U.S. patent number 3,853,011 [Application Number 05/369,195] was granted by the patent office on 1974-12-10 for method and apparatus for the suction removal of a liquid.
Invention is credited to Heinrich Baumann.
United States Patent |
3,853,011 |
Baumann |
December 10, 1974 |
METHOD AND APPARATUS FOR THE SUCTION REMOVAL OF A LIQUID
Abstract
A method and apparatus for removing a liquid sample from a
liquid-containing receptacle without contaminating the remaining
liquid, characterized by the provision of a suction conduit that is
arranged in spaced relation above the liquid in the receptacle,
said suction conduit having an inlet orifice that is spaced a given
distance from the liquid level. A source of suction pressure is
connected with the other end of said suction conduit to establish a
uniform flow of fluid from the receptacle to the suction conduit.
Means are provided for continuously lowering the inlet orifice end
of the suction conduit at the same rate that the level of liquid
decreases, thereby to maintain constant the given spacing distance
between the inlet orifice and the liquid level and, consequently,
the flow of liquid from the receptacle into the suction
conduit.
Inventors: |
Baumann; Heinrich (CH-4912
Aarwangen, CH) |
Family
ID: |
4345787 |
Appl.
No.: |
05/369,195 |
Filed: |
June 12, 1973 |
Foreign Application Priority Data
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Jun 14, 1972 [CH] |
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8880/72 |
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Current U.S.
Class: |
73/864.24;
422/922 |
Current CPC
Class: |
G01N
35/10 (20130101); B01L 3/021 (20130101); F04F
3/00 (20130101) |
Current International
Class: |
B01L
3/02 (20060101); G01N 35/10 (20060101); F04F
3/00 (20060101); G01n 001/14 () |
Field of
Search: |
;73/421,423A ;210/83
;23/259 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Swisher; S. Clement
Attorney, Agent or Firm: Laubscher; Lawrence E.
Claims
What is claimed is:
1. Apparatus for removing a quantity of liquid from a receptacle
without contaminating the remaining liquid, comprising
a. a suction conduit having at one end an inlet orifice;
b. means supporting said suction conduit above the liquid contained
in said receptacle with the inlet orifice spaced a given distance
from the liquid level;
c. a source of suction pressure connected with the other end of
said suction conduit, the pressure of said suction source being
sufficient to establish a flow of liquid from said receptacle into
the suction conduit via said inlet orifice; and
d. means for continuously lowering the inlet orifice end of said
suction conduit at the same rate that the level of liquid in the
receptacle decreases upon removal of liquid therefrom, thereby to
maintain constant the spacing distance between the liquid level and
inlet orifice, and the flow of liquid from said receptacle into
said suction conduit via said inlet orifice, whereby the lower end
and outer surfaces of the suction conduit are maintained free from
contact with the liquid in the receptacle.
2. Apparatus as defined in claim 1, wherein said suction conduit
lowering means comprises cam and follower means including a rotary
cam, an axially reciprocating cam follower member, and spring means
biasing said cam follower member into engagement with said rotary
cam.
3. Apparatus as defined in claim 2, wherein the cam surface of said
rotary cam has a configuration to effect, in succession:
a. rapid displacement of the inlet orifice end of said suction
conduit from a position remote from the liquid level to the
position adjacent and spaced the given distance from said liquid
level;
b. progressively lowering of the inlet orifice end of the suction
conduit at a uniform rate; and
c. rapid withdrawal of the inlet orifice end of the suction conduit
from the receptacle.
4. Apparatus as defined in claim 2, wherein said suction conduit
remains connected with said suction pressure source when the
orifice end of the suction conduit reaches its lower limit of
travel, whereby the flow of liquid to said suction conduit is
terminated and ambient drying fluid is drawn into the suction
conduit.
Description
This invention relates to an improved method and apparatus for
removing samples of liquid from a liquid-containing receptacle in a
contamination-free manner. More particularly, the liquid is removed
from the receptacle by means of a suction conduit the outer
surfaces of which are prevented from coming into contact with the
liquid in the receptacle.
It is well known in the prior art to remove liquid from a
receptacle by means of a syphon tube, suction conduit, or the like.
One problem inherent in such known devices is that the inlet
orifice of the vacuum pressure removal means is submerged below the
upper level of the liquid in the receptacle, whereby the liquid in
the receptacle is subject to contamination by materials carried by
the outer surfaces of the removal means. In the case where liquid
samples are to be removed from a plurality of receptacles by a
single suction removal means, quite often the specimen from one
receptacle clings to the outer surfaces of the suction means and is
transferred thereby to a subsequent receptacle. This contamination
is particularly undesirable when analyzing various liquids such as
blood with which various reactants are mixed prior to examination
by photometric analyzing means of the type in which a light beam is
directed through the mixture to determine a physical characteristic
thereof (for example, the opacity of the mixture). Also, this
buildup of residues on the outer surfaces of the suction removal
means forms an undesirable porous layer that often acts as a sponge
for absorbing materials that would contaminate liquid in a
subsequent receptacle into which the suction removal means are
submerged. The present invention was developed to avoid the above
and other drawbacks of the known suction removal systems.
