U.S. patent number 3,592,391 [Application Number 04/794,274] was granted by the patent office on 1971-07-13 for nozzle for atomizing molten material.
This patent grant is currently assigned to Knapsack Aktiengesellschaft. Invention is credited to Ludwig Bender, Klaus Frank, Wilfried Gerhardt.
United States Patent |
3,592,391 |
Bender , et al. |
July 13, 1971 |
NOZZLE FOR ATOMIZING MOLTEN MATERIAL
Abstract
A nozzle for atomizing molten material includes annularly
arranged outlet openings for an atomizing agent with a central
aperture for the molten material. The axis of each outlet opening
is inclined in the vertical plane with respect to the vertical axis
of the central aperture at an angle .alpha.. Each outlet opening
axis is also skewed with respect to the central aperture axis so
that in the horizontal plane it deviates therefrom by the angle
.beta. . The angle .alpha. is between 20.degree. and 50.degree. and
the angle .beta. is between 10.degree. and 40.degree. with greater
angles .beta. being associated with greater angles .beta. and with
smaller angles .alpha. being associated with smaller angles
.beta..
Inventors: |
Bender; Ludwig (Bruhl near
Cologne, DT), Gerhardt; Wilfried (Knapsack near
Cologne, DT), Frank; Klaus (Hermulheim near Cologne,
DT) |
Assignee: |
Knapsack Aktiengesellschaft
(Knapsack near Cologne, DT)
|
Family
ID: |
25162188 |
Appl.
No.: |
04/794,274 |
Filed: |
January 27, 1969 |
Related U.S. Patent Documents
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Application
Number |
Filing Date |
Patent Number |
Issue Date |
|
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543156 |
Apr 18, 1966 |
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Current U.S.
Class: |
425/7; 75/338;
222/594; 239/406; 239/434.5; 222/591; 222/603; 239/424.5;
264/12 |
Current CPC
Class: |
B05B
7/1606 (20130101); B22F 9/082 (20130101) |
Current International
Class: |
B05B
7/16 (20060101); B22F 9/08 (20060101); B05b
007/10 () |
Field of
Search: |
;239/424.5X,422,424,433,434.5X,296,418,406 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: King; Lloyd L.
Parent Case Text
CROSS-REFERENCE TO RELATED APPLICATION
This application is a division of copending application Ser. No.
543,156, filed Apr. 18, 1966, now abandoned.
Claims
We claim:
1. In a ring nozzle for atomizing molten materials including a
hollow nozzle ring structure having pipe connections thereto, a
frustoconical outlet slit for discharging an atomizing agent
therefrom, a central aperture for passing the molten material
therethrough, the improvement according to which said frustoconical
outlet slit is subdivided by sloped guide plates into separate
uniform channels running around its circumference, the outlet
openings of said channels being placed in a plane common to them
perpendicular with respect to the axis of said central aperture,
said frustoconical outlet slit forming an angle .alpha. with
respect to the axis of said central aperture, said guide plates
forming an angle .beta. with respect to a plane running through the
axis of said central aperture; said angle .alpha. being between
20.degree. and 50.degree., said angle .beta. being between
10.degree. and 40.degree., smaller angles .alpha. being associated
with smaller angles .beta. and greater angles .alpha. being
associated with greater angles .beta..
2. A nozzle as set forth in claim 1 including means connected to
said central aperture for feeding molten materials which thereafter
becomes a powder substantially all of which is of grain size
smaller than 0.05 mm. therethrough, and means connected to said
outlet slit for feeding an atomizing agent therethrough.
3. A nozzle as set forth in claim 1 wherein said outlet openings
are bore shaped.
4. A nozzle as set forth in claim 1 wherein said outlet openings
are exchangeable and universally swingable orifices.
5. A nozzle as set forth in claim 1 wherein the narrowest portion
of said central aperture is 4 to 10 cm. wide.
6. A nozzle as set forth in claim 1 wherein .alpha. is from
30.degree. to 40.degree. and .beta. is from 25.degree. to
35.degree..
