U.S. patent number 3,901,434 [Application Number 05/405,085] was granted by the patent office on 1975-08-26 for non-extruding lid seal for centrifuges.
This patent grant is currently assigned to Beckman Instruments, Inc.. Invention is credited to Herschel E. Wright.
United States Patent |
3,901,434 |
Wright |
August 26, 1975 |
Non-extruding lid seal for centrifuges
Abstract
A centrifuge rotor having chambers for sample containers and a
cover is formed with fluid release openings in the cover to form
what amounts to a pressure relief valve. The release openings
communicate with a seal-ring groove in the cover. This guards
against possible expulsion of the seal ring from the seal-ring
groove in the event that one or more of the containers should
rupture so that the fluid escaping from the container, producing
centrifugal force and fluid pressure acting upon the cover, should
bend it up sufficiently to open a gap for expulsion of the sealing
ring thereby permitting the fluid to escape. The provision of the
fluid release openings communicating between the seal-ring groove
and the exterior of the cover permits sufficient fluid to escape
through the opening in the event of partial distortion of the
sealing ring upon the bending of the cover to allow the cover to
return to sealing condition and to retain the remainder of the
fluid within the rotor.
Inventors: |
Wright; Herschel E. (Santa
Clara, CA) |
Assignee: |
Beckman Instruments, Inc.
(Fullerton, CA)
|
Family
ID: |
23602217 |
Appl.
No.: |
05/405,085 |
Filed: |
October 10, 1973 |
Current U.S.
Class: |
494/16; 137/860;
277/641; 277/928; 494/38; 277/910 |
Current CPC
Class: |
B04B
5/0414 (20130101); Y10S 277/91 (20130101); Y10S
277/928 (20130101); B04B 2007/025 (20130101); F16K
15/142 (20130101) |
Current International
Class: |
B04B
5/04 (20060101); B04B 5/00 (20060101); B04b
001/00 () |
Field of
Search: |
;277/29 ;251/DIG.1
;137/525 ;233/1A,1B,2R,26,27 |
References Cited
[Referenced By]
U.S. Patent Documents
Foreign Patent Documents
Primary Examiner: Smith; Robert I.
Attorney, Agent or Firm: Steinmeyer; R. J. Mehlhoff; F.
L.
Claims
What is claimed is:
1. In a rotating receptacle having a chambered rotor and a cover
therefor, a fluid pressure and centrifugal force relieving seal
comprising:
confronting peripheral portions of the rotor and the cover having
confronting, normally contiguous, contacting surfaces, one of the
members comprising the rotor and the cover having an annular groove
at the confronting surface thereof, said groove having a first wall
substantially parallel to the plane of the contacting surfaces and
an outer cylindrical wall intersecting the first wall, the grooved
member having a pressure-releasing hole extending to the exterior
thereof from the intersection of said intersecting walls, and
a resilient deformable sealing ring in said groove of such
cross-sectional dimensions as normally to lie tangent to walls of
the groove in the grooved member and to the confronting surface of
the other member for sealing the confronting surfaces, whereby
distortion of either of the members by fluid pressure or
centrifugal force causing parting of the confronting surfaces of
sufficient magnitude to distort the sealing ring out of tangency
with either of the said groove walls opens said hole to permit
release of sufficient fluid pressure to permit restoration of
contact between said contiguous surfaces.
2. The seal defined in claim 1 wherein the pressure releasing hole
extends radially.
3. The seal defined in claim 1 wherein the cover is the grooved
member.
4. The seal defined in claim 1 wherein the cover is the grooved
member and the pressure releasing hole extends parallel to the axis
of rotation of the rotor.
5. The seal defined in claim 1 wherein the rotor is the grooved
member.
6. The seal defined in claim 5 wherein the pressure releasing hole
extends radially.
Description
BACKGROUND OF THE INVENTION
Fixed angle centrifuge rotors have been provided with a body having
cavities for sealed sample tubes and a lid for the body with a seal
to isolate the interior of the rotor from the high vacuum
environment of the centrifuge chamber. This isolation is desirable
to prevent possible leakage of contents of the centrifuge tubes
from contaminating the vacuum system if the contents are corrosive
or infectious. Conventional lid seal systems have been satisfactory
for preventing minor leakage but difficulties may arise in case of
a gross leakage resulting from faulty tubes or improper assembly
techniques.
In case of a gross leakage, the rotor lid flexes under the
influence of increasing fluid pressure so that the lid may bend far
enough away from the rotor body to open a gap large enough to
permit the seal ring to be expelled from the rotor. In that event,
at least the seal ring must be replaced, and at most it can cause
severe rotor imbalance, permanent lid deformation and great
difficulty in lid removal.
It is accordingly an object of the invention to overcome the
difficulties of existing centrifuge constructions and to make the
centrifuge in such a manner as to form a pressure sensitive relief
valve which will release only sufficient fluid to permit
re-establishment of contact of the seal ring in the seal ring
groove after a build up of fluid pressure has caused the rotor lid
and the body of the rotor to part somewhat, and to distort the seal
ring partially.
