U.S. patent number 3,616,032 [Application Number 04/740,877] was granted by the patent office on 1971-10-26 for method of attaching polyvinyl base to pressure vessel.
This patent grant is currently assigned to Pressed Steel Tank Co., Inc.. Invention is credited to Willert O. Kugler.
United States Patent |
3,616,032 |
Kugler |
October 26, 1971 |
METHOD OF ATTACHING POLYVINYL BASE TO PRESSURE VESSEL
Abstract
A primer is applied to the exterior surface of the bottom of a
metal vessel. The vessel and primer are heated above the plastic
temperature of a base made of polyvinyl chloride and, while above
that temperature, are pressed into engagement with the polyvinyl
chloride base. The primer preferably is partially thermosetting and
partially thermoplastic. After a sufficient amount of time to
achieve surface fusion between the primer and the base, but before
heat can permeate the base too deeply, cooling water is poured into
the vessel to rapidly cool the vessel bottom and the fusion
interface.
Inventors: |
Kugler; Willert O. (Milwaukee,
WI) |
Assignee: |
Pressed Steel Tank Co., Inc.
(Milwaukee, WI)
|
Family
ID: |
24978440 |
Appl.
No.: |
04/740,877 |
Filed: |
June 28, 1968 |
Current U.S.
Class: |
156/286; 220/605;
220/634; 156/307.1; 220/628 |
Current CPC
Class: |
B01J
3/04 (20130101) |
Current International
Class: |
B01J
3/04 (20060101); C09j 003/00 () |
Field of
Search: |
;156/293,285,286,287,306,309 ;29/472.9 ;264/90-92 ;161/214
;117/75,123A ;220/69 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Padgett; Benjamin R.
Assistant Examiner: Solyst; Gary G.
Claims
I claim:
1. A method for securing a base made from a thermoplastic material
to the bottom of a generally hollow, metallic vessel comprising the
steps:
coating the exterior surface of the bottom of said vessel to be
secured to said base with a primer comprised of a blend of
thermoplastic and thermosetting materials;
heating the bottom of said vessel to a temperature above that at
which said base material plasticizers, said primer coating being
baked onto said vessel during the heating step;
pressing said heated vessel, while still heated above said
temperature, into engagement with said base so that the heat from
said heated vessel plasticizers the surfaces of said base engaged
by said heated vessel; and
rapidly cooling said vessel, after said heated vessel and said base
have been engaged a sufficient time to produce a fusion interface
between the surface of said base and said primer coating, to
prevent the further heating of said base beyond said surface of
said base.
2. The method of claim 1, wherein said base is made of polyvinyl
chloride.
3. The method of claim 1 wherein said base is hollow and said
uniform pressure is applied by drawing a vacuum within said base
when said base is engaged with said vessel bottom and said base is
pressed into engagement with said vessel bottom by atmospheric
pressure on said base.
4. The method of claim 1 wherein a cooling medium is introduced
into vessel to cool said vessel bottom and said interface.
5. The method of claim 2 wherein said coated vessel is heated to a
temperature in the range of about 450.degree. to about 500.degree.
F. and the plastic temperature of the material of said base is in
the range of about 325.degree. to about 350.degree. F.
6. The method of claim 2 wherein said base is hollow and a vacuum
is drawn within said base when said base is engaged with said
vessel and said base is pressed into engagement with said vessel by
atmospheric pressure on said base.
7. The method of claim 2 wherein said vessel bottom is treated for
receipt of said primer prior to application of said primer
thereto.
8. The method of claim 7 wherein said treatment is sand
blasting.
9. The method of claim 1 wherein a uniform pressure is applied over
the abutting surfaces of said vessel bottom and said base.
Description
BACKGROUND OF THE INVENTION
1. Field of Invention
This invention relates to the attachment of bases to containers
and, more specifically, to the attachment of nonmetallic bases made
of, for example, polyvinyl chloride to pressure vessels, or vessels
in general.
2. Description of Prior Art
Various proposals have been made for the attachment of bases of
synthetic material, such as polyvinyl chloride, to metallic
containers. Chief among these have been the use of adhesives. Due
to base separation from the container, adhesives have not proven to
be entirely satisfactory. U.S. Pat. No. 3,165,228,issued to Milton
F. Kroesch and Willert O. Kugler, and assigned to the assignee of
this application, discloses a solution to this problem of base
attachment and this application is concerned with yet another
solution to that problem.
SUMMARY OF INVENTION
An object of this invention is to provide an improved method of
securing a synthetic attachment to a metallic container, more
specifically, the attachment of a base made of polyvinyl chloride
to metallic containers such as pressure vessels. For the
achievement of these and other objects, this invention proposes
that the area to which the particular attachment is to be secured
be primed with a primer having both thermosetting and thermoplastic
properties. The attachment is heated and heating is sufficient so
that when the primed area and attachment are in engagement surface
fusion with the attachment occurs. Heating is preferably achieved
by heating the area to be engaged by the attachment to the desired
temperature. Pressure can be applied to the contacting areas as
fusion is taking place and the area of the attachment is rapidly
cooled before excessive heat penetration of the attachment occurs.
but after the heat has been held a sufficient length of time to
achieve surface fusion.
