U.S. patent number 3,736,360 [Application Number 05/192,999] was granted by the patent office on 1973-05-29 for control system for vacuum furnaces.
This patent grant is currently assigned to Allmanna Svenska Elektriska Aktiebolaget. Invention is credited to Carl Bergman, Paul Larsson.
United States Patent |
3,736,360 |
Bergman , et al. |
May 29, 1973 |
CONTROL SYSTEM FOR VACUUM FURNACES
Abstract
A control system for an electrically heated furnace for
sintering powder bodies, especially bodies of hard metal, has a
vacuum pump connected to the interior of the furnace chamber by a
suction conduit. The furnace includes a plurality of heating
elements for different zones, a temperature sensitive instrument
for each zone and a controlled measuring instrument for one of the
zones which is the master zone. These instruments are connected to
a master regulator for the furnace and slave regulators for the
individual zones. A throttle valve in the vacuum conduit, or a
controlled tap connected to the vacuum conduit, make it possible to
keep the pressure in the furnace constant despite the fact that the
pump runs at a constant speed. A pressure-sensing member connected
to the vacuum conduit is also connected to the regulators for the
heating elements.
Inventors: |
Bergman; Carl (Vasteras,
SW), Larsson; Paul (Vasteras, SW) |
Assignee: |
Allmanna Svenska Elektriska
Aktiebolaget (Vasteras, SW)
|
Family
ID: |
20299179 |
Appl.
No.: |
05/192,999 |
Filed: |
October 27, 1971 |
Foreign Application Priority Data
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|
|
|
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Oct 27, 1970 [SW] |
|
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14477/70 |
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Current U.S.
Class: |
373/112; 236/15R;
236/15C; 373/135 |
Current CPC
Class: |
G05D
16/202 (20130101); B22F 3/1007 (20130101); B22F
3/10 (20130101); C04B 35/56 (20130101); B22F
2203/03 (20130101); B22F 2201/20 (20130101) |
Current International
Class: |
B22F
3/10 (20060101); C04B 35/56 (20060101); G05D
16/20 (20060101); F27d 007/06 () |
Field of
Search: |
;13/24,31 ;219/496
;236/15A,15B,15C,78A,92 |
References Cited
[Referenced By]
U.S. Patent Documents
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|
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3428250 |
February 1969 |
Holthausen |
3291969 |
December 1966 |
Speransky et al. |
|
Primary Examiner: Envall, Jr.; Roy N.
Claims
We claim:
1. Method of controlling a vacuum furnace system comprising a
vacuum furnace having an electrical heating element, regulating
means between said element and an electric power source controlling
the heating effect of said elements, a vacuum pump, and a suction
conduit element having a gas flow regulating means therein joining
the furnace to the vacuum pump, which method comprises sensing the
vacuum in said suction conduit element and controlling said gas
flow regulating means in response to variations of such vacuum to
maintain the pressure in the furnace substantially constant.
2. Method according to claim 1, which comprises controlling the
heating effect of the furnace elements in response to variations of
said vacuum.
3. Method according to claim 1, which comprises supplying gas from
a gas source to the conduit element between the furnace and the
vacuum pump by a gas flow regulating means, said supplying of gas
maintaining the vacuum pressure level within the preselected
level.
4. Method according to claim 1, which comprises controlling the
heating effect of the furnace elements in response to the setting
of the gas flow regulating means.
5. Vacuum furnace equipment which comprises an electrically heated
furnace element, a vacuum pump, a suction conduit element joining
the furnace to the vacuum pump, heating means in said furnace, a
current source, power control equipment arranged between the
current source and the furnace element to regulate the heat
supplied to the furnace, which includes a pressure sensing member,
which senses the pressure in the furnace or conduit element and
includes means to deliver an output signal dependent on the
pressure, and a gas flow regulating member, and means connected to
said pressure sensing member for setting the flow regulating member
in a position in accordance with said pressure dependent signal to
maintain the vacuum in said suction conduit element substantially
constant.
6. Vacuum furnace equipment according to claim 5, including means
responsive to said pressure sensing member to control the heat
supplied to the furnace.
7. Vacuum furnace equipment according to claim 5, in which said gas
flow regulating member comprises a throttling member in the suction
conduit, and means setting said throttling member in response to
the output signal of said pressure sensing member to maintain the
pressure in the suction conduit above a minimum preselected
value.
8. Vacuum furnace equipment according to claim 7, which comprises a
unit which senses the setting of the throttling member and includes
means to emit an output signal dependent on the setting of said
member, which influences the power control equipment regulating the
heat effect supplied to the furnace.
9. Vacuum furnace equipment according to claim 5, which comprises a
valve with an adjustable throttling member connected to the suction
conduit element between the furnace element and the vacuum pump,
and means responsive to the output signal of the pressure sensing
member to control said throttling member to supply gas to the
suction conduit when the pressure in this conduit falls below a
minimum preselected value.
