U.S. patent number 3,746,976 [Application Number 05/131,923] was granted by the patent office on 1973-07-17 for self-cleaning aperture tube for coulter study apparatus.
This patent grant is currently assigned to Coulter Electronics Inc.. Invention is credited to Walter R. Hogg.
United States Patent |
3,746,976 |
Hogg |
July 17, 1973 |
SELF-CLEANING APERTURE TUBE FOR COULTER STUDY APPARATUS
Abstract
A two chamber aperture tube for obtaining signals from particles
suspended in a fluid which passes through a scanning aperture. The
suspension enters the primary bore provided in one chamber and
passes immediately to an inlet port or orifice in an elongate
nozzle provided in the second chamber. The chambers are
interconnected by conduits including a pump and filter such that
flow of the suspension is continuous about a closed path to ensure
that proper signals from all particles in the suspension are
obtained.
Inventors: |
Hogg; Walter R. (Miami Lakes,
FL) |
Assignee: |
Coulter Electronics Inc.
(Miami, FL)
|
Family
ID: |
22451620 |
Appl.
No.: |
05/131,923 |
Filed: |
April 7, 1971 |
Current U.S.
Class: |
324/71.1 |
Current CPC
Class: |
G01N
15/12 (20130101); G01N 15/1218 (20130101) |
Current International
Class: |
G01N
15/10 (20060101); G01N 15/12 (20060101); G01n
027/00 () |
Field of
Search: |
;324/71R,71CP
;73/432PS |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Rolinec; Rudolph V.
Claims
I claim:
1. In a particle measuring apparatus including a container of
particulate liquid suspension to be tested, an aperture tube
extending into said container, a vacuum source for moving the
liquid from the container into and through the aperture tube, a
first electrode in the container and a second electrode in the
aperture tube to establish an electrical field between said
container and the aperture tube, and a detector, the aperture tube
having a first and a second chamber, the first chamber having an
aperture in communication with the liquid suspension in the
container, said second chamber having an orifice provided therein
at a point closely spaced from and directly opposite the interior
of said aperture, means connecting said second chamber to said
vacuum source and means to initially fill the first chamber with
particle free liquid and the second chamber with the liquid
suspension, the improvement comprising, a conduit extending between
said chambers to provide a closed path for liquid flow
therebetween, a pump interposed in said conduit to create liquid
flow about said path, and a filter member in said conduit, whereby
the suspension will flow from the container through the aperture
and the orifice into said second chamber to mix with the liquid
already therein and circulate about said path, said filter member
removing the particles from the liquid before the same is returned
to the first chamber.
2. The structure as claimed in claim 1 in which an elongate neck
extends from the second chamber into the first chamber and said
orifice is provided in said neck.
3. An aperture tube for use in particle measuring apparatus
including a container of particulate liquid suspension into which
the aperture tube extends, said tube including a first and a second
chamber, the first chamber having an aperture in communication with
the liquid suspension, said second chamber having an orifice
provided therein at a location directly opposite the interior of
said aperture, means for connecting said second chamber to an
external source of vacuum, conduit means extending between said
chambers to provide a closed path for liquid flow therebetween, a
pump interposed in said conduit means to create liquid flow about
said path, and a filter member in said conduit means, whereby the
suspension will flow through said aperture in the first chamber and
through said orifice in the second chamber and then through said
conduit and said pump and said filter member where the particles
from the suspension are removed before the same is forced into the
first chamber and returned through said orifice.
4. An aperture tube as claimed in claim 3 in which an elongate neck
extends from said second chamber into said first chamber and said
orifice is provided in said neck.
