U.S. patent number 3,777,447 [Application Number 05/267,905] was granted by the patent office on 1973-12-11 for method for packaging viscous vinyl plastic solutions.
This patent grant is currently assigned to Schering Corporation. Invention is credited to Richard H. Herbine, David J. Morrison.
United States Patent |
3,777,447 |
Herbine , et al. |
December 11, 1973 |
METHOD FOR PACKAGING VISCOUS VINYL PLASTIC SOLUTIONS
Abstract
A simplified technique well suited for automated, high speed
filling of packages with viscous vinyl plastic solutions, such as
denture adhesives, which exhibit a (1) viscous taffy-like, sticky
consistency and (2) a high degree of uniformity when utilized by
the consumer. The first step of the technique requires he
introduction of beads of the vinyl polymer into the open end of the
package while simultaneously completely wetting each bead with a
suitable solvent; a later step requires the aging of the wetted
beads within the sealed package until the beads are fully dissolved
and form a uniform product. In the preferred embodiment, the
solvent is introduced into the open end of the package by a
conduit. In the alternative embodiment, the solvent is injected
into the package by an elongated needle with radial apertures, such
needle being axially inserted into the interior of the package and
being axially removed when the wetting step has been completed.
Inventors: |
Herbine; Richard H.
(Ziegerville, PA), Morrison; David J. (Plainfield, NJ) |
Assignee: |
Schering Corporation
(Bloomfield, NJ)
|
Family
ID: |
23020633 |
Appl.
No.: |
05/267,905 |
Filed: |
June 30, 1972 |
Current U.S.
Class: |
53/467; 53/239;
53/474; 53/431 |
Current CPC
Class: |
C08L
31/04 (20130101); C08L 31/04 (20130101); A61K
6/30 (20200101); A61K 6/30 (20200101); A61K
6/66 (20200101) |
Current International
Class: |
A61K
6/00 (20060101); B65b 003/08 () |
Field of
Search: |
;53/36,35,37,3,239,247,248 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Schran; Donald R.
Claims
What we claim is:
1. A method for packaging a viscous vinyl plastic solution
comprising the steps of:
a. introducing a small quantity of a solvent for the vinyl polymer
into the open package;
b. introducing beads of said vinyl polymer and an additional larger
quantity of said solvent into said open package so that each beads
is thoroughly wetted;
c. sealing said open package; and
d. storing said sealed package for a time at least sufficient for
the vinyl plastic therein to form a homogeneous solution.
2. The method of claim 1 wherein said vinyl plastic is polyvinyl
acetate.
3. The method of claim 1 further including the step of introducing
a small quantity of solvent into the package after the last bead
has been deposited therein.
4. The method of claim 1 further including the steps of subjecting
the beads to a centrifugal force to separate the beads from one
another prior to introducing the beads into the package.
5. The method of claim 1 wherein the solvent is pressurized before
being introduced into the package through an axially extending
conduit.
6. The method of claim 1 wherein the solvent is pressurized before
being introduced into the package through an axially extending
elongated needle having radial apertures for discharging the
solvent.
7. The method of claim 6 wherein the needle is axially lowered into
the package prior to introducing the solvent into the package, and
the needle is axially withdrawn from the package subsequent to
discharging the solvent, the axial movement of the needle assisting
in the wetting of the beads in the package.
8. The method of claim 1 wherein said sealed package is stored for
a time frame of at least one week.
Description
BACKGROUND OF THE INVENTION
1. Field of the Invention
The instant invention relates generally to methods for thoroughly
wetting beads of a vinyl polymer with a suitable solvent so that
the resultant viscous vinyl plastic solution can be aged within the
confines of a consumer package.
2. Description of the Prior Art
Products, such as denture adhesives, which possess the above noted
taffy-like consistency and high degree of uniformity are currently
manufactured and packaged by cumbersome and inefficient manners
unsuited for mass production, automated facilities. For example, in
one method, the ingredients of the product are blended together by
a heavy-duty mechanical mixer. Then, the batch of blended material
is pressurized and/or advanced from the mixer into a filling head.
The packages to be filled are passed beneath the filling head, and
the product is introduced into each package in sequential fashion.
A semi-skilled laborer controls the operation of the head and
attempts to regulate the amount of blended viscous material
introduced into each package. The laborer then manually severs the
taffy-like material with a knife or shears, and the filled package
is subsequently sealed, as by a crimping operation. Problems are
frequently encountered with "tailing" of the viscous product; such
"tailing" makes the subsequent sealing operation much more
difficult and the "tail" detracts from the aesthetic appeal of the
consumer product, with lowered commercial acceptance. Furthermore,
such conventional filling technique is time-consuming, tedious, and
far better suited for small, low-volume packaging runs than for
continuous, high speed packaging lines.
