U.S. patent number 3,744,762 [Application Number 05/181,364] was granted by the patent office on 1973-07-10 for homogenizing method and apparatus.
This patent grant is currently assigned to Alfa-Laval Bergedorfer Eisenwerke GmbH. Invention is credited to Werner Schlicht.
United States Patent |
3,744,762 |
Schlicht |
July 10, 1973 |
HOMOGENIZING METHOD AND APPARATUS
Abstract
A method and apparatus for homogenizing liquids containing a
plurality of non-admixable phases. The liquid is forced under
pressure and at high speed from the radially outward to the
radially inward periphery of an annular gap, and during the passage
it is made to undergo cavitation once or repetitively.
Inventors: |
Schlicht; Werner (Hamburg,
DT) |
Assignee: |
Alfa-Laval Bergedorfer Eisenwerke
GmbH (Hamburg, DT)
|
Family
ID: |
5782877 |
Appl.
No.: |
05/181,364 |
Filed: |
September 17, 1971 |
Foreign Application Priority Data
|
|
|
|
|
Sep 19, 1970 [DT] |
|
|
P 20 46 326.7 |
|
Current U.S.
Class: |
366/338;
366/175.2; 366/340; 138/42 |
Current CPC
Class: |
B01F
5/0663 (20130101) |
Current International
Class: |
B01F
5/06 (20060101); B01f 005/08 () |
Field of
Search: |
;259/4,DIG.30 ;138/42,43
;251/127 |
References Cited
[Referenced By]
U.S. Patent Documents
Foreign Patent Documents
|
|
|
|
|
|
|
1,371,350 |
|
Jul 1964 |
|
FR |
|
138,592 |
|
Nov 1961 |
|
SU |
|
Primary Examiner: Price; William I.
Assistant Examiner: Cantor; Alan I.
Claims
What is claimed as new and desired to be protected by Letters
Patent is set forth in the appended
1. A homogenizing method for liquids containing non-admixable
phases, comprising the first step of establishing an annular gap
having an outer and an inner periphery; the second step of passing
a multi-phase liquid under pressure and at high speed through said
annular gap from said outer towards said inner periphery thereof;
and the third step of causing the development of cavitation in said
liquid during passage thereof through said annular gap.
2. A method as defined in claim 1, wherein said third step
comprises causing the repeated development of cavitation during
passage of said liquid through said annular gap.
3. A homogenizing apparatus, particularly for homogenizing liquids
containing a plurality of non-admixable phases, comprising first
means defining an annular gap having an outer and an inner
periphery and being bounded by a pair of juxtaposed surfaces; and
second means for effecting the development of cavitation in liquid
passing at high speed and under pressure through said annular gap
from said outer towards said inner periphery thereof.
4. An apparatus as defined in claim 3, said second means comprising
at least one annular groove provided in at least one of said
surfaces, the dimensions of said annular groove and of said annular
gap being so coordinated that the liquid pressure within said
annular gap is below, and in the region of said annular groove is
above the boiling pressure of the continuous phase of said
liquid.
5. An apparatus as defined in claim 4; and further comprising at
least one additional annular groove provided in said one surface
and concentric with said one annular groove.
6. An apparatus as defined in claim 5, wherein said annular grooves
are closer to said inner periphery than to said outer
periphery.
7. An apparatus as defined in claim 3; and further comprising at
least one shear nozzle upstream of said annular gap and through
which said liquid is compelled to pass.
Description
BACKGROUND OF THE INVENTION
The present invention relates generally to the homogenization of
liquids, and more particularly to the homogenization of liquids
containing several non-admixable phases. Still more particularly
the invention relates to a method and an apparatus for effecting
such homogenization.
The art already knows homogenizing apparatus in which liquids
containing several non-admixable phases --which liquids are usually
supplied in form of emulsions--are forced under high pressure from
the radially inner to the radially outer periphery of an annular
gap. In so doing the droplets of the dispersed phase are subdivided
as a result of the shear tension which is caused during the passing
of the liquid through this gap. After exiting at the radially outer
periphery of the gap the liquid particles impinge at high speed on
an abutment surface provided for this purpose, the intention being
to obtain a subsequent further reduction in size of the particles
by fragmentation.
These prior-art approaches to the problem at hand have been found
suitable in a variety of instances. It has, however, been observed
that in so far as the degree of homogenization which can be
obtained with them, their effectiveness is definitely limited.
Hence, there continues to exist a need for a method and an
apparatus which will provide improved homogenization in a simple
and effective manner.
SUMMARY OF THE INVENTION
It is, accordingly, an object of the present invention to provide
this improvement.
More particularly it is an object of the present invention to
provide an improved method for homogenizing liquids containing
several non-admixable phases.
A concomitant object of the invention is to provide an apparatus
for carrying out the novel method.
In pursuance of these objects, and of others which will become
apparent hereafter, one feature of the invention resides in a
homogenizing method for liquids containing non-admixable phases,
which method comprises, briefly stated, the step of establishing an
annular gap having an outer and an inner periphery. Thereupon, a
multi-phase liquid containing separate non-admixable phases is
passed under pressure and at high speed through the annular gap
from the outer towards the inner periphery thereof. During the
passage through this gap the liquid is caused to undergo
cavitation. This method provides the desired improvements.
An apparatus for carrying out the novel method comprises means
defining an annular gap having a radially inner and a radially
outer periphery and being bounded by a pair of juxtaposed surfaces.
The supply channel for the liquid to be homogenized communicates
with the radially outer periphery and the removal channel
communicates with the radially inner periphery, and during passage
between the juxtaposed surfaces bounding the radial gap the liquid
is caused by suitable means to undergo cavitation.