Description
BACKGROUND OF INVENTION
The atomization of molten materials, especially of molten metals,
has long been known. When a ring nozzle is used to achieve the
atomization, the gaseous or liquid atomizing agent is caused to
flow, generally at acute angles with respect to a stream of molten
material traveling in free fall through that nozzle; when the
nozzle is an annular slit nozzle, the atomizing agent accordingly
issues therethrough in the form of a closed cone-shaped shell. On
the other hand, a multiple-hole ring nozzle causes the individual
streams of atomizing agent to issue in the form of an interrupted
or skeletal cone-shaped shell.
In German Pat. No. 917,226 it has been proposed to introduce the
atomizing agent tangentially with respect to the horizontally
arranged nozzle ring structure, whereby an additional rotary motion
about the nozzle axis is imparted to the atomizing agent issuing
through an annular slit nozzle.
During the atomization, all reasonable means must be employed to
prevent the stream of molten material, e.g. the metal stream, from
being flung back into the region of relative subpressure produced
by the atomizing agent issuing under pressure, because the nozzle
would otherwise become clogged. As taught, e.g. in German Pat. No.
847,675, this difficulty can be obviated by allowing the atomizing
agent, atomized so as to form a cone-shaped shell, to strike the
stream of molten material falling down in vertical direction, or to
strike its vertical axis at an angle .alpha..ltoreq. 20.degree..
The disadvantage accruing from so acute an angle of cone resides in
the fact that the metal stream strikes the atomizing agent with
some delay and accordingly at a moment when the metal stream is
less hot and fluid. This results in the metal stream being torn by
the atomizing agent in customary manner into fine and smooth
particles which often have a rounded-off shape. At this relatively
delayed moment, the energy inherent to the atomizing agent is but
small. This means that fine grain fractions with a size of less
than 0.050 mm. are obtained at unsatisfactory rates, and a
determined proportion of oversize grains (>0.20 mm.) must be
screened off and melted again.
A still further apparatus for atomizing molten metals, which also
uses a multiple-hole ring nozzle, has been described in U.S. Pat.
No. 2,956,304. In contrast with German Pat. No. 847,675, the angle
.alpha. defined above, identified by the letter c in the U.S.
Patent, is greater than 20.degree., i.e. varies from 20.degree. to
60.degree., and preferably from 40.degree. to 50.degree.. The
atomizing agent is caused to issue in the form of rather flat
streams which may strike the vertical axis of the metal stream at
an angle varying between 0.degree. and 90.degree. and perpendicular
to the angle c (=.alpha.). The atomizing agent streams or more
accurately their vertical planes may finally diverge from the
vertical axis at an angle d (=.beta.). Nothing having been
disclosed as regards the size angle d (=.beta.) may have and the
interdependence of the three angles, the expert cannot successfully
reduce to practice the teachings disclosed therein.
SUMMARY OF INVENTION
The present invention relates to an apparatus for atomizing molten
materials by means of an atomizing agent, wherein a stream of
molten material is allowed to travel in free fall through the
center aperture of a ring nozzle, and the atomizing agent is forced
to travel under pressure through guiding channels, arranged
concentrically about the said center aperture, and to issue in the
form of guide streams producing, about the said stream of molten
material, an inversed shell (more accurately a frustoconical-shaped
shell), whose generatrixes include with the vertical axis of the
molten material stream an angle .alpha., and wherein each
particular guiding stream on that frustoconical shell diverges from
that vertical axis at an angle .beta., which comprises adjusting or
selecting the angle .alpha. to vary from >20.degree. to
50.degree., preferably from 30.degree. to 40.degree., and adjusting
or selecting the angle .beta. to vary from 10.degree. to
40.degree., preferably from 25.degree. to 35.degree., smaller
angles .alpha. being associated to smaller angles .beta., and
greater angles .alpha. being associated to greater angles .beta..
The atomizing agents include gases, steam or water. They are
generally sprayed under a guage pressure of 1 to 20, preferably 3.5
to 13 atmospheres.
