U.S. patent number 3,577,635 [Application Number 04/771,966] was granted by the patent office on 1971-05-04 for method for isostatic compression, such as the manufacture of powder bodies.
This patent grant is currently assigned to Allmanna Svenska Elektriska Aktiebolaget. Invention is credited to Carl Bergman, Harry Claesson.
United States Patent |
3,577,635 |
Bergman , et al. |
May 4, 1971 |
METHOD FOR ISOSTATIC COMPRESSION, SUCH AS THE MANUFACTURE OF POWDER
BODIES
Abstract
A body to be compressed is inserted within a flexible container
containing a compression medium compatible with the body and the
container is then placed within an outer compression chamber
containing another compression medium compatible with the container
and chamber.
Inventors: |
Bergman; Carl (Vasteras,
SW), Claesson; Harry (Vasteras, SW) |
Assignee: |
Allmanna Svenska Elektriska
Aktiebolaget (Vasteras, SW)
|
Family
ID: |
20300490 |
Appl.
No.: |
04/771,966 |
Filed: |
October 30, 1968 |
Foreign Application Priority Data
|
|
|
|
|
Nov 8, 1967 [SW] |
|
|
15322/1967 |
|
Current U.S.
Class: |
29/615; 100/211;
264/570; 419/42; 419/68; 425/78; 425/405.2; 264/313; 419/2; 419/49;
425/77; 425/86 |
Current CPC
Class: |
B22F
3/04 (20130101); H05B 3/52 (20130101); H05B
7/08 (20130101); Y10T 29/49091 (20150115) |
Current International
Class: |
B22F
3/04 (20060101); H05B 7/00 (20060101); H05B
7/08 (20060101); H05B 3/42 (20060101); H05B
3/52 (20060101); H01c 015/04 (); H01c 017/00 () |
Field of
Search: |
;18/5 (I)/ ;29/615
;204/88,109,111 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Campbell; John F.
Assistant Examiner: Shore; Ronald J.
Claims
We claim:
1. Method of subjecting bodies to high pressure, preferably the
manufacture of powder bodies, such as hard metal products,
electrical heating elements comprising an electric conductor
surrounded by a body of compressed power material and possibly a
surrounding, tubular casing, and welding and furnace electrodes,
said method comprising isostatic compression, characterized in that
objects to be compressed are placed in a hollow container with at
least one elastomeric or displaceable wall or bottom, which
container is also filled with liquid pressure medium and is sealed
and placed in a pressure chamber for hydraulic or pneumatic
pressure medium, after which the pressure in the chamber is
increased and the container compressed so that the container
including liquid pressure medium and objects is also compressed and
thus the objects are isostatically compressed.
2. Method of manufacturing powder bodies according to claim 1,
characterized in that before compression the powder body is placed
in a thin casing of plastic, metal foil or the like, substantially
only to keep the powder material together before the
compression.
3. Method of manufacturing electrical heating elements according to
claim 1, characterized in that a skeleton tube sealed at the ends
and surrounding the powder body is used as casing.
4. Method of manufacturing electrical heating elements according to
claim 1, characterized in that the container is filled with water
and the chamber, outside the container, is filled with hydraulic
oil before compressing.
Description
BACKGROUND OF THE INVENTION
The present invention relates, among other things, to a method of
subjecting bodies or liquid to high pressure, such as in the
manufacture of powder bodies, for example hard metal products,
electrical heating elements comprising an electrical conductor
surrounded by a body of compressed powder material and possibly a
surrounding, tubular casing, welding or furnace electrodes,
etc.
In a known method of manufacturing such bodies, for example,
heating elements for washing machines, etc., a central conductor is
packed into a surrounding powder, in this case of insulating and
heat-conducting type, possibly surrounded by a tube or other casing
and the body is pressed in a suitably shaped tool or between
rollers having a certain groove shape so that the powder (and
casing) is compressed around the central conductor. This method has
certain disadvantages. A tool of a certain shape is required and it
is difficult to avoid cracks, irregularities and air pockets in the
finished product especially if it is afterwards bent or shaped to a
nonlinear shape such as zigzag or spiral which is usual for heating
elements. The difficulty connected with the requirement of a
special shape is also apparent with hard metal bodies (usually
powder of hard material particles such as tungsten carbide and a
binding metal such as nickel or cobalt), welding electrodes, etc.
and the possibility has therefore been considered of manufacturing
such bodies by other methods.
One such known method consists of placing one or more powder
bodies, for example, of the above mentioned type, in a high
pressure chamber for gaseous or hydraulic pressure medium and
producing a high pressure in the chamber so that the bodies are
compressed on all sides and the powder becomes even and relatively
free from pockets of air, etc. By means of such isostatic
compression it is also possible to manufacture bodies having a more
complicated shape, such as curved hard metal blades, heating
elements in spiral shape or having some other nonlinear shape,
etc., and the curing is preferably carried out before compacting.
Sintering may take place either before and/or afterwards. This
method provides high quality products, high production speed and
good accuracy of dimensions even without subsequent calibration.
The cost of manufacturing the bodies is low.
One disadvantage which sometimes arises with this isostatic
compression is that for the pressure medium in the pressure chamber
(pressure container) it is necessary to use a pressure medium which
is suitable for the pressure chamber, for example, noncorroding,
but which may cause trouble in the compressed body. A pressure
medium suitable for the compressed body, on the other hand, may be
unsuitable for the pressure container. As an example may be
mentioned that hydraulic oil in a finished hard metal body may
decrease its usefulness. Hydraulic oil in a heating element, due to
the nonconducting characteristic of the oil, makes the element
difficult to test for insulation and remaining oil may cause an
unpleasant odor when the heating element is used, and the oil may
be difficult to remove. Disadvantages with similarly manufactured
electrodes could also be shown.