Accordingly, the primary object of the present invention is to
provide an improved method and apparatus for removing a liquid
sample from a receptacle by means of a suction conduit the end and
outer surfaces of which are maintained out of contact from the
liquid in the receptacle whereby contamination of liquid in the
receptacle is avoided. In accordance with the present invention,
the suction conduit is arranged with its inlet orifice spaced a
given distance above the level of the liquid in the receptacle,
whereupon suction is applied to the other end of the suction
conduit to initiate discharge flow of the fluid from the receptacle
into the suction conduit. Means are provided for lowering the inlet
orifice end of the suction conduit at the same rate that the level
of the liquid descends during removal of the liquid from the
receptacle, thereby to maintain constant both the spacing distance
between the inlet orifice and the liquid level, and the flow of
liquid from the receptacle into the suction conduit.
In accordance with a further object of the invention, after the
desired quantity of fluid has been removed from the receptacle, the
suction conduit is maintained stationary while the suction force
continues to be applied to the other end of a suction conduit.
Consequently, the flow of liquid from the receptacle into the
suction conduit will be terminated, and the ambient gaseous fluid
(normally air) will be drawn through the suction passage to
completely dry the inner wall surfaces thereof.
In accordance with a further object of the invention, the inlet
orifice end of the suction conduit is displaced vertically relative
to the level of the liquid in the receptacle by means of rotary cam
and axially displaceable cam follower means. The cam configuration
is such that initially the inlet orifice end of the suction conduit
is quickly brought from a remote position to the desired position
spaced from the liquid level, whereupon the inlet orifice end is
continuously lowered at a uniform rate corresponding with the rate
of decrease of the liquid level. The inlet end of the suction
conduit is then quickly returned to its original remote position by
the cam follower means, whereupon a further receptacle may be
conveyed in position for removal of a specimen sample.
Other objects and advantages of the present invention will become
apparent from a study of the following specification when viewed in
the light of the accompanying drawing, in which:
FIG. 1 is a diagrammatic illustration of the liquid sample removal
means of the present invention; and
FIG. 2 is a detailed diagrammatic illustration of the
contamination-free manner in which the liquid sample is drawn from
the upper surface of the liquid in the receptacle.
Referring first to FIG. 1, a succession of identical receptacles 2
are transported by conveyor means 4 longitudinally of a trough 6
containing a liquid bath 8. The receptacles contain uniform
quantities 10 of a liquid to be analyzed (for example, blood
specimens). Preferably the liquid bath has a controlled temperature
(which, in the case of a blood specimen, may be 37.degree. C.),
whereby the temperature of the liquid specimen is controlled
accordingly.
In accordance with the present invention, means are provided for
removing portions of the liquid specimens from a receptacle without
contaminating the remaining liquid. To this end, there is provided
a suction conduit 12 having at one end an inlet orifice 12a.
Connected with the other end of the suction conduit is a source of
vacuum pressure 14. The inlet orifice end of the suction conduit 12
is connected with a vertically-arranged axially-displaceable cam
follower member 16 that is elevated and lowered, respectively,
relative to the corresponding receptacle 2 by the rotary cam member
18. The configuration of the cam 18 is such that when a given
receptalce is conveyed to the sample removal position I directly
beneath the cam follower, the cam follower is displaced quickly
downwardly by the cam 18 to lower the inlet end of the suction
conduit from a remote position to a position immediately adjacent,
but spaced the given distance "d" (FIG. 2) from, the level of the
liquid. Owing to the vacuum established within the suction conduit
by the vacuum pressure source, there is initiated a flow of liquid
from receptacle 2 to the suction conduit 12 via orifice 12a. As
shown in FIG. 2, this fluid flow is established with the lower end
and outer wall surfaces of the suction conduit completely out of
contact from the liquid 10 in the receptacle 2. Owing to the
contour of the rotary cam, the inlet orifice end of the suction
conduit is progressively lowered at a given rate substantailly
equal to the rate at which the liquid level decreases during the
suction removal process, whereby the spacing distance "d" between
the inlet orifice 12a and the liquid level, and the flow of liquid
into the suction conduit, are maintained constant.
When the cam follower 16 reaches its lower limit of travel, the
suction on the suction end of the conduit 12 is continued, whereby
ambient air is drawn through the conduit to prevent drops of the
removed sample from being discharged by gravity from the suction
conduit into the receptacle, or from forming an undesirable film or
residue on the inner wall surface of the suction conduit. At the
end of this drying instant, the cam follower is quickly displaced
upwardly by the biasing spring 20 and the contour of the cam 18 to
rapidly withdraw the inlet end of the suction conduit to its
initial remote position. Preferably the conveyor 4 is a
step-by-step conveyor having dwell periods slightly greater than
the time required for one complete revolution of the cam 18.
It is important to note that, in accordance with the present
invention, at no time does the outer surface 12b of the suction
conduit 12 come into contact with the liquid 10, whereby
contamination of the fluid in any receptacle by the suction conduit
is positively avoided.
While in accordance with the Patent Statutes the best form and
embodiment of the invention has been illustrated and described, it
will be apparent that various modifications may be made without
deviating from the disclosed inventive concepts.
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