U.S. patent number 3,861,652 [Application Number 05/306,921] was granted by the patent office on 1975-01-21 for mixing device.
This patent grant is currently assigned to E. I. du Pont de Nemours and Co.. Invention is credited to Richard Allen Clark, John William Coryell.
United States Patent |
3,861,652 |
Clark , et al. |
January 21, 1975 |
MIXING DEVICE
Abstract
The use of a screen structure between groups of static mixing
elements located in a conduit through which tow or more liquids
flow increases mixing efficiency.
Inventors: |
Clark; Richard Allen
(Waynesboro, VA), Coryell; John William (Waynesboro,
VA) |
Assignee: |
E. I. du Pont de Nemours and
Co. (Wilmington, DE)
|
Family
ID: |
23187470 |
Appl.
No.: |
05/306,921 |
Filed: |
November 15, 1972 |
Current U.S.
Class: |
366/336 |
Current CPC
Class: |
B01F
5/0612 (20130101); B01F 5/0694 (20130101); B01F
5/0682 (20130101) |
Current International
Class: |
B01F
5/06 (20060101); B01f 015/02 () |
Field of
Search: |
;259/4,18,36,60
;138/38 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Jenkins; Robert W.
Claims
What is claimed is:
1. In a device for mixing a plurality of flowing liquids including
a hollow cylindrical tube and a plurality of curved mixing elements
positioned in said tube, the improvement comprising: said elements
being formed in spaced groups and a cylindrical shaped screen
positioned between at least two spaced groups of elements, said
screen having a diameter less than the diameter of the conduit,
said screen being connected to the walls of the conduit at one end
and being closed at the other end.
2. The device as defined in claim 1, including a second cylindrical
shaped screen positioned between said groups of elements, said
second screen being the same as the first screen and having its
closed end adjacent the closed end of the first screen.
Description
BACKGROUND OF THE INVENTION
This invention relates to a device for mixing two or more liquids
of highly differing viscosities. In particular, the invention is
concerned with an improvement on a mixer having no moving
parts.
Armeniades et al., in U.S. Pat. No. 3,286,992 disclose a mixer that
consists of a hollow tube or pipe containing a series of curved
dividing elements that provide repeated division and recombination
of the materials to be mixed as they flow through the tube. The
chief mechanisms for accomplishing mixing in such a device are flow
division and radial mixing. Flow inversion and backmixing
contribute to a lesser extent. Where miscible liquid systems are
being combined, diffusion across the flow strata in the mixer
enhances mixing somewhat. However, for an all-liquid system in
which the constituents possess widely differing viscosities, mixing
performance is determined almost exclusively by the amount of flow
division attained. In such systems in which the viscosity ratio of
the liquids is 1,000 or higher, globules or "islands" of the high
viscosity component tend to form after passing the first few curved
dividing elements of the mixer. These discrete particles then pass
the remaining elements essentially unchanged. This problem is
aggravated in those systems in which the low viscosity component is
in volumetric excess.
Attempts to overcome this problem by increasing the number of
dividing elements often result in a prohibitively large pressure
drop through the mixer. The problem of excessive pressure drop
through such mixers is recognized by Grout et al., U.S. Pat. No.
3,664,638.
SUMMARY OF THE INVENTION
It has been found that the problem of undissolved high viscosity
inhomogeneities in such systems may be overcome by the use of one
or more fine mesh screens or other foraminous structures placed
between sets of Armeniades et al. mixer elements. The use of a
screen between the mixer elements greatly increases the mixing
efficiency. Thus, fewer mixer elements are needed and a lower
pressure drop results.
BRIEF DESCRIPTION OF THE DRAWING
FIG. 1 is a partially sectioned view of one embodiment of the
invention, showing a screen section between mixing sections;
FIG. 2 is a partial perspective view partly in section of the
screen section of FIG. 1.
DETAILED DESCRIPTION OF THE ILLUSTRATED EMBODIMENT
In the drawing, a hollow cylindrical tube 10 of uniform cross
section consists of a premixing section 12, an initial mixing
section 13, a screen section 14 and a final mixing section 15. Low
viscosity liquid A is fed directly into premixing section 12 and
high viscosity liquid B is introduced through flow distributor 16
having several orifices 17. From delivery end 18 of the tube issues
a homogeneous mixture of A and B. Within the initial mixing section
13 and final mixing section 15 of tube 10 are sets of curved
elements 20, 21, 22, etc., and 30, 29, etc., respectively. As more
fully described in the aforementioned Armeniades et al. patent, the
downstream edge of each of the elements 20, 21 . . . 29, 30, are
positioned at a substantial angle to the upstream edge of the next
adjacent one. The elements are preferably physically connected,
e.g., by welding or brazing at their contact point 33. Two
cylindrical screens 34 having solid end plates 36 are mounted in
the end walls 35 of screen section 14.
The screens placed between sets of the curved mixer elements are
positioned in such a way that the liquid stream is required to pass
through the meshes of the screens. The screens may be planar,
cylindrical or of any desired shape. If planar, they are
conveniently positioned transversely in the hollow tube between
sets of the mixing elements. If cylindrical, they may be
positioned, for example, as shown in the drawing. In general, a
screen having a mesh opening approximately equal to the maximum
particle size of the undissolved high viscosity globules gives
satisfactory results. In such a case, the screen does not serve as
a filter since the average particle size is smaller than the mesh
opening. However, the invention will operate satisfactorily even if
the average particle size is not smaller than the mesh opening.
Usually screens of 100 mesh or finer will be effective and are
preferred.
In an example, a mixer consisting of a set of 35 Armeniades et al.
elements followed by two 200-mesh cylindrical screens followed in
turn by a set of 21 elements produced complete mixing in the
following system: 4 parts of a high viscosity liquid (440 poises)
and 6 parts of a low viscosity solvent (1 centipoise) at
30.degree.C. The viscosity ratio was 44,000/1. Good mixing was
indicated by no discernible globules of the high viscosity
component in the effluent and no buildup on the screens. Similar
results were obtained in a two component liquid system having a
viscosity ratio of approximately 150,000/1.
In the operation of the embodiment illustrated in the drawing, it
is preferred that the coaxially oriented flow distributor 16 and
the initial mixing section 13 be disposed within 10.degree. of a
vertical position, most preferably, absolutely vertical. Flow
direction, either up or down, has not been found to make a
significant difference in efficiency of mixing.
The concept of using fine mesh screens between sets of Armeniades
et al. mixer elements for the purpose of dividing or dispersing the
higher viscosity component is applicable to any liquid system. It
is especially beneficial in those cases where precise drop size is
a critical objective or in those instances where an excessive
number of mixer elements would otherwise be required to achieve the
desired degree of mixing and/or in obtaining homogeneous mixing
with minimum pressure drop.
Although the invention has been described using two spaced groups
of elements or mixing sections 13, 15 of the same diameter, more
than two mixing sections as well as mixing sections of differing
diameters may be used with a screen section incorporated between at
least two of the mixing sections.
* * * * *