SUMMARY
Thus, with the above noted deficiencies of the prior art packaging
techniques for viscous solutions of vinyl plastics clearly in mind,
the instant invention contemplates processes for accurately filling
packages with beads of vinyl polymeric material and a suitable
solvent to form a viscous, taffy-like product of high uniformity
after aging within the sealed package. The solvent is introduced
into the package by a conduit or an elongated needle with radial
apertures. The package is sealed after being filled and the
problems associated with the mechanical blending of the ingredients
and the manual severing of the blended mass, such as the tailing,
are obviated.
Furthermore, the viscous vinyl plastic solution produced by the
instant invention is a highly uniform product. Uniformity indicates
that imperfections or "fish-eyes," or undissolved beads similar in
size to granules of sand, are absent from the product when utilized
by the consumer. "Fish-eyes" reduce the effectiveness of the
various properties of the product containing same; for example,
with reference to denture adhesives, the gripping power of the
adhesive might be reduced.
Thus, it will be appreciated that the instant packaging method can
readily be practiced with commercially available apparatus to
economically perform high-speed, automated packaging of viscous
vinyl plastic solutions under sanitary conditions while maintaining
a high degree of uniformity in the consumer product.
Other objects, advantages and desirable features of the instant
invention will become apparent in light of the following
description of the invention when construed in connection with the
accompanying sheet of drawings.
DESCRIPTION OF THE DRAWINGS
FIG. 1 is a schematic representation of a system for practicing the
unique method of the instant invention;
FIG. 2 is a vertical cross-section, on an enlarged scale, of a
preferred embodiment of selected segments of a hopper, auger, jig,
and conduit employed within the system of FIG. 1;
FIG. 3 is a vertical cross-sectional view of an alternative
embodiment wherein an elongated needle is substituted for the
conduit of FIG. 2; and
FIG. 4 is a horizontal cross-sectional view on an enlarged scale,
of the jig and the package with the needle inserted therein, such
view being taken along line 4-4 in FIG. 3 and in the direction
indicated.
DESCRIPTION OF THE INVENTION
Referring now in greater detail to the drawings in which similar
reference numerals identify similar components, FIG. 1 depicts a
representative system of commercially available components for
practicing the unique method of the intant invention, and FIG. 2
illustrates, in greater detail, the more significant components of
the system. More particularly, the system includes a hopper
indicated generally by reference numeral 10. Hopper 10 comprises an
upper funnel 12 whose narrow bottom end opens into the first
cylindrical section 14. Section 14, in turn, opens into the second
larger cylindrical section 16, which terminates in a tapering
section 18 that leads into a third, smaller cylindrical section 20.
An annular ring 22 is defined at the lower end of the hopper.
A jig 24 holds the package, such as a collapsible tube, to be
filled. A cam 26 and a follower 28 are provided for raising the jig
at the initiation of the filling operation, and for lowering same
when the operation has been completed. A pump 30 pressurizes the
liquid to be delivered over conduit 32 to the package retained
within jig 24. The conduit terminates in a downwardly facing,
axially extending nozzle that communicates with the package to be
filled. Additionally, feed means, indicated generally by reference
numeral 34, are provided to assist the movement of solid materials
through hopper 10.
An electrical controller 36 with manually adjustable knobs 38, 40
and appropriate leads 41, 43 and 45 regulates (1) the operation of
motor 42 that drives feed means 34, as well as (2) the operation of
motor 44 that drives pump 30 and (3) the operation of motor 46 that
drives cam 26 to raise and lower jig 24. By properly manipulating
knobs 38 and 40, the timed operation of feed means 34 and pump 30
relative to one another is altered. The flow of pressurized fluid
through conduit 32 can be regulated by valve 48. By-pass loop 50
may relieve pressure built-ups in the conduit.
Examining FIG. 2 in somewhat greater detail, the structural details
of hopper 10, feed means 34, conduit 32 and jig 24 are clearly
visible. Feed means 34 extends axially through sections 12, 14 and
16 and terminates near the upper end of section 16. Feed means 34
comprises a vertically extending shaft 52 with a helical spiral 54
wound thereabout; an annular plate 56 is secured to the lower end
of the fillers, Auger-type filler, such as those described above,
are well known and may be purchased from the G. Diehl Mateer
Company of Wayne, Pa., or may be seen in U.S. Pat. Nos. re 23,888
and re 24,079 granted to G. Diehl Mateer.
Conduit 32 passes through an aperture 58 in the wall of third
cylindrical section 20, and terminates in a right-angled section
that is coincident with the vertical axes of hopper 10 and jig 24.
