U.S. patent number 3,791,917 [Application Number 05/338,826] was granted by the patent office on 1974-02-12 for process for producing kraft paper laminate of top stock and base stock layers.
This patent grant is currently assigned to Bird Machine Company, Inc.. Invention is credited to Joseph A. Bolton, III.
United States Patent |
3,791,917 |
Bolton, III |
February 12, 1974 |
PROCESS FOR PRODUCING KRAFT PAPER LAMINATE OF TOP STOCK AND BASE
STOCK LAYERS
Abstract
A process is disclosed for producing kraft paper laminate of top
stock and base stock layers from kraft fiber slurry digested to
high yield, wherein the digested slurry is subjected to fine
screening to separate from about 10% to about 30 percent of its
fiber, substantially all of the separated fibers being suitable for
top stock, and forming the top stock and bottom stock layers of the
laminate respectively from the so separated fibers and the
remaining fibers of the slurry.
Inventors: |
Bolton, III; Joseph A. (North
Attleboro, MA) |
Assignee: |
Bird Machine Company, Inc.
(South Walpole, MA)
|
Family
ID: |
23326319 |
Appl.
No.: |
05/338,826 |
Filed: |
March 7, 1973 |
Current U.S.
Class: |
162/55; 162/130;
162/188 |
Current CPC
Class: |
D21F
1/00 (20130101); D21B 1/12 (20130101); D21H
27/30 (20130101); D21H 11/04 (20130101) |
Current International
Class: |
D21F
1/00 (20060101); D21B 1/12 (20060101); D21H
11/04 (20060101); D21H 27/30 (20060101); D21H
11/00 (20060101); D21B 1/00 (20060101); D21h
005/00 (); D21h 001/02 () |
Field of
Search: |
;162/130,129,188,55,132,13 |
References Cited
[Referenced By]
U.S. Patent Documents
Other References
Pulp and Paper Manufacture, Volume III; 2nd Edition McGraw-Hill
Book Company, New York 1970 pp. 131-147..
|
Primary Examiner: Bashore; S. Leon
Assistant Examiner: Alvo; M. Steven
Claims
I claim:
1. A process for producing a kraft paper laminate of top stock and
base stock layers from kraft fiber slurry which has been digested
to a yield of at least 54 percent, which comprises the steps
of:
subjecting said digested slurry to fine screening to separate said
slurry into a first fraction passing through said screen and a
second fraction not passing through said screen, said first
fraction containing between about 10 and about 30 percent of the
total fiber content of the slurry which consists substantially only
of the shorter fiber having characteristics suitable for top stock,
said second fraction containing the remaining, mainly longer fibers
of said slurry;
utilizing fiber of said first fraction in forming the top stock
layer of said paper; and
utilizing fiber of said second fraction in forming the base stock
layer of said paper.
2. A process according to claim 1 wherein said first fraction
contains about 20 percent of the total fiber content of said slurry
and is utilized in substantial entirety to form said top stock
layer.
3. A process according to claim 1 wherein the fiber of said first
fraction is washed, and the fiber of said second fraction is
refined and washed, prior to said forming steps.
4. A process according to claim 1 wherein all the fiber of said
digested slurry is washed and refined prior to said screening
step.
5. A process according to claim 1 wherein said slurry is subjected
to said screening in a screening zone defined between a co-axial
screen and rotor both of substantially circular cross-section, the
rotor providing pulses of high frequency and intensity in said zone
to prevent plugging of said screen.
6. A process according to claim 1 wherein said first fraction
contains only fiber which will pass through screening apertures of
a diameter not exceeding about 0.06 inch.
7. A process according to claim 6 wherein said first fraction
contains only fiber which will pass through screening apertures of
a diameter of 0.55 inch.
8. A process according to claim 1 wherein said first fraction
contains only fiber which will pass through screening slots of a
width not exceeding about 0.02 inch.
Description
BACKGROUND OF THE INVENTION
1. Field of the Invention
This invention relates to a process for producing a kraft paper
laminate of top and base stock layers from high yield kraft
slurry.
2. Description of the Prior Art
Although it has other uses, kraft paper laminate of the type
concerned is used primarily in the production of box board, in
which a corrugated paper liner is adhesively secured between two
sheets of the kraft paper. So prevalent is this use that paper
machines for forming the two superposed layers of the paper
laminate have come to be known as "liner-board machines."
