U.S. patent number 3,688,514 [Application Number 05/100,271] was granted by the patent office on 1972-09-05 for cryostats.
This patent grant is currently assigned to L'Air Liquide, Societe Anonyme pour L'Etude et. Invention is credited to Roger Prost.
United States Patent |
3,688,514 |
|
September 5, 1972 |
CRYOSTATS
Abstract
A cryostat, which makes use of a cryogenic liquid at very low
temperature, for example liquid helium, as a medium to surround a
specimen being tested, comprises a double-walled tank disposed
within and spaced from a double-walled insulating jacket under
vacuum. The suspension of the tank is effected by a double annular
connection with the bottom of the inner wall of the insulating
jacket. A reflector screen is cooled by the nitrogen of a
reservoir. The cryostat can be used for testing materials or for
enabling apparatus to function at very low temperature.
Inventors: |
Roger Prost (Saint Egreve,
FR) |
Assignee: |
L'Air Liquide, Societe Anonyme pour
L'Etude et (N/A)
|
Family
ID: |
9045135 |
Appl.
No.: |
05/100,271 |
Filed: |
December 21, 1970 |
Foreign Application Priority Data
|
|
|
|
|
Dec 24, 1969 [FR] |
|
|
6944794 |
|
Current U.S.
Class: |
62/51.1 |
Current CPC
Class: |
F17C
3/085 (20130101); F17C 2221/017 (20130101) |
Current International
Class: |
F17C
3/00 (20060101); F17C 3/08 (20060101); F17c () |
Field of
Search: |
;62/45,514,514A |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: William J. Wye
Attorney, Agent or Firm: Young & Thompson
Claims
What is claimed is:
1. A cryostat comprising: a. a tank for receiving a cryogenic
liquid and a specimen to be tested, the said tank having a large
upper opening, a thick bottom, an internal lateral wall and an
external lateral wall, a rim connecting together said walls at
their upper ends, said walls defining between them an annular
heat-insulating space, b. a jacket disposed around and spaced from
the said tank, said jacket having a thick bottom, an internal
lateral wall and an external lateral wall defining between them an
annular heat-insulating space, a flange connecting together said
walls of the jacket at their upper ends, c. said tank bottom and
said jacket bottom defining between them a lower heat-insulating
space communicating with said annular heat-insulating spaces of the
tank and jacket, d. and tank-supporting means comprising radial
extension means between said tank bottom and said internal wall of
said jacket, said external wall of said tank being fixed to said
supporting means, one part of said supporting means being disposed
between said tank bottom and said external wall of said tank and
being gas permeable, another part of said supporting means being
disposed between said external wall of said tank and said internal
wall of said jacket and being gas impervious.
2. A cryostat as claimed in claim 1, said jacket extending upwardly
beyond said tank, a flange secured between the upper edges of the
internal and external lateral walls of the jacket, a cover on said
jacket flange, and a reservoir for a cryogenic liquid and occupying
most of the space between the jacket, the tank and the cover.
3. A cryostat as claimed in claim 1, said one part of said
supporting means comprising stays spaced from one another and
defining passages between said lower insulating space and said tank
insulating space.
4. A cryostat as claimed in claim 1, said one part of said
supporting means comprising stays having internal passages between
said lower insulating space and said tank insulating space.
5. A cryostat as claimed in claim 2, and a refrigerated shield in
the insulation space of the jacket, said shield being in thermal
contact with said reservoir by means of the internal wall of the
jacket, and spacers between said internal wall of jacket and said
reservoir.
6. A cryostat as claimed in claim 2, and suspension means between
said reservoir and said cover.
7. A cryostat as claimed in claim 6, said suspension means
including a heat-insulated conduit for filling the reservoir.
8. A cryostat as claimed in claim 2, and a passage pipe extending
completely through the reservoir and opening at its lower end below
the tank and at its upper end opposite a conduit passing through
the cover.
Description
The present invention relates to cryostats which use a cryogenic
liquid at very low temperature, for example liquid helium, as a
medium to surround a specimen being tested.
There are known cryostats which comprise a tank holding a cryogenic
liquid and a specimen, the tank preferably having double walls
under vacuum, positioned inside a jacket or casing, which itself
has a double side wall under vacuum, the insulating jacket
extending to a considerable distance above the tank and being
disposed at a distance from the side wall of the tank, with a
common bottom space provided between a tank bottom and a jacket
bottom with a single wall. In this type of cryostat, the
interstitial space between the internal wall of the jacket and the
external wall of the tank serves for the circulation of vapors
originating from the cryogenic liquid contained in the tank, these
vapors first of all circulating downwardly and along the external
side wall of the tank and then upwardly and along the internal wall
of the external insulating jacket. Cryostats of this type are
particularly useful, because they can be made with a large neck,
that is to say, with a large opening for inserting the specimens to
be tested, which thus may have considerable dimensions; however,
they are particularly complex and difficult to construct,
particularly because of the method of fixing the tank, which is
effected at the upper lever of the external jacket in the immediate
vicinity of the cover, passing in succession through the internal
tank wall, then to the upper edge of the tank, through the external
tank wall and finally through the internal wall of the insulating
jacket, so that these walls necessarily all have to be of
dimensions for resisting the stresses caused by weight and exerted
by the liquid and the specimen placed in the tank.
An object of the present invention is to provide a cryostat, the
design of which permits a particularly robust and simple
construction. A further object of the invention to provide a
cryostat of this type which has improved insulating means for the
tank containing the cryogenic liquid.