Other and further objects, features and advantages of the invention
will become apparent as the description proceeds.
SUMMARY OF THE INVENTION
In carrying out the invention in a preferred embodiment of a
centrifuge rotor having a vertical axis of rotation, the rotor is
generally formed in a conventional manner with a body having an
interior adapted to hold, in inclined positions, sealed tubes of
samples to be centrifuged and having a cover or lid for the body
with a seal between the lid and the rotor body to prevent fluid
from escaping from the rotor in case some defect should cause some
leakage of fluid from one or more of the sample tubes. In
conventional apparatus the seal consists of a deformable sealing
ring in an annular sealing groove formed in the cover at the
surface thereof which confronts a contiguous surface of the body of
the rotor.
However, in accordance with the invention, one or more openings are
provided from the intersection of the horizontal and outer vertical
walls of the sealing ring groove to release some of the fluid in
case of a gross leakage from the tubes permitting fluid to escape
from the tubes to the interior of the body of the rotor. Release of
some fluid relieves the pressure of fluid which has escaped from
the sample tubes sufficiently to permit the gap between the cover
and the body of the rotor caused by such fluid pressure to close
again and to restore the sealing ring to its normal position in the
groove to prevent expulsion of the sealing ring from its groove and
to retain the remainder of the fluid in the interior of the
rotor.
A better understanding of the invention will be afforded by the
following detailed description considered in conjunction with the
accompanying drawing.
DRAWINGS
In the drawings:
FIG. 1 is a fragmentary view of a section cut by a plane through
the vertical axis of rotation of a fixed angle centrifuge rotor
forming an embodiment of the invention;
FIG. 2 is a half, top plan view of the embodiment of FIG. 1;
FIG. 3 is a series of diagrams fragmentarily illustrating the
sealing ring portion of a conventional construction and
illustrating the manner in which the sealing ring is expelled and
the entire body of fluid in the interior of a centrifuge rotor is
permitted to escape in the event that a gross leakage of fluid from
a tube in the centrifuge should take place and exert fluid pressure
and centrifugal force tending to pry up the cover of the rotor;
FIG. 4 is a series of diagrams corresponding to the diagrams of
FIG. 3 illustrating the behavior of a centrifuge rotor constructed
in accordance with the invention under the conditions represented
in FIG. 3 and illustrating the manner in which pressure is relieved
to prevent expulsion of the sealing ring and permit reclosure of
the gap between the cover and the rotor body;
FIG. 5 is a pair of diagrams fragmentarily representing the sealing
ring portion of the rotor in accordance with a modified embodiment
of the invention.
Like reference characters are utilized throughout the drawing to
designate like parts.
DETAILED DESCRIPTION
In a typical fixed angle centrifuge rotor, the rotor is formed with
a body 11 having a vertical axis of rotation 12 and provided with a
cover 13. The body has an externally threaded stem 14 to receive an
internally threaded handle 15 to secure the cover 13 upon the body
11. The body has inclined chambers 16 for receiving tubes 17 of
fluid samples to be centrifuged and the tubes 17 are provided with
caps 18 which normally seal in the contents of the tubes 17. There
is some space in the interior of the body 11 above each sample
chamber 16 and under the cover 13 to form a cavity 19 into which
fluid from the tubes 17 may escape in the event that any of them
should be defective or improperly mounted or the caps 18 should
have defective seals.
In order to retain such escaping fluid in the interior of the
rotor, there are sealing rings 21 and 22, retained in annular
grooves 23 and 24, respectively.
The sealing rings serve to prevent escape of any fluid in the
cavity 19 when there is a minor leakage from one or more of the
tubes 17. However, in the event of a gross leakage, sufficient
centrifugal force and fluid pressure may build up under the cover
13 to bend up the outer edges and cause confronting faces 25 and 26
(shown in FIG. 3) of the body 11 and the cover 13, respectively, to
part and form a gap 27 as shown in FIG. 3B.
In accordance with the invention, the construction is arranged to
provide means for discharging fluid until fluid pressure has been
sufficiently relieved. In the embodiment of the invention
illustrated in FIGS. 1, 2 and 4, this is accomplished by providing
holes 28 in the cover 13 extending to the exterior from the
intersection of the plane-surfaced wall 31, perpendicular to the
rotor axis of rotation 12, and the cylindrical-surface outer wall
32 of the annular groove 24 which is concentric with the rotor axis
of rotation 12. This provides a discharge passageway from the
peripheral groove 24 to the exterior of the rotor.