According to a currently preferred embodiment of the apparatus at
least one of the surfaces is provided with one or several
concentric annular grooves which preferably are closer towards the
radially inner periphery than the radially outer periphery of the
annular gap. The dimensions of the grooves and the width of the
annular gap are so coordinated with one another and with the
pressure at which the liquid is supplied that in operation there
will develop in the annular gap alternating regions in which the
pressure of the liquid is respectively above and below the boiling
pressure of the continuous phase of the liquid. It is further
advantageous, in a sense improving the homogenizing effect, to
provide upstream of the annular gap at least one shear nozzle known
per se and through which the liquid is made to pass, in order to
supply the liquid in adequately prehomogenized state to the annular
gap.
The novel features which are considered as characteristic for the
invention are set forth in the appended claims. The invention
itself, however, both as to its construction and its method of
operation, together with additional objects and advantages thereof,
will be best understood from the following description of specific
embodiments when read in connection with the accompanying
drawing.
BRIEF DESCRIPTION OF THE DRAWING
The single FIGURE is a somewhat diagrammatic axial section through
an apparatus according to the present invention.
DESCRIPTION OF THE PREFERRED EMBODIMENTS
Discussing the drawing now in detail, it will be seen that in the
illustrated apparatus there is provided a hollow cylindrical jacket
or casing 7 in which there are mounted--spaced from one another in
the direction of fluid flow through the jacket, as indicated by the
two arrows--a homogenizing plate 4 and the axially apertured
homogenizing seat member 5. The plate 4 has a supply channel 1
composed of the illustrated axial inlet bore, radial passages and
an outer annular chamber portion. All of these portions of the
channel 1 are clearly illustrated and none of them are believed to
require a more detailed discussion. To effect pre-homogenization of
the liquid a shear nozzle 8 known per se is installed in the axial
bore of the channel 1 so that the liquid to be homo-genized must
pass through the nozzle 8 before it can reach the annular gap still
to be described.
An axial removal or outflow channel 3 communicates with the
aperture in the homogenizing seat 5.
According to the present invention the juxtaposed surfaces of the
plate 4 and the seat 5 define with one another a radial annular gap
2 having a radially outer and a radially inner periphery. The
liquid entering through the nozzle 8 will flow around the plate 4
and enter the gap 2 at the radially outer periphery thereof,
passing at high speed and under pressure in the radially inward
direction to the radially inner periphery of the gap 2 and from
there into the channel 3. In the illustrated embodiment both of the
surfaces bounding the gap 2, which are identified with reference
numerals 4a and 5a, respectively, are each provided with three
concentric annular grooves 6. However, only one of these surfaces
could be provided with only one of these grooves, or with two or
more of them. The width of the gap 2 and the dimensions of the
grooves 6 are so coordinated with one another that in the gap 2
there will develop in operation alternating regions in which the
pressure to which the liquid is subjected will be below and above
the boiling pressure of the continuous phase of the liquid.
Because the flow of the liquid is radially inward from the outer to
the inner periphery through the gap 2, the pressure will decrease
in the gap because of the linear decrease in cross-section. This
means that, if the dimensions and flow conditons are appropriately
selected and coordinated, the pressure of the liquid passing
through the gap 2 will drop below the boiling pressure of the
continuous phase in the gap 2, but not in the annular grooves 6. In
so far as the annular grooves 6 are concerned, it will be
appreciated that the sudden cross-sectional increase experienced by
the liquid on encountering the grooves 6 results in a shock-like
increase of the pressure above the boiling pressure, so that the
vapor bubbles which have formed in the annular gap prior to
encountering of the respective grooves 6 because the pressure had
been below the boiling pressure, will collapse and the droplets of
the dispersed liquid phase will be very finely distributed.
Advantageously the grooves 6 will be closer to the inner periphery
of the gap 2 than to the outer one, and by utilizing several of the
grooves 6 which are encountered successively as the liquid passes
through the gap 2, alternating vaporization and cavitation zones
are obtained. Because the cross-section of the annular gap 2
decreases in direction from the outer towards the inner periphery
the pressure in each successive annular vaporizing zone is lower
than in the preceding one, so that renewed vaporization will result
in each cavitation zone.
It is pointed out that the configuration and the dimensioning of
the plate 4 and of the seat 5, as well as the width and radial
length of the annular gap 2 and the arrangement and dimensioning of
the grooves 6, as well as the speed at which liquid is supplied
into the gap 2, can be determined and coordinated with reference to
one another by persons with ordinary skill in the art given the
above information and in dependence upon the liquid to be
homogenized and the degree of homogenization which it is desired to
obtain. It is not absolutely necessary that the liquid be
pre-homogenized, as by passing it through the nozzle 8, before
entering into the gap 2, but if it is desired to obtain
homogenization conditions, then it is important that such
pre-homogenization be provided.
It will be understood that each of the elements described above, or
two or more together, may also find a useful application in other
types of constructions differing from the types described
above.
While the invention has been illustrated and described as embodied
in the homogenization of liquids, it is not intended to be limited
to the details shown, since various modifications and structural
changes may be made without departing in any way from the spirit of
the present invention.
Without further analysis, the foregoing will so fully reveal the
gist of the present invention that others can by applying current
knowledge, readily adapt it for various applications without
omitting features that from the standpoint of prior art fairly
constitute essen-tial characteristics of the generic or specific
aspects of this invention and, therefore, such adaptations should
and are adapted to be comprehended within the meaning and range of
equivalence of the following claims.
* * * * *