The top and base stock layers, and the kraft fibers that go into
them, have markedly different characteristics. The top stock layer,
usually the only side exposed, is relatively thin and needs high
quality fibers which are short and flexible for strength,
smoothness, and brightness. The thicker base layer can tolerate
some fibers of lower quality such as long fiber "shives."
The kraft fiber slurry used for each layer is produced from the
wood in digesters, which may be of the continuous or batch types,
wherein the wood chips are subjected to chemical action in the
presence of heat and pressure. The "yield" of a digester is
expressed as the percentage of oven dry (O.D.) wood in the slurry
leaving the digester to the O.D. wood fed to the digester. Yield
varies inversely with the length and severity of the digestion
treatment; whereas, the quality of the slurry varies directly
therewith. The quality of the slurry varies inversely with the
percentage of "rejects" which it contains, this percentage being
commonly accepted as the proportion that will not pass a "10 cut
flat screen" (slots about 0.01 inch wide by 1 1/2 inch long).
Except at low yields, continuous digesters produce less rejects and
hence better quality stock at a given yield than do batch
digesters.
In general, what is presently regarded as high yield digestion has
a yield of 54 percent or higher while lower yields may be classed
as "medium" if about 50 percent or above or "low" if lower.
The mills have strong incentives to digest to high yields. One of
these is savings in wood cost, since an increase of yield of only a
few per cent can save a mill as much as a million dollars or more
annually in wood cost. Also, high yield digestion requires less
chemicals and digester capacity, again saving substantial cost,
with a corollary advantage that the lower amount of chemical can be
more completely removed from mill waste water, with consequent
benefit to the ecology. Less waste fiber in high yield kraft saves
money and again improves purification of mill waste water and stack
gases, benefiting the ecology. On the other hand, the quality of
the slurry measured by its reject content decreases markedly and
disproportionately with increased yield, particularly at or
approaching high yields.
The rejects portion of the digested slurry is suitable with
ordinary refining for use as the base stock layer of the kraft
paper laminate, but is not suitable for the top stock layer. In
consequence it has been a prevalent practice to digest separately
the wood needed for the top stock layer and that required for the
base stock layer. The wood for the top stock is digested to low or
medium yield and is suitable for use in the top layer using low
horsepower prerefining for knot breaking, ordinary screening and
washing, and low horsepower refining for freeness control. The base
layer stock is digested to high yield and, similarly treated but
with additional refining in a regular higher horsepower base stock
refiner, is used as the base stock. The main disadvantage of this
practice is its high capital cost, requiring two sets of digesters,
blow tanks, prerefiners, screens and washers, as well as the
regular refiner for the base stock. In addition, the savings and
other advantages from high yield digestion are only partially
realized.
More recently a process has come into use in which all the wood for
both layers is digested together to high yield. In this process the
total slurry is subjected to special refining in what may be called
an "ultrarefiner" which applies sufficient attrition forces to
reduce the shive count to a maximum acceptable for top stock, the
refined product being separately fed to form both the top stock
layer and the base stock layer on the linerboard machine. This
process has the advantages of high yield digestion but
ultrarefiners are expensive equipment costly to operate, and the
product is a compromise, in that the top stock layer is not as good
as is desirable and the base stock layer is better than is
necessary.
In another compromise process known to applicant, the mill is batch
digesting all the wood for both layers in a single digestion system
to a medium yield of about 52 percent. The digested slurry is
subjected to screening (0.070 inch diameter holes) to provide a 50
percent accept fraction which is washed and about 40 percent of it
used directly to form the top stock layer. The 50 percent reject
fraction is subjected to refining in ordinary base stock refiners,
washed and, with the about 60 percent remainder of the accept
fraction added to it, is used to form the base stock layer. This
process is less costly to install and operate than the process
involving ultrarefiners since it uses less costly, ordinary
refiners on only half the stock. However, the process has the
drawbacks of only partially realizing the advantages of high yield
versus low yield digestion, and the product is a compromise in that
the screening accepts portion contains some fibers undesirable for
the top stock layer.
SUMMARY OF THE INVENTION
An object of this invention is to provide a process of making a
kraft paper laminate of top and base stock layers from a single
slurry which has been digested to a high yield, which process does
not involve the high capital and operation cost of the process
utilizing ultrarefiners and yet obtains fully the advantages of
high yield digestion.