PRIOR ART OPERATION
The performance in a typical prior art construction when gross
leakage of fluid from sample tubes builds up and a quantity of
fluid is present in the cavity 19 is illustrated in FIG. 3. If
there is a sufficient body of fluid 33 which, being subject to
centrifugal force, exerts a fluid pressure to pry the
circumferential portion of the cover 13 upward, the confronting
surfaces 25 and 26 part so that they are no longer contiguous as
illustrated in FIG. 3A and form a gap 27 as illustrated in FIG. 3B.
Fluid pressure acting upon the sealing ring 22 tends to deform it
as illustrated in FIG. 3B, pressing it away from the inside wall 34
of the groove 24. If the body of fluid 33 builds up as illustrated
in FIG. 3C, there is still greater centrifugal force and fluid
pressure so that the gap 27 becomes still greater and there is
still further distortion of the shape in cross section of the
sealing ring 22. Then when the bending force upon the cover 13 has
become sufficiently great, the surfaces 25 and 26 part to such an
extent as to form a gap 27 of sufficient width that the force of
the liquid on the sealing ring 22 causes the ring to be expelled
instead of merely being partially extruded and the entire body of
liquid 33 escapes from the rotor. This has several deleterious
effects.
Not only is the body of liquid lost in the vacuum lines and is the
centrifuge system subjected to the contamination or corrosion of
the entire body of fluid, but the cover 13 may be warped or
distorted to such an extent as to be permanently damaged. Moreover,
there may be great difficulty in removing the cover 13 and at the
very least a new sealing ring 22 must be installed. Still worse,
the distortion of the rotor cover 13 may cause such serious
imbalance of the rapidly rotating rotor as to damage the mountings
or create a safety hazard.
OPERATION IN ACCORDANCE WITH THE INVENTION
The results of the presence of a body of leakage fluid 33 in a
rotor having the relief passageway 28 is illustrated in FIG. 4.
Before the leakage of fluid 33 into the cavity 19 takes place, the
confronting surfaces 25 and 26 are properly in contact, as
illustrated in FIG. 4A. Then upon the presence of leakage fluid 33,
as illustrated in FIG. 3B, a parting of confronting surfaces again
takes place and the sealing ring 22 is partially extruded into the
gap 27 as a result of deformation thereof.
With a still greater mass of fluid 33, as illustrated in FIG. 4C,
still greater distortion and extrusion of the sealing ring 22 take
place. As in the case of FIG. 3C, the sealing ring 22 is also
pressed away from the inner wall 34 of the groove 24 so that
sealing no longer takes place at this wall. Moreover, the sealing
ring 22 also begins to be pulled away from the upper wall 31 of the
groove 24, thus breaking the seal between the ring 22 and the upper
wall 31. Consequently, as shown in FIG. 4D, there is an open escape
passageway for the body of fluid 33 from the gap 35 between the
parted surfaces (but inward from the ring 22 which is still
retained in the groove 24 because the confronting surfaces have not
sufficiently parted to permit the expulsion of the ring 22), the
space between the ring 22 and the inner wall 34 of the groove 24,
the space between the ring 22 and the upper wall 31 of the groove,
and the hole 28.
Consequently, a small stream 36 of fluid is discharged. However, as
soon as this occurs, the mass of fluid 33 is reduced, there is no
longer sufficient centrifugal force and fluid pressure to cause the
parting of confronting surfaces which resulted in the gap 35 so
that the gap recloses and the confronting surfaces 25 and 26 are
again in contact as illustrated in FIG. 4A.
It will be observed that the discharge of fluid from the hole 28
has taken place before the gap 35 has become great enough to permit
expulsion of the sealing ring 22. Consequently, the sealing ring 22
is retained in the annular groove 24; the seal by the ring 22
between the surface 25 of the body 11 of the rotor and the surfaces
of the groove 24, particularly in the upper wall 31 and the outer
wall 32, is restored so that there is again a complete seal between
the cover 13 and the body 11. Thus, a condition of equilibrium
exists in which a maximum amount of fluid is retained in the rotor
without the risk of the severe consequences associated with sealing
systems not having the pressure relief means described. In this
way, the construction described is basically a relief valve which
is pressure sensitive. Fluid release may be provided either by the
vertical openings 28, or by radial openings 28'.
By way of illustration an embodiment of the invention has been
illustrated and described in which pressure relief is achieved by
means of the holes 28 in the cover 13 extending to the exterior
from the intersection of the upper and outer walls of the groove
24. However, the invention is not limited thereto and does not
exclude other means for providing such pressure relief. For
example, as illustrated in FIG. 5A and FIG. 5D, one or more fluid
release openings 37 may be provided in the peripheral walls of the
rotor body 11 which extend from the intersection 38 of the lower
wall 39, perpendicular to the rotor axis of rotation, and the outer
cylindrical wall 41 of an annular groove 42 formed in the surface
25 of the body 11.
While certain embodiments of the invention have been fully
illustrated and described, it will be obvious to those skilled in
the art that various modifications and alterations may be made
therein and it is intended to cover all such modifications and
alterations as may fall within the spirit and scope of the
invention.
* * * * *