U.S. patent number 3,744,763 [Application Number 05/106,425] was granted by the patent office on 1973-07-10 for apparatus for producing emulsions or suspensions.
This patent grant is currently assigned to Bayer Aktiengesellschaft, Deutsche Supraton, Bruchmann & Zucker KG. Invention is credited to Hildegard Schnoring, Friedrich J. Zucker.
United States Patent |
3,744,763 |
Schnoring , et al. |
July 10, 1973 |
APPARATUS FOR PRODUCING EMULSIONS OR SUSPENSIONS
Abstract
For the production of emulsions or suspensions, a centrifugal
homogenising machine is used which has a rotor, an end face of
which has rings formed with recesses. The rings revolve between
similar rings arranged on the housing, the emulsion being
introduced through at least two supply pipes arranged
concentrically of one another towards the end surface of the
rotor.
Inventors: |
Schnoring; Hildegard
(Wuppertal-Elberfeld, DT), Zucker; Friedrich J.
(Mulheim/Rhur, DT) |
Assignee: |
Bayer Aktiengesellschaft
(Leverkusen, DT)
Deutsche Supraton, Bruchmann & Zucker KG (Dusseldorf,
DT)
|
Family
ID: |
5760924 |
Appl.
No.: |
05/106,425 |
Filed: |
January 14, 1971 |
Foreign Application Priority Data
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|
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|
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Jan 30, 1970 [DT] |
|
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P 20 04 143.4 |
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Current U.S.
Class: |
366/178.1;
366/303; 366/317 |
Current CPC
Class: |
B01F
5/0451 (20130101); D21D 1/006 (20130101); B01F
3/0807 (20130101); B01F 7/00758 (20130101); B01F
2005/0008 (20130101); B01F 7/00766 (20130101) |
Current International
Class: |
B01F
7/00 (20060101); B01F 5/00 (20060101); B01f
007/16 () |
Field of
Search: |
;259/DIG.30,7,8,23,24,9,10,25,26,96,6,22 ;415/157,158 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Price; William I.
Assistant Examiner: Coe; Philip R.
Claims
We claim:
1. In a centrifugal homogenizing machine for the production of
emulsions or suspensions of one material in another material,
comprising:
a. a housing,
b. a rotor rotatably mounted in the housing, and having an end face
coaxial with the rotor, rotor ribs projecting axially outwardly
from the end face, in concentric and spaced relation defining
recesses between successive ribs,
c. housing ribs mounted on the housing projecting into the rotor
recesses for cooperation of the rotor and housing ribs for the
homogenizing upon rotation of the rotor,
d. two supply pipes disposed for concentric introduction,
respectively, of said materials centrally towards the end face of
the rotor for passage of the material between the rotor and housing
ribs, said supply pipes being axially spaced from the end face of
the rotor providing a gap between the supply pipes and the end
face,
e. a housing outlet for effluent from between the rotor and housing
ribs,
the improvement which comprises:
f. said supply pipes being adjustably mounted on the housing
permitting adjustment of the axially extended gap between the
supply pipes and end face of the rotor.
2. Machine according to claim 1, the mounting of the supply pipes
on the housing being for movement of the supply pipes together to
adjust said gap.
3. Machine according to claim 1, the supply pipes being separately
adjustable as aforesaid.
Description
The present invention relates to an apparatus for the production of
emulsions or suspensions, consisting of a centrifugal homogenising
machine, which is constructed from a housing, in which is arranged
a rotor, the end face of which is formed with rings having
recesses. The rings rotate between similar rings arranged on the
housing and a supply pipe opens centrally against the end face of
the rotor.
Emulsions and suspensions are normally produced in a form in which
two or more liquids are stirred together.
In the case where an emulsion is formed, the two liquid phases are
immiscible, whereas with the formation of a suspension, the two
substances in certain circumstances react wholly or partially with
one another to form a solid substance, which is then suspended in
the residual liquid.
The quality and particularly the stability of an emulsion or
suspension is characterized by the size of the drops or grains and
by the spectrum of the drop or grain sizes. Depending on the
intended use, different grain sizes with a corresponding grain size
spectrum are required.