5. In a particle measuring apparatus which responds to the changes
of electrical impedance due to the displacement of electrolyte by
particles suspended therein in an aperture which constricts an
electric field, including a container of liquid suspension to be
tested, a dual-chamber aperture tube having a first and a second
chamber extending into said container, a vacuum source for moving
the liquid from the container into and through the aperture tube, a
first electrode in the container and a second electrode in the
aperture tube to establish the electric field, and a detector, the
first chamber having an aperture forming a communication between
said container and said first chamber, the second chamber having an
orifice forming a communication between said first and said second
chambers, said orifice being positioned close to and directly
opposite said aperture, the improvement comprising, means for
preventing particles from the contents of the container from being
transferred to suspension in the contents of the first chamber.
6. The structure as claimed in claim 5 in which said means comprise
a conduit extending between said chambers to provide a closed path
for liquid flow therebetween, a pump interposed in said conduit to
create liquid circulation about said path, and a filter for
removing particles from the circulating liquid, such that the
volume of liquid which flows into said orifice is the sum of the
circulation about said closed path plus the flow from said
container into said first chamber.
7. The structure as claimed in claim 6 in which said vacuum source
is adapted to withdraw liquid from the low pressure side of said
pump.
8. The structure as claimed in claim 7 in which an elongate neck
extends from the second chamber into the first chamber and said
orifice is provided in said neck.
9. The structure as claimed in claim 7 in which filling means are
provided to fill the aperture tube, said conduit and said pump with
liquid prior to performing the first test of particle suspension
contained in said container.
10. The structure as claimed in claim 9 in which said filling means
comprise a two-way stopcock and an open-close stopcock, said
two-way stopcock being adapted to apply vacuum either to said first
or said second chamber or to neither, said open-close stopcock
being adapted to connect one chamber to a reservoir of suspension
liquid.
11. The structure as claimed in claim 10 in which an elongate neck
extends from the second chamber into the first chamber and said
orifice is provided in said neck.
Description
CROSS-REFERENCE TO RELATED PATENT
The structure to which this invention applies is of the type
described and disclosed in U.S. Pat. No. 3,299,354 (herein called
"the Related Patent") issued Jan. 17, 1967 for "Aperture Tube
Structure for Particle Study Apparatus" to the same inventor, and
owned by the same assignee, as the invention herein. The said
Related Patent is incorporated herein as a part hereof by specific
reference.
BACKGROUND OF THE INVENTION
1. Field of the Invention
This invention relates generally to the art of studying the
physical properties of particles carried in suspension and more
particularly is concerned with improved apparatus for obtaining
signals from particles passing through a scanning aperture without
extraneous interference from other particles.
2. Description of the Prior Art
The structure disclosed in the Related Patent substantially
decreases the possibility of undesirable spurious particle reading
and count signals which occurred in prior art devices. This is
accomplished by replacing the so-called aperture tube of prior art
structures with a pair of chambers having an interconnection for
separating the electrical and mechanical effects of the particles
passing through the aperture. Particles passing through the
aperture of the apparatus immediately are transported away from the
proximity of the aperture so that there is little or no chance of
spurious signals resulting from said particles.
One of the objects of the invention disclosed in the Related Patent
was to provide an aperture tube which is self-cleaning in that the
suspension in the immediate vicinity of the aperture is kept free
of extraneous particles. As acknowledged in the patent, however,
eddy currents of fluid in the aperture tube at the downstream end
of the primary bore occurred, and these eddy currents swirled into
the secondary bore immediately adjacent the primary bore. It was
believed that the fluid would be stagnant liquid substantially
devoid of particles, hence not introducing appreciable extraneous
signals, but while this was largely true, the action was not
sufficiently perfect to satisfy the more critical demands of
today's technology. A small percentage of particles were not caught
by the orifice in the elongate neck of the second chamber and these
sometimes produced extraneous signals by virtue of the eddy
currents at the bottom of the central chamber of the aperture
tube.
SUMMARY OF THE INVENTION
To resolve the aforesaid problems with regard to extraneous
signals, the present invention provides a selfcleaning aperture
tube as disclosed in the related patent, with the addition of a
pump device interposed between the first and second chambers to
produce a closed system in which there are no inlets or outlets
other than the primary bore in the first chamber. The pump operates
to draw the particle suspension up through the second chamber and
force the same back into the first chamber, completing a circuit
around this path and creating a sheath flow at the orifice. The
flow created by the pump is such as to ensure that all particles
introduced into the aperture tube are caught by the orifice of the
second chamber so as to prevent the occurrence of extraneous
signals.
