for extraneous solid materials, such
as packaging materials, dirt, sand, detritus, drilling fluid
solids, pieces of the borehole sidewall rock and the like, to
contact and become lodged in the openings or movable parts of the
apparatus. The presence of these extraneous solid materials cuts
down or can even shut off flow through the apparatus or bind and
prevent movable parts from moving thus decreasing or destroying the
efficiency of the apparatus.
In order to protect the openings and movable parts in such
apparatus it is known to fill the openings and coat the movable
parts in the apparatus with a plugging material prior to
positioning the apparatus downhole. After the apparatus is
positioned, the plugging material melts away or is othewise removed
to clear the openings or leave the movable parts free of extraneous
materials. Previously known plugging or coating materials include
inorganic solids such as hydrated nitrates of chromium, iron,
mercury and nickel; pure organic compounds such as various acids,
and crude organic materials such as paraffin, gilsonite, beeswax,
metals and metallic alloys.
It is an object of this invention to provide an improved apparatus
and method for positioning downhole in a well an apparatus having
openings therethrough or movable parts. It is a further object to
provide such an apparatus and method wherein the openings are
plugged or movable parts coated with a removable plugging material
during the handling and positioning of the apparatus.
It is a still further object to provide such a removable plugging
material having improved bonding to the apparatus.
It is another object to provide an organic removable plugging
material which is harder than previously used organic
materials.
It is still another object to provide such an organic removable
plugging material which melts at a temperature lower than that of
the borehole in which it is positioned or can be removed from the
openings or movable parts by contacting the same with a
solvent.
Other objects, advantages and features of the invention will become
apparent from a consideration of the following specification and
appended claims.
BRIEF SUMMARY OF THE INVENTION
A method of protecting and maintaining open cavities or recesses
such as openings in or movable parts of apparatus during placement
of such apparatus downhole in a well comprising: (a) filling the
cavities of the apparatus with a blend of a wax and a polymer, and
(b) positioning the apparatus downhole in a well. If the
temperature of the borehole at the downhole location is higher than
the melting point of the wax-polymer blend, the well is shut in
until the blend melts. Alternatively or if the temperature of the
borehole is lower than the melting point of the blend, hot oil or
other solvent for the blend is flowed through the apparatus.
DESCRIPTION OF THE PREFERRED EMBODIMENT
Many types of liners and screens have been used for years to
control production of unconsolidated formation sand in oil, gas and
water wells. Common types of liners consist of tubing in which
slots or other holes of various sizes and configurations are cut.
Well fluids can pass from the formation through the slots into the
tubing and up the tubing out of the well, but sand or other
formation particles bridge in the slots and are prevented from
passing through the liner. Modifications of these liners can be
made, as by wrapping the exterior of the liner with wire or a
similar material which is spaced at regular intervals. Another
modification is a liner having the openings in it coated on the
exterior thereof by a permeable solid material such as plastic
coated sand or concrete. Such permeable coating acts as the filter
media and the liner itself acts as a base or form to support the
permeable coating. The process of this invention can be carried out
using any of these liners and screens.
Similarly the invention may be carried out using any downhole
apparatus which contains a part or element which must be moved in
relation to other parts or elements once the apparatus is
positioned downhole. Typical are packers which contain jaw members
which are in a contracted position during passage of the packer
through the borehole but which are moved out into contact with the
borehole sidewall once the packer has been lowered to its desired
location. Such apparatus have cavities or recesses between the
moving parts and the stationary parts.
The temporary plugging or blocking material of this invention is a
blend of a wax and a polymer. It has been found that wax alone does
not adhere well to the metal surfaces of the cavities which are to
be plugged. Also wax alone has too low a softening point compared
to its melting point. This means that with an apparatus being
positioned, which apparatus contains cavities filled with wax, the
wax softens before the apparatus reaches its final location. This
premature softening may result in the wax acutally attracting and
picking up undesired solid plugging material and holding the same
in the cavity area. Addition of a polymer to the wax forms a blend
having a softening point which is desirably close to the melting
point and which bonds better to metal than wax alone. Approximately
equal weights of wax and polymer are preferred. As little as 20
percent by weight polymer imparts a substantial increase in
softening point. More than about 75 percent by weight polymer
results in a blend with a softening point and melting point which
are too high for most applications.
The wax is preferably a synthetic paraffin wax having a softening
point not substantially below its melting point. The polymer may be
a solid polyvinyl acetate, a polyolefin such as a polyethylene, a
polyamide, a rosin-type polymer such as a rosin ester, for example
a glycerol ester of rosin or a synthetic polyterpene.
The softening point of the blend should preferably be within
10.degree. to 15.degree. of its melting point. The melting point of
the blend should be a temperature above ambient temperature and
equal to or slightly less than the temperature at which the
apparatus which is coated with the blend can be heated during use.
In well operations the melting point should be greater than the
surface temperature but equal to or less than the temperature of
the borehole in which a coated apparatus is positioned.
A series of tests were made to determine the strength with which
wax and wax-polymer blends adhered to metal. The metal used was two
rectangular mild steel specimens 3/16 inch by 1 inch by 2 1/4 inch.