In accordance with the present-day state of the art, emulsions and
suspensions are produced by one of the liquids being wholly or
partially introduced into a container equipped with a mixing member
and by then adding the other liquid or liquids.
The disadvantage of this procedure is that the residence time of
the components to be mixed and of the products being formed
therefrom differs in length. As a consequence, a difference is
produced in the number of actions on the individual volumetric
elements by the mixing member. From experience, these differences
in the number of impacts can assume values of several orders of
magnitude. The shorter the total residence time which has to be
maintained, the more serious is the effect of this difference.
Particularly when producing suspensions or emulsions with small
grain sizes, a short residence time is necessary, in order to
prevent grain size displacements which are caused by "Oswald
ripening", i.e. growth of the large particles at the expense of the
small particles because of dissolution and crystallization.
It is also known that the number of nuclei per unit of volume is
also determined by the oversaturation effects produced with the
combining of one of the phases, and that after nucleus formation
has occurred from the over-saturated solution, further addition of
solutions contributes predominantly to the growth of the already
formed nuclei or crystals, and thus reduces the number of the
individual parts which are formed, such as nuclei, droplets,
crystals.
It is known that such emulsions or suspensions produced in various
ways as described can be after-treated in so-called homogenising
machines, both piston-type homogenising machines and so-called
centrifugal apparatus, in order to obtain a comminution of the
oversize particles which are formed. However, this process has the
disadvantage of a relatively high expenditure and also the
disadvantage that the process can only proceed batchwise. In
addition, the division of the particles once they are formed is
only possible with relatively high energy consumption.
It is the object of the present invention to obviate the
disadvantages of the prior known apparatus. This is obtained by
using a centrifugal homogenising machine as initially referred to,
which machine is characterized by at least two supply pipes
arranged concentrically of one another.
The effect achieved in this way is that the homogenising machine as
known per se can be supplied with at least two phases, which are
very satisfactorily mixed together by the rotational movement and
by the beating action on the openings of the rotating rings.
It has proved to be particularly advantageous to make the gap
between the mouth of the supply pipes and the rotor adjustable.
It is advantageous for the gap for each supply pipe to be
separately adjustable. The product entering centrally into the
machine is accelerated radially by the rotation of the rotor and is
subjected to high shearing, deflecting and cavitation forces
between the rotating and stationary rings, which comprise, for
example, teeth, holes, pins and the like.
By the coaxial supply of the two components, it has been found in
connection with tests for the production of suspensions and
emulsions that a considerable technical advance can be produced as
regards the degrees of fineness of the grains and the grain size
spectrum.
Suspensions and emulsions can be produced in an extremely short
time with the apparatus of the invention, under conditions which
can be accurately controlled.
Another particular advantage consists in the continuous operation
of the apparatus. As a result of the adjustability of the gap
between the mouth of the supply pipes and the end face of the
rotor, it is possible substantially to determine the size of grains
in the suspensions to be produced.
The apparatus according to the invention is to be more fully
explained by reference to one constructional example shown in a
drawing:
FIG. 1 is an elevation in section of one embodiment of the
invention; and
FIG. 2 is an elevation in section of another embodiment according
to the invention.
In the figures, like reference characters refer to corresponding
parts.
A shaft 2 of a rotor 3 is mounted in bearings 4 and 5 in a housing
1. An end face 6 of the rotor is formed with ribs or toothed rings
7, which rotate between the ribs or toothed rings 8 fixedly
arranged on the housing 1. The two phases from which the emulsions
or suspension is to be formed are supplied through supply pipes 9
and 10, the discharge openings 11 and 12 of which are directed
concentrically and centrally towards the end face 6 of the rotor 3.
The two phases are accelerated radially and the actual suspending
or emulsifying action takes place in the region of the toothed
rings 7 and 8. The prepared emulsion or suspension leaves the
apparatus through a discharge pipe 13. The gap 14 between the rotor
and the outlet ends 11 and 12 of the supply pipes 9 and 10 is
adjustable by means of an adjusting screw 15. In the embodiment of
FIG. 1, the gap between the supply pipes and the rotor is
adjustable by moving the supply pipes as a unit; in FIG. 2 the
adjustment can be made by moving each pipe separately.
* * * * *