U.S. patent number 3,749,370 [Application Number 05/153,649] was granted by the patent office on 1973-07-31 for mixing device for powdered materials.
This patent grant is currently assigned to Commissariat A L'Energie Atomique. Invention is credited to Albert Clech, Georges Marchand, Jean-Yves Pasquiou, Jacques Regnier.
United States Patent |
3,749,370 |
Clech , et al. |
July 31, 1973 |
MIXING DEVICE FOR POWDERED MATERIALS
Abstract
The mixing device for powdered material and especially fissile
material which remains geometrically subcritical even when a large
quantity is present comprises a stationary cylindrical tank having
a horizontal axis and obturatable openings for the introduction and
withdrawal of materials ; a rotary drum which is coaxial with the
tank and forms the internal wall of a substantially leak-tight
annular space whose external wall is constituted by the tank; a
core of neutron-moderating material located within the drum and
covered with material having a high neutron capture cross-section ;
stirring arms mounted on the external wall of the drum and means
for driving the drum in rotation.
Inventors: |
Clech; Albert (Hainneville,
FR), Marchand; Georges (Clamart, FR),
Pasquiou; Jean-Yves (Equerdreville, FR), Regnier;
Jacques (Cherbourg, FR) |
Assignee: |
Commissariat A L'Energie
Atomique (Paris, FR)
|
Family
ID: |
22548117 |
Appl.
No.: |
05/153,649 |
Filed: |
June 16, 1971 |
Current U.S.
Class: |
366/143;
366/180.1 |
Current CPC
Class: |
B01F
7/00533 (20130101); B01F 7/04 (20130101); B01F
7/007 (20130101); B01F 2215/0095 (20130101) |
Current International
Class: |
B01F
7/02 (20060101); B01F 7/04 (20060101); B01F
7/00 (20060101); B01f 007/04 (); B01f 015/00 () |
Field of
Search: |
;259/2,9,10,DIG.16,109,110,81R,89,25,26,45,46 ;264/.5
;252/31.1R |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Jenkins; Robert W.
Assistant Examiner: Coe; Philip R.
Claims
1. A mixing device for powdered materials comprising: a stationary
tank of revolution having a horizontal axis and provided with
obturatable openings for the introduction and withdrawal of
materials; a drum which is coaxial with the tank and forms the
internal wall of a substantially leak-tight annular space whose
external wall is constituted by said tank, said drum being adapted
to carry stirring arms; and means for driving the drum in rotation
about a horizontal axis and a core of neutron-moderating material
covered with material having a high neutron capture cross-section
in the drum.
2. A device according to claim 1, wherein the neutron-moderating
material is constituted by a polyethylene cylinder covered with a
sheet of cadmium.
3. A device according to claim 1, wherein the drum is occupied at
least partially by a core of homogeneous neutron-moderating and
neutron-absorbing material.
4. A device according to claim 1, wherein the drum is fixed on a
driving shaft carried by a frame and has an axial length which is
greater than that of the tank, sliding sealing means being
interposed between the tank and the drum.
5. A device according to claim 1, wherein provision is made at the
top of the tank for an inspection opening whose axial length
represents a substantial fraction of the total length of the tank,
said opening being intended to be closed by means of a leak-tight
door.
6. A device according to claim 1, wherein the discharge opening for
powdered materials which is placed at the bottom portion of the
tank terminates in a transfer duct and can be sealed-off by a gate
which is displaceable within said duct in a direction parallel to
the axis.
Description
This invention relates to a mixing device for powdered materials
and especially for fissile materials.
Fissile materials which are provided in the form of a powdered mass
(this term being understood to designate flakes and granules as
well as powders proper) are often required to undergo a mixing or
stirring process in order to make the mass homogeneous.
The problem of criticality arises immediately in operations of this
type. It is known that the critical mass of a given fissile
material (e.g., plutonium oxide, oxides of uranium-235 or
uranium-233, uranium carbide or plutonium carbide) is a function of
two parameters, namely density and moisture content. The importance
of the range of variation is immediately apparent if it is borne in
mind that, in the case of plutonium oxide, for example, the
critical mass varies between approximately 100 kilograms and a few
kilograms. In fact, during a stirring operation, the density of a
powdered material can increase to a very appreciable extent under
the action of its own weight. Moreover, the moisture content which
is usually of very low value can increase to a considerable extent
as a result of an incident. In consequence, the mixers which are
employed in conventional industrial applications are not suited to
this purpose unless the capacities are limited to extremely low
values which are in any case objectionable. In all these mixers,
the powdered material to be treated is in fact collected together,
with the result that a criticality accident is always possible if
reliance is placed on maintenance of low values of density and/or
moisture content in order to prevent the attainment of
criticality.
The aim of the present invention is to remove these difficulties
and more specifically to provide a mixing device for powdered
material which remains geometrically subcritical even in the case
of large capacities.
To this end, the invention proposes a device which comprises : a
stationary tank of revolution having a horizontal axis and provided
with obturatable openings for the introduction and withdrawal of
materials; a drum which is coaxial with the tank and forms the
internal wall of a substantially leak-tight annular space whose
external wall is constituted by the tank, said drum being adapted
to carry stirring arms ; and means for driving the drum in rotation
about its axis.