10. Vacuum furnace equipment according to claim 5, which comprises
a unit which senses the setting of the throttling member and
includes means to emit an output signal dependent on the setting of
said member, which influences the power control equipment
regulating the heat effect supplied to the furnace.
Description
BACKGROUND OF THE INVENTION
1. Field of the Invention
The present invention relates to a control system for a vacuum
furnace for sintering powder bodies, preferably bodies of hard
metal. The control system regulates the heating of the furnace
during that part of the heating process when degassing takes place.
The control system can be used in furnaces of the type described in
Swedish published specification No. 333,437.
2. The Prior Art
Bodies of hard metal are manufactured of powder containing carbides
of tungsten, tantalium, titanium or vanadium or a mixture of two or
more carbides of these substances and a binder which may consist of
cobalt and/or nickel, or possibly iron. The total carbide content
is usually 70-99 percent and the content of binder 1- 30 percent.
The powder has a great tendency to absorb or react with the gases
in the atmosphere, mainly oxygen (O.sub.2) and water vapour. These
substances are removed by degassing during heating, by performing
the heating under vacuum. When hard metal is being degassed it is
desirable to keep the pressure below a certain level during the
entire degassing process. The heating is usually carried out as
quickly as possibly, i.e., the heating is performed with the
highest power or with the highest permissible temperature gradient
tolerated by the furnace or and workpiece. The gas emission is
usually very irregular, however, for hard metal and it has a
pronounced maximum which for many composites is at about
700.degree.C. If, as is desirable, the gases are to be removed
without the pressure rising above a certain level, an extremely
large and expensive vacuum equipment is necessary with a constant
temperature gradient. Too much gas emission may also cause cracks
in the workpiece due to the explosive action of the gases. In
certain cases, therefore, the power supply has been controlled in
accordance with the temperature.
SUMMARY OF THE INVENTION
According to the invention the heating is controlled depending on
the pressure in the furnace and the furnace equipment is provided
with pressure-sensing members to sense the pressure in the furnace
or in a suction conduit and power regulating members which, in
accordance with the output signal from said pressure sensing
member, regulate the power supply to the heating element in the
furnace. Further characteristics of the invention include a control
system for an electrically heated furnace for sintering powder
bodies, especially bodies of hard metal, has a vacuum pump
connected to the interior of the furnace chamber by a suction
conduit. The furnace includes a plurality of heating elements for
different zones, a temperature sensitive instrument for each zone
and a controlled measuring instrument for one of the zones which is
the master zone. These instruments are connected to a master
regulator for the furnace and slave regulators for the individual
zones. A throttle valve in the vacuum conduit, or a controlled tap
connected to the vacuum conduit, make it possible to keep the
pressure in the furnace constant despite the fact that the pump
runs at a constant speed. A pressure-sensing member connected to
the vacuum conduit is also connected to the regulators for the
heating elements.
The invention offers several advantages. The gas emission within
the temperature range where it is maximum can be limited to a
maximum value adapted to a vacuum equipment and the size of the
equipment can be considerably reduced, often to only 25 percent of
what was previously considered suitable. The control also makes it
possible to very accurately determine the pressure within the
temperature ranges where the gas emission is slight, so that the
pressure can be held permanently above the level at which damaging
gasification of components forming the hard metal is obtained, for
example cobalt. In many cases it is suitable to keep a pressure of
1.10.sup.-.sup.1 torr in the furnace. The loss of cobalt is then
negligible. The control system also makes it possible in a
controlled manner to regulate the pressure according to the
temperature.
BRIEF DESCRIPTION OF THE DRAWINGS
The invention will be described further with reference to the
accompanying drawings.
FIG. 1 shows schematically one embodiment of the invention,
FIG. 2 a variant of a regulating means included in the means shown
in FIG. 1,
FIG. 3 gas emission from a hard metal body weighing 150 kg when
heated with constant supply of power, i.e., with an approximately
constant temperature gradient and
FIG. 4 shows the temperature of the workpiece as a function of the
time when using the invention.
DESCRIPTION OF THE PREFERRED EMBODIMENTS
In FIGS. 1 and 2, 1 designates a sintering furnace which is sealed
with respect to the surroundings so that a vacuum can be maintained
therein. The furnace is connected by a conduit 2 to a pump 3. In
the furnace is a workpiece 4 which has been formed by compacting
powder. The furnace 1 is divided into four different zones, each
with its own heating element 5a, 5b, 5c and 5d which through a
cable 6 are supplied with electric power from a current source, not
shown, by way of regulators 7a, 7b, 7c and 7d. The cable contains
conductor pairs 6a, 6b, 6c and 6d for the elements in each of the
heating zones. The regulators may be constructed of AC regulators
with thyristors, for example ASEA type YQNA and of power regulators
comprising PI regulators, multipliers and summating means made by
ASEA and designated QRTN 201, QRTF 205 and QRTF 201 and measuring
units for voltage and current to the heating elements.