DESCRIPTION OF DRAWINGS
FIG. 1 illustrates a base and vessel at an intermediate stage in
the process; and
FIG. 2 illustrates the base and vessel during the rapid cooling
stage of the process.
DESCRIPTION OF PREFERRED EMBODIMENT
The invention will find particular application in attaching bases
to pressure vessels and, therefore, will be discussed in that
environment but the invention has wider application.
Pressure vessel 10 includes elongated sidewalls 12 and an
ellipsoidal bottom 14. Vessel 10 is generally intended to stand
upright and this requires a support base. One form of base has been
an integral bumped-back bottom which consists of, for example, a
concave central portion with an annular supporting ridge or an
undulating-type bottom having a plurality of support feet arranged
generally in a cloverleaf design. These bases are effective in
standing the vessel upright, but they are not the most efficient
from a pressure standpoint and require a heavier gauge bottom, as
compared to the walls of the vessel, and are also more costly to
fabricate. The ellipsoidal bottom provides a most efficient
pressure configuration and allows a uniform wall thickness
throughout the vessel. A separate, attached base permits the use of
the ellipsoidal bottom. In one aspect this invention is directed to
this problem of attaching a separate base and thereby permitting
use of the ellipsoidal base. Over and above this problem, which is
peculiar to pressure vessels, many other vessels and containers
require secure attachment of a support base and one which will
remain securely attached over extended use and in environments
generally considered deteriorating to the base and a secure bond
between base and vessel. This invention also offers a solution to
those more general problems.
Base 16 is made of polyvinyl chloride (PVC) and includes an outer
skirt 18, a central semispherical web 20 and a foot 22 which
extends axially beyond web 20. Foot 22 can be either a continuous
annular ring as illustrated or a plurality of individual, radially
extending foot sections arranged in a circle.
To attach base 16 to vessel bottom 14 the vessel bottom is coated
with a primer 24. The primer can be coated on, sprayed on, hot
dipped or applied in anyone of a number of other forms of
application.
The PVC base exbibits a temperature i.e. a plastic temperature at
which the base becomes somewhat plastic an d can be made to fuse
with another element. In the case of PVC this temperature is
approximately 325.degree.-350.degree. F. After having applied the
primer, the vessel is heated above the plastic temperature. The
amount of the overheat (temperature above the plastic temperature)
will depend to a large measure on the thickness of the vessel walls
which is a major factor in the heat retention characteristic of the
vessel; that is, the thicker the vessel wall the lower the overheat
and vise versa.
This preheating of the vessel brakes the primer and prepares the
vessel for fusion to the PVC base. The heated vessel, while still
above the plastic temperature, is engaged with the base, the upper
end of the skirt engaging the primed sidewall and the web engaging
the primed vessel bottom as illustrated in FIG. 2. Heat from the
vessel initially renders the area of the base engaging the vessel
plastic and a fusion of the primer and PVC base occurs providing a
fusion interface or primer and PVC of the base. After a
predetermined time the vessel bottom and the fusion interface of
primer and base is cooled rapidly to terminate penetration of heat
into the base. The time between initial engagement and cooling is
selected to allow sufficient time for adequate fusion but not so
long as to result in excessive heat penetration which might be
detrimental to the base. This time can be determined by experience.
As stated above, the temperature to which the vessel bottom should
be heated will depend on the thickness of the bottom wall. For a
vessel having a wall thickness of approximately 0.200 inches,
heating the vessel to approximately 450.degree.-500.degree. F. has
provided satisfactory results.
During the fusion step it is desirable to apply a uniform pressure
over the abutting surfaces of the base and vessel bottom. This
pressure can be applied in any number of ways. An effective way is
illustrated for use where the base 16 is hollow. A vacuum is drawn
within the base vacuum apparatus 26 so that atmospheric pressure
presses uniformly on the outer walls of the base and results in
uniform pressure on the engaging surfaces.
cooling can be achieved effectively by pouring a cooling medium
into the vessel, for example water can be used.
A number of suitable primers can be used. A primer which has
provided particularly satisfactory results is one which is
partially thermosetting and partially thermoplastic. This type of
primer produces an effective fusion, and a primer which possesses
these characteristics of being partially thermosetting and
partially thermoplastic is available commercially from Michigan
Chrome and Chemical Co. and is identified as C1445. This primer is
a blend of thermoplastic and thermosetting resins in a mixture of
solvents.
Fusion may also be further enhanced by sand blasting the vessel
bottom prior to applying the primer and base. Sandblasting cleans
the surface and also pits the surface which results in an anchor
lock of the primer and base material with the vessel bottom.
Sandblasting also cleans the attachment area and, as an
alternative, the attachment area can be cleaned chemically.
Although but one embodiment of the present invention has been
illustrated and described, it will be apparent to those skilled in
the art that various changes and modifications may be made therein
without departing from the spirit of the invention or from the
scope of the appended claims.
* * * * *