Another object is to provide such a process wherein the fiber of
the top stock layer is essentially only fiber having the desired
characteristics, and provides a top stock layer of a quality at
least as good as that produced by the separate digestion systems
process and better than is obtained in the other two processes
mentioned above.
It was conceived that if there were a way of cleanly segregating
from high yield kraft slurry enough of the "good" (non-reject)
fiber portion to form the top stock layer, such segregated portion
could be used with little or no refining of it as the furnish for
that layer, and this would enable the remainder of the fiber
content of the slurry to be used with only ordinary refining to
form the base layer. At first it was believed that fine screening
to effect such a segregation would not be possible because the high
reject concentration at high consistency (4 percent or more) would
blind the screen. However, it has been discovered that the desired
result can be obtained by very fine screening (holes about 0.06
inch diameter or less or slots about 0.02 inch wide or less),
provided the slurry as it passes over the screen is subjected to
pulses of very high frequency and intensity. The bumped rotor of
the screening machine disclosed in U.S. Pat. No. 3,363,759,
operated at high speed, has been found capable of supplying the
requisite pulsation.
In the preferred process according to the invention, the wood is
digested only sufficiently to provide a high yield kraft fiber
slurry of at least 54 percent yield, and preferably higher
particularly where the digesters are continuous. The slurry, either
as "hot stock" (prewashing) or "brown stock" (postwashing) is
subjected to screening in a screening machine between a cylindrical
screen and a coaxially mounted cylindrical rotor, preferably the
screen having apertures in the diameter range 0.030 inch to 0.055
inch and an open area in the range about 15 to 30 percent of the
total screening area of the screen, or slots having a width between
about 0.01 and about 0.02 spaced between 5 and 12 per inch, the
rotor being in accordance with U.S. Pat. No. 3,363,759, rotated at
high speed (e.g. about 5,000 to 7,500 feet per minute), the machine
being operated to reject about 80 percent of the slurry content. In
this preferred process the about 20 percent fraction passing the
screen as accepts, which consists almost entirely of the "good" top
stock quality fiber, is used either without refining or with a
small amount of refining for freeness control to form the top-stock
layer of the laminate made on the linerboard machine, being first
washed if the slurry was screened as hot stock. The about 80
percent portion rejected by the screen is used to form the base
layer of the laminate, being first subjected to regular base stock
refining and, if the slurry was screened as hot stock, being also
washed.
The refining cost is reduced if the reject portion only is refined
after screening. On the other hand, since this procedure requires
separate washers for the accept and reject portions from the
screen, it may be more desirable to refine the slurry in a pulp
refiner so that it can be washed in entirety in one system of
washers before it is screened.
The preferred process just described has been found to produce an
accept fraction, having less than 1 percent of the reject content
of the slurry and provides a better quality top stock layer of the
laminate than the process using an ultrarefiner as described above,
having better brightness and strength with less of the undesirable
shives. The top stock layer so produced is similarly better than
that obtained with the 50--50 screening process and at least as
good as the product of the process separately digesting the stock
for each layer, while the base stock layer is as good as is
required. The superior quality of the top stock layer is due in
part to the fact that the screen accepts fraction of the high yield
kraft is of better quality than stock produced from medium or low
yield kraft. The equipment cost and its operating cost in the
process of this invention are substantially less than in the
process utilizing ultrarefining, which is the only prior process
known to applicant in which all the stock for both layers is
digested to high yield, with all the advantages this entails.
The screening machine used in the preferred process as described is
capable not only of effecting the desired clean separation of the
"good" top stock fiber but also of separating most of it even where
its amount is low such as 30 percent or less, a surprising result
when it is considered that it is mixed with such a large amount of
reject material. Apparently, the high frequency and intensity of
the pulsation produced by the rotor keeps the slurry content in a
constant state of agitation such that virtually all of the fiber in
the slurry has access to the open area of the screen.
The about 20-80 percent separation at the screen is preferred for
several reasons. One is that these are about the right proportions
to provide top and base layers of requisite thickness. A more
important reason is that the machine operates very effectively in
separating in these proportions. Separation at a higher ratio of
accepts to rejects is likely to produce accepts with more
undesirable fiber content and provides more fiber than is needed
for the top stock, with about 30 percent the upper limit for
providing accepts of requisite quality. Separation at a lower ratio
is possible but if less than about 10 percent probably will not
provide sufficient fiber for the top stock layer and will
necessitate another screening of the rejected portion to make up
the deficiency.