It is apparent that the fissile material occupies a volume which
has the shape of a circular ring : both the thickness and diameter
of this ring can be chosen so as to ensure absolute safety in the
case of all materials to be processed, such materials being usually
limited to plutonium and uranium compounds. It is further apparent
that a given device can be adapted to the treatment of a material
having a critical mass of lower value than the material for which
it was designed at the cost of simple modifications (reduction in
thickness of the ring).
In a preferred embodiment of the device, the drum is occupied at
least partially by a core of neutron-moderating material which is
covered with material having a high neutron capture cross-section
(such as cadmium, for example). The drum which is preferably
cylindrical as well as the tank can be fixed on a driving shaft
which is rotatably mounted in bearings and carried by a frame, the
axial length of said drum being greater than that of the tank and
sliding sealing means being interposed between the tank and the
drum.
A better understanding of the invention will be obtained from the
following description of a device which constitutes one particular
embodiment as given by way of example without any limitation being
implied. In this description, reference is made to the single
accompanying FIGURE which is a sectional view along the vertical
midplane of the device.
As illustrated in the FIGURE, the device essentially comprises a
tank 10 and a rotary drum 12.
The tank consists of a circular shell which is constructed of
stainless steel sheet, for example, and supported for rotation by a
frame which is not shown in the drawing. Said tank is provided at
the top with a large inspection opening having a length which
represents a substantial fraction of the axial length of the tank.
Said opening is normally closed by a door 14 which is secured in
leak-tight manner around the periphery of the opening by means of
detachable components such as screws (not shown). On each side of
the inspection opening and in the axial direction, the tank is
provided with two nozzles 16 for the admission of powdered material
to be homogenized. Said nozzles terminate in flanges 18 for the
connection of supply tubes.
Similarly, the bottom portion of the tank 14 is provided with a
nozzle 20 for the discharge of homogenized material, said nozzle
being provided with a coupling flange 22. The nozzle 20
communicates with the interior of the tank by means of an opening
which is sealed-off by means of a gate 24 when stirring is in
progress. Said gate can be withdrawn laterally so as to free the
opening as a result of displacement in a direction parallel to the
axis by means of a control jack 26 which is placed outside the
tank. In order to permit said displacement of the gate 24, the
nozzle 20 is provided with a lateral extension 28. The tank is
further provided with a vent 29 for connecting the interior of the
tank to atmospheric pressure.
The drum 12 which is rotatably mounted within the tank 10 is made
up of a rotary cylinder 30 of sheet steel, for example, which is
attached to two end-plates 32. Said two end-plates are keyed on a
driving shaft 34 which is rotatably mounted in bearings 36 of a
stationary supporting frame. A reduction-gear motor (not shown)
serves to drive the shaft at a suitable speed. The drum has an
axial length which is greater than that of the tank. In order to
prevent leakage in the connection zones of large diameter, the tank
is adapted to carry stuffing-boxes 38 which maintain leak-tight
packings applied against the end portions of the drum 12. The drum
is provided with helical stirring arms 40 which serve both to bring
the powdered material towards the center after this latter has been
poured through the nozzles 16 and to assist the mixing process.
The interior of the drum 12 is occupied by a core which is intended
to absorb the neutrons. Said core 42 is constituted by a mass of
light material which is intended to slow-down the neutrons and by a
sheet of material having a high neutron capture cross-section which
covers said mass. It is possible in particular to employ a cadmium
sheet having a thickness varying between a few tenths of a
millimeter and one millimeter on a mass of polethylene : the fast
neutrons emitted by the fissile material are slowed-down by the
mass of light material and are thus much more strongly absorbed by
the sheet of cadmium.
Instead of a neutron-moderating core covered with cadmium, it is
possible to employ a mixture of moderator and absorbent material
such as boron-containing polyethylene associated with plaster.
The following data relating to a homogenization device which has
actually been constructed for the treatment of plutonium oxide can
be mentioned by way of example : the cylindrical tank had an
internal diameter of 620 mm and an internal length of 800 mm. The
drum had an external diameter of 500 mm so that the annular space
for receiving plutonium dioxide had a thickness of 60 mm. The
interior of the core around the shaft was occupied by polyethylene
and this latter was surrounded by a sheet of cadmium over a
distance of 820 mm (the core accordingly extended over a distance
of 10 mm beyond the annular mixing space at each end of this
latter).
The operation of the device can readily be understood from the
foregoing description : the fissile material (plutonium dioxide,
for example) is introduced through one of the nozzles 16 and the
mass employed can correspond to 50 kg of plutonium metal if the
dimensions are those given above.
It is apparent that the device offers an advantage only on
condition that the level of fissile material at rest is located
above bottom portion of the drum : in practice, the useful capacity
is approximately one-half of the annular volume.
The drum is driven in rotation at a speed of the order of 20
revolutions per minute. At the end of a time interval which is
variable according to the state of the material which is introduced
and which in practice is always less than one hour, the discharge
gate 24 is opened by means of the jack 26 and the fissile material
is poured off while the drum is maintained in rotation so that the
arms 40 bring the product back towards the central plane of the
device and the gate.
* * * * *