One zone in the furnace is the master zone and the others are slave
zones. In all the zones there are thermoelements 8a, 8b, 8c and 8d
which give the real value to the control equipment for the
temperature in the four zones of the furnace. Furthermore, in one
zone, the master zone, there is a thermoelement 9 which sets the
desired value for the temperature in the slave zones, which is
equal to the real value in the master zone. Through conduits 10a,
10b, 10c, 10d and 10e in the conductor bundle 10 the thermoelement
is in communication with a temperature regulator 11 which is a
master regulator and temperature regulators 12a, 12b and 12c which
regulate the temperatures in the different zones of the furnace. As
master regulator a regulator can be used which has a scale 13 on
which a desired value can be set for the final sintering
temperature to be reached. The real value is obtained from the
thermoelement 8d in the master zone in the furnace. A regulator of
the make Eurotherm 0.degree.-1800.degree.C type PID can be used.
Temperature regulators of the make Eurotherm -3 -3mV type PID can
be used as slave regulators. The slave regulators regulate the
temperature in the respective slave zones so that it is as close to
the temperature in the master zone as possible. The desired value
for the slave regulators comes from the thermoelement 9 in the
master zone and the real value from the thermoelements 8a, 8b and
8c in each zone. A pressure gauge 15, for example of a type having
a logarithmic scale, is connected to the conduit 2 and emits a
signal dependent on the value shown on the indicator. The signal is
supplied to a vacuum regulator 16.
A PI regulator sold by ASEA under the designation QALB may be used.
The regulator 16 activates a servomotor 17 in FIG. 1 to set a
throttle valve 18 in the vacuum conduit 2 so that the pressure in
the furnace 1 can be kept constant in spite of a constant speed of
the pump 3. The equipment also includes a regulator 19 which can
either be directly actuated by the output signal from the regulator
or by a member which senses the position of the valve 18. In this
way the regulator senses how much of the pump capacity is being
used and delivers a signal dependent on this, this signal being
delivered through the conduit 20 to the regulators 7a, 7b, 7c and
7d so that these increase the power supply to the furnace when the
pump capacity is not fully exploited. The regulator 19 may be a PI
regulator, make ASEA, type QALB 210.
If a furnace with high power is used, the use of all the available
power may cause too rapid heating for certain types of material if
the capacity of the vacuum pump does not limit the heating rate. It
may therefore be suitable to use a power limiter 21 which senses
the temperature derivative. This may be provided with a setting
device for the desired value. The real value can be obtained by
measuring the alteration of resistance in the heat coils in the
master zone. When the real value exceeds the desired value the
power limiter emits an output signal which is supplied to the
regulators 7a, 7b, 7c and 7d so that they decrease the power
supplied to the furnace. The power limiter may be built up of
resistance measuring units, a motor operating device for reference
comparison and a PI regulator, make ASEA, type QALB 210.
If the equipment is to operate at different pressures at different
furnace temperatures it may be provided with a program mechanism 24
into which the desired value for the pressure is programmed. This
program mechanism delivers an output signal dependent on the
program, this signal being supplied to the vacuum regulator 16.
In the embodiment according to FIG. 2 the pressure in the furnace 1
is regulated when the quantity of gas emitted is less than the pump
capacity at the desired pressure, by letting air into the conduit 2
through a controllable valve 25. This valve is operated by means of
a servomotor 26 of the same type as the servomotor 17. Otherwise
the equipment is in agreement with that shown in FIG. 1 and the
function is the same.
The curve 30 in FIG. 3 shows the relationship between the quantity
of gas emitted from workpiece per time unit and the temperature
upon heating with constant temperature increase per time unit. The
time t hours and the temperature T.degree.C are indicated along the
abscissa. while along the ordinate the gas quantity emitted Q
torr.sup.. 1/sec is indicated. As can be seen from the values on
the abscissa, the workpiece is being heated 100.degree.C/h. The
curve 30 shows that the gas emission has a pronounced maximum at
about 750.degree.C. The gases emitted are mainly carbon monoxide
(CO), carbon dioxide (CO.sub.2), water vapour (H.sub.2 O) and
hydrogen (H.sub.2). According to the invention, the heating of the
furnace is dependent on the furnace pressure in such a way that the
temperature gradient in the range 600.degree.C to 850.degree.C is
limited to such a value that the gas emission corresponds to the
maximum capacity of the vacuum pump at the furnace pressure
selected.
FIG. 4 shows an example of the relationship between the time t in
hours and the temperature T in .degree.C. As can be seen from the
drawing, the curve representing the temperature gradient is
extremely flat in the range between 600.degree.C and
800.degree.C.
* * * * *