Smaller apertures or narrower slots in the screen than the minimums
of the preferred ranges are likely to reject too much of the
desired fiber or to blind; whereas, larger holes or wider slots
than the maximums of the preferred ranges are likely to yield
accepts of lower quality, with about 0.06 diameter holes and 0.02
wide slots being the maximums for providing an accepts fraction of
requisite quality.
BRIEF DESCRIPTION OF THE DRAWINGS
In the drawings:
FIGS. 1A and 1B are typical curves showing increase in percent
rejects with increased yield for respectively continuous digestion
and batch digestion of wood to kraft fiber.
FIG. 2 is a flow sheet illustrating a practice of the process of
the invention; and
FIG. 3 is a modification of the flow sheet of FIG. 2.
DESCRIPTION OF THE PREFERRED EMBODIMENTS
In FIG. 1 the two curves show the percent of rejects in continuous
and batch digested kraft respectively on the vertical scale at the
left for yields from low to high on the horizontal scale at the
bottom. It will be noted that for yields of 50 percent or lower
both curves show reject percentages below 20 percent. Above 50
percent yield the batch digestion curve climbs steeply, increasing
from less than 40 percent rejects at a yield of 53 percent to more
than 60 percent rejects at a yield of 56 percent. At a yield of 55
percent the continuous digestion curve shows a reject content of
only 30 percent but an increase of continuous digestion yield from
55 to 60 percent increases the reject content to about 70
percent.
It will be seen therefore that at the same high yields batch
digested slurry contains more rejects than does the continuous
digested slurry and higher yields are obtainable with continuous
digestion which will provide sufficient "good" fiber to form the
top stock layer.
FIG. 2 illustrates a practice of the process of the invention with
hot stock screening of the slurry to separate the top stock. From
digester 10 (continuous or batch) where it is digested to a high
yield, the kraft fiber goes to blow tank 12. At the exit of tank
12, dilution liquid is added through line 13 to form a slurry of
about 4 percent consistency which passes through prerefiner 14 from
which it is pumped by pump 16 to screening machine 18. Screening
machine 18 is constructed and operated as above described to
separate an accepted fraction, preferably of about 20 percent of
the slurry content, which contains substantially only fibers of the
"good" (non-reject) portion of the slurry fed thereto. This
accepted fraction goes to washer 20 from which it is fed to be
ultimately formed into the top stock layer on the linerboard
machine. The slurry portion rejected by the screen of machine 18
goes to regular base stock refiner 22, thence to coarse screen 24
(e.g. 0.078 to 0.094 holes) from which the reject fraction is
returned to the inlet of refiner 22, while the accepted fraction
goes from screen 24 via washer 26 to be ultimately formed into the
base stock layer of the paper laminate.
It will be understood that machines indicated singly in the
drawings may be in multiple. If screening machines 18 are used in
multiple, they are arranged in parallel, except as noted below.
Refiner 22 may be capable of operation as an ultrarefiner but if
so, will usually be operated at lower horsepower than is required
for ultrarefining.
The flow sheet of FIG. 3 differs from that of FIG. 2 in that
screening machine 18 operates on brown stock, there being
interposed between prerefiner 14 and machine 18 pulp refiner 30 and
washer 32, the latter making unnecessary washers 20 and 26 of FIG.
2.
In the process as illustrated in the flow sheet of either FIGS. 2
or 3, if screening machine 18 is operated to accept more fiber than
is needed for the top stock layer, the excess thereof may be added
to the rejected portion of slurry, preferably after it has been
refined. In either flow sheet, if the screening machine 18 does not
accept a sufficient quantity of fibers to form the top stock layer,
the deficiency may be made up, for example, by providing a second
screening machine 18 of like construction and operation to the
first one and feeding thereto some or all of the stock accepted by
screen 24, to provide an accept fraction containing acceptable
fiber lost in the portion rejected by the first machine 18, and
additional such fiber produced in the refining. The fraction
accepted by the screen of this second machine may then be added to
the fraction accepted by the screen of the first machine to form
the top stock layer, while the slurry portion rejected by the
screen of the second machine is used to form the base layer.
* * * * *