Each specimen weighed approximately 24 grams. Various waxes and
wax-polymer blends were heated to above their melting point and
while still hot painted with a paint brush onto a 1 square inch
surface area on one side at the end of each specimen. The coated
areas of the two strips were then pressed together and held until
the coating cooled and solidified. The joined strips were then
vertically suspended by one end in an oven. The temperature was
slowly raised and the temperature at which one strip fell away from
the other strip was noted. This was taken as the softening
point.
Wax Polymer Melting Point* Steel Specimens Example (1 part by
weight) (1 part by weight) (.degree.F.) Separated (Softening
__________________________________________________________________________
Point.degree.F) 1 Paraffin Wax A none 146 - 153 129 2 Paraffin Wax
A Synthetic polyterpene 135 - 150 134 3 Paraffin Wax B none 160 -
165 147 4 Paraffin Wax B Synthetic polyterpene 165 - 170 163 5
Paraffin Wax C none 200 158 6 Paraffin Wax C Synthetic polyterpene
200 - 210 210
__________________________________________________________________________
*ASTM D127
The foregoing tests show that addition of a polymer to the wax
raised the softening point close to the melting point.
A test was made using a 2 foot long section of a 5 1/2 inch outside
"FEATHER " slotted liner having an inside diameter of 5 inches. The
section contained 18slots uniformly positioned around its lateral
sidewall. Each slot was 2 inches long, 1/8 inch wide at the
interior of the liner and feathering to 1/2 inch wide at the
outside of the liner. The liner was typical of those used in
producing wells in California which produce sand along with the
well fluids. A blend of 50 parts by weight paraffin wax D and 50
parts by weight synthetic polyterpene was mixed together at a
temperature of 220.degree.F and applied while hot by a paint brush
to the slots of the liner until all the slots were filled. The
coated liner was allowed to come to room temperature. The
wax-polymer blend hardened and adhered strongly to the slot
sidewalls. The coated liner was placed in an oven and observed as
the temperature was slowly increased. The blend began to melt at
215.degree.F. After 1.5 hours additional heating, the wax-polymer
blend had all melted and completely run out of the slots leaving
them open. The temperature of the oven had risen to
220.degree.F.
This test proved that the wax-polymer blend could be satisfactorily
placed in the slots of a liner and harden so that no extraneous
solid material could enter the slot. When the liner was heated to
above the melting point of the blend, the blend completely ran out
of the slots freeing the liner for use in passing fluids.
A sample of the above wax-polymer blend was mixed with a typical
California crude oil. The blend was completely soluble in the oil
at a temperature of 180.degree.F. Similar results were obtained
with diesel fuel, kerosene and xylene in place of crude oil. These
tests indicate that wax-polymer blend can be removed at a
temperature lower than the melting point of the blend by the use of
a solvent such as crude oil, diesel fuel, kerosene or xylene.
WELL EXAMPLE
A well in the San Miguelito Field of California was drilled through
an oil and gas pay zone extending from 12,780 feet to 13,265 feet.
Since other wells in the field were known to have sand problems, a
slotted liner was positioned opposite the pay zone and the well
placed on production. After six months on production the well
casing collapsed. This was believed due to sand being produced
through the liner along with the gas and oil causing the formation
sand to shift and exert sufficient pressure against the casing to
collapse it. The liner was pulled from the hole and examined. Some
of the slots were eroded. It was postulated that most of the slots
had become plugged while the liner was originally being placed in
the hole. Thus all production had occured through the few remaining
unplugged holes. The high flow rate through these few holes caused
the holes to be eroded by the loose formation sand which was
produced along with the oil. The bottom of the well was then
redrilled through the producing interval. The estimated bottom hole
circulating temperature of this well was 210.degree.F.
Seventeen 30 foot long sections of 2 7/8 inch diameter pipe was
perforated with twenty 1/4 inch diameter holes per foot. A
wax-polymer blend was prepared by mixing together 50 pounds of
paraffin wax having a melting point of 200.degree.F and a softening
point of 158.degree.F and 50 pounds of a synthetic polyterpene
polymer and heating to 210.degree.F. The blend softened and melted
at 201.degree.F. The melt was applied to the liner sections by
brushing a sufficient quantity into the holes to fill the holes.
The blend hardened when it cooled below 201.degree.F. The liner was
made up by coupling the seventeen sections together as the liner
was run into the open hole at the bottom of the casing. The liner
was positioned opposite the pay zone. The well was returned to
production and produced at the same rate, 200 barrels oil per day,
as before placement of the liner but at a decreased pressure drop.
No sand was produced. Six months after placement of the liner the
well was still producing satisfactorily with no sand problems.
These results indicate that the wax-polymer blend stayed in the
liner openings throughout the placement of the liner and kept sand
from entering the openings during placement. The high production
rate indicates that the wax-polymer blend melted and ran out of the
liner openings when the liner reached the pay zone which had a
temperature above the melting point of the blend. The decreased
pressure drop indicates that a large number of liner openings were
open and available for fluid production.
* * * * *