Accordingly, the primary object of the invention is to provide an
improved structure which ensures that all particles passing through
the primary bore are caught by the orifice provided in the second
chamber of the aperture tube.
Other objects and advantages of the invention will occur to those
skilled in this art as a description of the invention proceeds in
connection with which a preferred embodiment is illustrated in the
accompanying drawing and set forth in the accompanying
specification.
BRIEF DESCRIPTION OF THE DRAWING
The drawing is identical to that of the Related Patent, except for
those elements added thereto in accordance with the invention
herein.
FIG. 1 is a sectional view through the apparatus of the Related
Patent, with the pump device and related elements of the invention
illustrated in diagrammatic form.
FIG. 2 is a fragmentary enlarged sectional view through the
apparatus in the vicinity of the aperture.
FIG. 3 is a diagrammatic view of a device operating in connection
with the manometer-syphon having the improved invention associated
therewith.
DESCRIPTION OF THE PREFERRED EMBODIMENT
In the following description, elements which are identical to those
disclosed in the related patent are referred to herein by the same
names and are indicated by the same reference numerals. Since the
related patent is incorporated herein as a part hereof by specific
reference, the disclosure thereof will not be repeated except in
instances where understanding of the invention herein will be
enhanced.
As illustrated in FIG. 1, a multiple chamber aperture tube or
vessel 14 comprising a first or central chamber 32 and a second
chamber 34 is suspended within a vessel 10. In operation, the
suspension 16 in vessel 10 will flow through the aperture 12 and
will, ideally, shoot directly into the orifice 40 and into the neck
36, to be carried thereafter along through chamber 34, conduit 46,
coupling 48, outlet conduit 50 and up branch 52. In the structure
of the Related Patent, the suspension would then continue to
discharge conduit 58 by way of passage 54 of stop-cock 56.
In order to ensure that all particles in suspension 16 are caught
by orifice 40 as they flow through aperture 12, the apparatus of
the invention includes a pump and associated elements designated
generally by the reference numeral 6, which elements have been
interposed between the two chambers 32, 34. In the embodiment
illustrated, a pair of T junctions 7, 8 have been spliced into
branch 52 and conduit 62, respectively, so as to introduce the
elements 6 into the flow system represented by the solid line
arrows throughout the aperture tube 14. A conduit 2 leads through a
filter 4 into pump 1 from junction 7, and conduit 3 leads out of
pump 1 into junction 8.
It is to be understood that the points of entry 7, 8 into the two
chambers 32, 34 could be made at any point along the lengths
thereof. The particular location shown is for illustrative purposes
only.
The addition of the elements 6 to the system of the related patent
produces a closed system within the aperture tube 14 whereby, upon
operation of pump 1, suspension 16 is sucked through neck 36, up
chamber 34, and through conduits 46, 50 and 2. The suspension then
passes through filter 4, where the particles suspended therein are
removed, and into pump 1. The particle free suspending liquid 16 is
then forced back into chamber 32 by way of conduits 3 and 62,
completing a circuit around this path and creating a sheath flow at
orifice 40. The sample flow as described in the related patent will
be unaffected since this closed system has no other inlets or
outlets.
Operation of pump 1 ensures that all particles in suspension 16 are
caught by the orifice 40 as they pass through aperture 12. The
added flow of clean suspension fluid, indicated by arrows 5 in FIG.
2, serves further to sweep the region of secondary bore 22 free of
all particles which are extraneous to those on which the sensing
operation is performed. By adjustment of the pump pressure, the
sheath flow 5 will be of proper strength to ensure that all
particles pass directly into orifice 40.
The operation and functions of all remaining elements illustrated
in the drawing are the same as described in the related patent.
* * * * *