The present invention relates to an improvement in or modification
of a conventional ring nozzle for carrying out the above
atomization which comprises, in horizontal arrangement, a
hollow-nozzle ring structure which has associated pipe connections
and, in its lower portion, is formed with nozzle-type openings
arranged in annular fashion for the atomizing agent, with the
center axes of the said outlet openings forming, in projection,
about the vertical axis of the center aperture of the ring nozzle,
an inversed frustoconical shell axially symmetrical thereto, whose
generatrixes include with the said vertical axis an angle .alpha.,
and the imaginary vertical plane lying on each of the said
projected center axes diverging from the said vertical axis at an
angle .beta.. This type of a ring nozzle, known as such, is more
especially characterized in that the angle .alpha. varies between
> 20.degree. and 50.degree., preferably 30.degree. and
40.degree., and the angle .beta. varies between 10.degree. and
40.degree., preferably 25.degree. and 35.degree., smaller angles
.alpha. being associated to smaller angles .beta., and greater
angles .alpha. being associated to greater angles .beta..
In accordance with a further feature of the present invention, the
nozzle-type outlet openings are bore-shaped, or slit-shaped, the
individual slits being separated from each other by means of baffle
plates, or are nozzle orifices which are exchangeable and
universally swingable. At its narrowest region, the center aperture
of the ring nozzle may be 4 to 10 cm. wide.
In a multiple-hole ring nozzle, the angles .alpha. and .beta. are
determined by the direction of the single-bore channels in the
nozzle body. On the other hand, in an annular slit nozzle,
subdivided by means of baffle plates, the angle is chiefly
determined by the position of those baffle plates. The function
assigned to angle .beta. is to prevent the atomizing agent streams
from forming a common point of intersection lying on the vertical
axis of the melt stream, and to enable them instead to form an
envelope circle about the said melt stream.
The whole atomization apparatus including melting furnace, pipes
for supplying the atomizing agent, water tank for receiving and
chilling of the atomized metal particles can be designed in
customary manner. The single-outlet openings for the atomizing
agent, which are disposed symmetrically on the nozzle ring, should
comprise at least three, but no more than 100, and generally 40 to
60 openings. It is advantageous to use not less than about eight to
12 outlet openings because a pyramid having a tri- or octahedral
base tends otherwise to be formed instead of an inversed
frustoconical shell by the atomizing agent streams. Obviously the
fewer the number of openings, the more skeletal the shell
becomes.
THE DRAWINGS
FIG. 1 is a schematic illustration of an apparatus embodying one
form of this invention in cross-sectional elevation; and
FIG. 2 is a schematic top plan view of the apparatus shown in FIG.
1.
DETAILED DESCRIPTION
FIG. 1 is an elevation view of a ring nozzle comprising an annular
hollow chamber 1, pipe connections 2 and nozzlelike outlet openings
3 for the atomizing agent. The generatrixes 4 of the inversed
frustocone-shaped shell, formed by the atomizing agent and
surrounding in axially symmetrical relationship the vertical axis 5
of the ring nozzle center aperture 6, and the said vertical axis 5
include the angle .alpha.. In other words as is apparent from FIG.
1 the angle .alpha. is the angle formed in the vertical plane, by
the atomizing stream with respect to the molten material passing
through aperture 6. Thus this angle is defined by the vertical axis
5 and by the axis of the atomizing stream which lies on the
generatrix 4. As is also apparent from FIG. 1 the outlets of the
atomizing agent passageways are coplanar.
FIG. 2 is a schematic top plan view which clearly shows how each
atomizing stream is skewed in the horizontal plane by the angle
.beta. whereby the atomizing streams do not converge upon a common
point but rather form a frustoconical-like shell having its apex at
the circle 10. As the streams continue to fall there would of
course be another mirrorlike frustoconical shell formed which would
have the common apex 10. As is likewise apparent from FIG. 2 the
angle .beta. is defined by the axis 4 of the stream with respect to
an imaginary vertical plane 8 extending through vertical axis 5 and
the point of discharge of the atomizing agent.
The ring nozzle in accordance with the present invention enables
the adjustment or selection of a large angle .alpha. without any
risk of the metal stream, which is about 1.0 to 1.6 cm. thick,
being flung back. This means for the atomizing agent that it
strikes the very hot and fluid metal stream relatively soon and
practically with undiminished power which thereby undergoes
obligatory atomization into fine metal powder including no more
than slight proportions of oversize grains.