SUMMARY THE INVENTION
According to the invention, the tank is fixed to the jacket by a
double annular connection, one fluid-tight connection extending
between the lower edges facing the external wall of the tank and
the internal wall of the jacket, while the other is between the
lower edges facing the internal and external walls of the tank.
This arrangement, which transfers to the bottom of the cryostat the
suspension of the tank from the external jacket, has the advantage
that the strains which are exerted on the tank, coming from the
insulation space, the mass of cryogenic liquid and the specimen
subjected to cold, are no longer transmitted through the tank
walls, but directly from the tank bottom to the external jacket. It
is thus no longer necessary to make the tank wall with a robustness
such that it is capable of transmitting the stresses or strains
being exerted on the tank: it is sufficient to provide a good
direct mechanical connection between the tank bottom and the
internal wall of the jacket, the shape of which, being a simple
cylindrical surface, is able to transmit these stresses without
appreciable risk of deformation.
According to another feature of the invention, in a cryostat of the
type in question, also comprising means forming an intermediate
refrigerated screen between the internal tank and the external
jacket, these means are provided by a nitrogen reservoir completely
overhanging the said tank and a heat-conducting screen around the
bottom and lateral walls of the tank, in the vacuum space of the
insulating jacket, and in thermal contact by its upper edge with
the liquid nitrogen reservoir. This arrangement is simple, and not
only ensures a thermal protection of the tank in the upward
direction, between the cover and the top of the tank, but also a
lateral and bottom protection by a single heat-conducting wall,
which is regularly and systematically cooled by the nitrogen
present in the upper reservoir. This arrangement, which ensures an
excellent insulation of the tank, is however very much less clumsy,
because it makes use of a reservoir forming a source of cold,
established in the necessary clearance volume between the top of
the tank and the cover.
DESCRIPTION OF THE PREFERRED EMBODIMENT
The features and advantages of the invention will however become
more apparent from the following description, given by way of
example and by reference to the accompanying drawing, in which the
single FIGURE is a sectional view of a cryostat according to the
invention.
Referring to this FIGURE, it is seen that the cryostat comprises a
tank 1, which is adapted for example to be filled with helium, the
said tank being mounted in the lower part of an external jacket 2.
The tank 1 is formed of a bottom 3 of adequate thickness and a
double lateral wall under vacuum, namely, firstly an internal wall
4 connected by an upper rim 5 to an external wall 6, which itself
is secured by an annular flange 7 to the base 8 of an internal wall
9 of the jacket 2, the external wall 10 of which is made fast with
a cryostat base 11. A series of annular stays 12, formed of tube
sections, is also disposed between the tank bottom 3 and the
annular flange 7, these tube sections thus permitting
communications between the double wall of the tank 1 and the double
wall of the jacket 2. This tank double wall and this jacket double
wall are thus simultaneously brought under vacuum. It is understood
that a rigid mechanical connection has been produced between the
tank bottom 3 and the internal wall 9 of the jacket 2, firstly by
the stays 12 and then by the flange 7.
As will be seen from the drawing, the lateral wall of the jacket 2
extends a considerable distance above the lateral wall of the tank
1; the jacket wall 2 is made fast at its upper end, by a flange 13
on which a cover 14 is fixed in fluid-tight manner. Situated in the
interstitial space between the cover 14 and the tank 1 is a
nitrogen reservoir 16, which extends over practically all the
diametral width of the internal wall 9 of the jacket 2, while
nevertheless providing a small interstitial annular clearance 17,
the purpose of which will be seen later. This nitrogen reservoir 16
is itself formed on one lateral side and on its upper side with a
double wall 18, 19, 20, 21, respectively, permitting the
establishment of an insulating jacket under vacuum. The reservoir
16 is suspended from the cover 14 by passage members 22 and 23, one
member 22 serving for the admission of liquid nitrogen into the
reservoir 16, while one member 23 serves for the discharge of the
vapors which are released. The said members 22 and 23 are heat
insulated by a double wall 24, 25, in communication with the vacuum
established around the liquid nitrogen reservoir 16. This liquid
nitrogen reservoir also has a flow pipe 26 over its full height and
opening at its bottom end opposite the tank 1 and at its upper end
in the form of a funnel 26a, beneath a pipe 27 for the admission of
helium through the cover 14. This reservoir 16 is thermally
associated with a heat shield 28 extending completely around the
bottom and lateral walls of the tank, between the walls 9 and 10 of
the double jacket 2 and between the bottom walls 3 and 11; this
shield 28 is in thermal contact at its upper end with the internal
jacket wall and then with a number of spacer members 29, which are
themselves in thermal contact with the liquid nitrogen reservoir
16.
It is seen that the arrangement as described permits the
transmission of the stresses exerted on the tank 1 essentially by
means of the stay tubes 12 and the annular flange 7, without
passing through the lateral walls (4, 6) of the tank, and that in
addition the interstitial space between the top of the tank 1 and
the cover 14 is occupied by a liquid nitrogen reservoir 16, the
purpose of which, apart from that of heat protection towards the
top of the refrigerating liquid in the tank 1, is essentially to
ensure a continuous cooling of the reflector shield 28 located in
the vacuum of the jacket 2, all around the lateral walls and the
tank bottom 1. It is apparent that this construction is very
robust, since it is sufficient to provide a relatively thick bottom
3 for the tank 1, and a small clearance, since the refrigerated
reflector shield 28, which is disposed in the double jacket 9, 10
and 3, 11, is associated with a liquid nitrogen reservoir, which
occupies the normally free clearance between the top of the tank 1
and the cover 14.
* * * * *