The jig, sections of which are broken away, has a cavity 60 shaped
to receive therein the outline of the package to be filled. In the
illustrative preferred embodiment of FIG. 2, cavity 60 receives a
collapsible metal tube with a cap already screwed onto its threaded
neck. Shoulder 22 on the lower end of hopper 10 assists in locating
jig 24 relative thereto as cam 26 and follower 28 elevate the
unfilled tube.
The method of this invention is particularly useful in the
packaging of viscous solutions of vinyl plastics. Typical of the
polyvinyl resin bases of such plastics are polyvinyl acetate,
polyvinyl alcohol, polystyrene and polyvinyl chloride. A further
description of such vinyl polymers can be found, for example, in
Kirk-Othner, Encyclopedia of Chemical Technology, 2nd Edition
(1970), Vol. 21, pp. 304-440. By way of further illustration, a
representative formulation which can be successfully packaged by
the method of this invention is a known denture adhesive prepared
by admixing in the manner of this invention 50-85 parts of
polyvinyl acetate beads having an average viscosity in the range of
15-25 cps. together with 15-70 parts of a suitable solvent therefor
such as ethyl alcohol, additionally incorporating the usual amounts
of plasticizer and coloring agents.
A predetermined quantity of beaded polymeric material is fed into
hopper 10 and then controller 36 is energized to start the
operation of motor 46 and thus elevate jig 24 against retaining
shoulder 22. Controller 36 also energizes motor 42 which drives
feed means 34 so that the helix 54 advances the beads onto plate
56. Plate 56 rotates rapidly and propels the beads radially
outwardly against the walls of chamber 12 by virtue of the
centrifugal force. The beads then follow the configuration of the
hopper walls and fall downwardly into the collapsible tube retained
within the cavity 60 in jig 24. The path of travel of the beads
through the hopper is indicated by appropriate directional arrows
in FIG. 2.
A second or two before the beads following the contour of hopper 10
fall down into the tube held within cavity 60 in jig 24; motor 44
is turned on to drive pump 30 and thus pressurize a predetermined
quantity of the solvent, plasticizer and coloring agent for
discharge from conduit 32. The initial quantity of liquid dispensed
wets the bottom of the inverted tube in the vicinity of the cap to
thereby prevent undissolved beads from gathering at such spot and
clogging the narrow neck of the tube. Thereafter, the liquid and
the beaded material are simultaneously introduced into the tube
retained in jig 24 so that each bead is saturated with the solvent
until the predetermined quantity of beads has been collected in the
tube. Lastly, conduit 32 continues to supply liquid for a fraction
of a second after the last bead has been discharged. It will be
noted that the discharge end of conduit 32 is located on the
vertical axis of hopper 10 and jig 24 so that the beads will be
saturated in a uniform fashion. After saturation, jig 24 is lowered
by motor 46 and cam 26, and the filled tube is removed therefrom
and then sealed by crimping or rolling over the open end of the
tube. Lastly, the tube is then retained in a storage facility where
it will be allowed to age. The aging process, which takes place in
a commercially acceptable time frame aids in the formation of a
uniform product of high quality.
The aging process occurs in the sealed tube over a period of at
least one week. In many instances, however, an aging period of four
to six weeks is commonplace. The range of one to six weeks defines
a commercially acceptable time frame.
FIGS. 3 and 4 depict an alternative embodiment of the means for
saturating the beads of polymeric material with solvent to form a
viscous vinyl plastic solution. An elongated needle 62 with a
series of radial apertures 64, 66, 68 and 70 is utilized in lieu of
conduit 32. Needle 62 is inserted axially into the tube retained
within jig 24, and the pre-determined quantity of liquid containing
the solvent, plasticizer, and color is then discharged, under
pressure, through apertures 62, 64, 66 and 68. The needle can be
slowly withdrawn as the tube is gradually filled with the polymeric
beads, and many levels or rows of axially spaced apertures may be
utilized.
The force of the liquid discharged through the aperture, the
constantly changing position of needle 62 as it is moved upwardly,
plus the capillary action and gravimetric force of the solvent upon
the beads, assures wetting of all the beads. Over a period of time,
such as 1-6 weeks, all of the beads dissolve completely in the
solvent in the sealed package, thus forming 2 uniform viscous mass
of high quality identical to the finished product previously
manufactured by conventional blending techniques. Additionally,
since the product is formed within the package, by combining of
ingredients, the problems of accurately weighing or measuring a
quantity of viscous material, and then manually severing same
without producing an unsightly "tail" of taffy-like material are
obviated.
Manifestly, numerous modifications of the above described apparatus
and method will occur to the skilled artisan without departing from
the spirit or essential characteristics of the unique, two-phase
method described in the specification. Consequently, the appended
claims should be accorded a wide range of equivalency.
* * * * *