The present ring nozzle can be used for atomizing the most varied
substances, e.g. slag, fertilizer salts, plastic materials and
particularly metals and their alloys. The atomizing agents include
water and steam and in addition thereto nitrogen, argon or air. The
fact that oversize grains are always obtained in but minor
proportions is especially advantageous. The individual oversize
grain is more compact owing to the strong suction effect or
subpressure produced by the nozzle and owing to some vacuum
degasification taking place. This suction effect thus produces what
might be considered a preatomization wherein the subpressure
prevailing between the atomizing agent shell and the falling molten
material attracts the molten material to break it up into a
plurality of more or less coarse melt particles which are later
atomized into fine particles by direct contact between the
atomizing agent and the particles. The inclined position of the
baffle or guide plates 14 of FIG. 1, or bores ensures that each
individual stream of the atomizing agent issues through a bevelled
nozzle channel, which means that the ring nozzle is operated
outside critical pressure conditions as a Laval nozzle. Under
critical pressure conditions, sonic speed is just produced in the
narrowest cross-sectional area of the nozzle. Under overcritical
pressure conditions, a speed higher than sonic can only be produced
in Laval type or bevelled nozzles.
The following Examples illustrate the invention:
EXAMPLE 1
(Comparative Example)
Atomization of liquid iron by means of a ring nozzle in which angle
.alpha. was 22.5.degree. and angle .beta. was 0.degree..
Attempts were made to atomize the liquid iron by means of steam
under a gauge pressure of 2 atmospheres. This proved impossible as
the liquid metal stream was flung back. Further increase of the
steam pressure resulted in a portion of the steam issuing even
through the neck of the nozzle.
EXAMPLE 2
(Comparative Example)
Atomization of liquid ferrosilicon (15 percent by weight Si) by
means of a ring nozzle in which angle .alpha. was 22.5.degree. and
angle .beta. was 5.degree..
The casting temperature was 1,430.degree. C., and the nozzle was
charged with steam under a gauge pressure of 3.5 atmospheres.
Screen analysis resulted in the following grain fractions:
At a gauge pressure above 3.5 atmospheres, the nozzle became
clogged by liquid metal flung back.
EXAMPLE 3
Atomization of liquid ferromanganese (30 percent by weight Mn) by
means of a ring nozzle in which angle .alpha. was 22.5.degree. and
angle .beta. was 15.degree..
The melt had a temperature of 1,390.degree. C., and the nozzle was
charged with steam under a gauge pressure of 5.5 atmospheres.
Screen analysis resulted in the following grain fractions:
At a steam gauge pressure of more than 6 atmospheres, metal was
again found to be flung back.
EXAMPLE 4
Atomization of ferromanganese (75 percent by weight Mn) by means of
a ring nozzle in which angle .alpha. was 30.degree. and angle
.beta. was 35.degree..
The casting temperature was 1,380.degree. C., and the nozzle was
charged with steam under a gauge pressure of 3.5 atmospheres.
Screen analysis of the powder resulted in the following grain
fractions:
EXAMPLE 5
Atomization of liquid ferrosilicon (15 percent by weight Si) by
means of a ring nozzle in which angle .alpha. was 40.degree. and
angle .beta. was 35.degree..
The casting temperature was 1,440.degree. C., and the nozzle was
charged with steam under a gauge pressure of 7.5 atmospheres.
Screen analysis resulted in the following grain fractions:
EXAMPLE 6
The atomization was carried out by means of a ring nozzle of the
type described in example 5. The casting temperature was
1,460.degree. C.
Ferrosilicon (15 percent by weight Si) was atomized by means of
that nozzle which had been charged with steam to serve as the
atomizing agent under a gauge pressure of 13 atmospheres. Screen
analysis of the powder obtained resulted in the following grain
fractions:
EXAMPLE 7
The atomization was carried out by means of a ring nozzle of the
type described in Example 5. The casting temperature was
1,460.degree. C.
Ferrosilicon (75 percent by weight Si) was atomized by means of
steam under a gauge pressure of 12 atmospheres. Screen analysis of
the powder obtained resulted in the following grain fractions:
* * * * *