With, for example, isostatic compression of hard metal bodies it is
preferred to use a pressure medium of water-soluble type, such as
glycerine and ethylene glycol, and in the manufacture of heating
elements, water. Such pressure media, however, may cause corrosion
and the like in the walls of a pressure chamber which in turn may
cause rupture or other damages in the high pressure apparatus. It
can thus be said that it is often difficult to find a pressure
medium which is suitable both for the high pressure container and
for the compressed object.
STATEMENT OF THE INVENTION
The invention provides a solution of these and other similar
problems and is characterized in that objects to be compressed are
placed in a container having at least one elastomeric or
displaceable wall or bottom, which container is also filled with
pressure medium, sealed and placed in a pressure chamber for
hydraulic or pneumatic pressure medium, after which the pressure in
the chamber is increased and the container compressed so that the
object within is also compressed. The advantages of isostatic
compression are thus utilized to the full and at the same time
large scale production is effected. The pressure medium operating
on the object can be selected taking the object into consideration
and that in the out pressure chamber can be selected with a view to
the technical conditions required in the chamber. Thus, expensive
molding tools are avoided and the shape or length of the object is
irrelevant.
The invention also relates to a means for performing this method.
The means is characterized in that it comprises a container having
at least one elastomeric or displaceable wall or bottom for powder
bodies or the like and for pressure medium, which container can be
sealed and immersed in a pressure chamber to compress the container
and bodies placed in this, by means of a pressure medium in the
chamber. Such a means operates effectively as an inner pressure
vessel. The elastic wall, etc. rapidly alters shape when pressure
is effected in the outer chamber and the inner container is
compressed until pressure equality is reached in container and
chamber. The bodies in the container will be isostatically
compressed with the same pressure as occurs in the chamber without
coming into contact with the outer pressure medium. Suitably, the
container is provided with a bottom in the form of a perforated
wall, a grid or net which is surrounded by the elastic wall.
Instead of an elastomeric wall (bottom) in the form of an
elastomeric membrane, the wall may be displaceable in the form of a
piston, movable in a cylindrical space. Regarding the minimum
volume for the compressible parts of the container, see below.
DESCRIPTION OF THE DRAWINGS
The invention is further exemplified in the accompanying drawings
where FIG. 1 shows a container in a high pressure chamber, which
container is provided with a wall (bottom) in the form of an
elastomeric membrane. FIGS. 2 and 3 show alternative
embodiments.
DESCRIPTION OF THE PREFERRED EMBODIMENTS
FIG. 1 shows a container 12, which by means of a cross member or
other lifting device, can be lowered into a pressure chamber 11,
said container having thin metal walls, such as thin steel. The
container 12 may of course be placed in the chamber before being
filled. In certain cases several containers may be placed in the
same pressure chamber. A powder body, or several powder bodies,
here for example a spiral heating element billet 13, is placed in
the container 12 and then the container filled with suitable
pressure medium, such as water and closed with the lid 14.
The powder body or bodies may consist of hard metal bodies,
consisting of hard material grains (tungsten carbide, etc.) and
binder (Co or Ni), possibly enclosed in a thin casing of plastic or
the like which is removed after compression and before subsequent
treatment such as turning. The powder in the hard metal bodies must
be compressed to become sufficiently dense and strong so that it
can be subsequently machined, for example in a lathe, before being
sintered after which further machining is extremely difficult. It
is desirable to prevent substances penetrating into the powder
which might deteriorate the quality of the bodies, and this is done
by using a pressure medium which is harmless when in direct contact
with the body and by enclosing the body in a casing during the
compression. There is a risk, however, that a small amount of
pressure medium will penetrate into the powder body when the casing
is removed and for this reason the composition of the pressure
medium is also important. A suitable pressure medium is glycerine,
possibly with the addition of ethylene glycol.
The powder body 13 may also comprise heating elements or
thermoelements having straight or curved shape, consisting of one
or more central electrical conductors surrounded by a powder of
electrically insulating, but heat-conducting type, such as aluminum
oxide or quartz. A thin plastic casing, later removable, or a
sheathing tube to hold the powder together, sealed at the ends
before the compression, may be placed around the body.
In order to obtain satisfactory strength, heat-conductivity and
other desired properties, the powder in these bodies must be
strongly compressed and this should be done after the body has been
bent to its final shape. As can be seen, the heating element 13 in
the case shown is meander formed before the compression. The method
can also be used for welding and furnace electrodes, machine
components in powder form, hotplates, powder bodies consisting of
several layers, etc. A suitable pressure medium of the manufacture
of heating elements (with or without casing) is water which is
electrically conducting and thus permits the usual insulation test
in the finished product, but which evaporates and disappears when
the element is used.
At the bottom of the container 12 a perforated plate 15, net or
grid is arranged to permit the passage of pressure medium and below
this an elastomeric or flexible membrane or sack 16 is sealingly
arranged. The membrane encloses a compression space which must be
at least as large as the decrease in total space which takes place
in the container 12 when full pressure has been reached in the
outer chamber, that is the space at 16 (sack space) must at least
correspond to the compression of the total space in the container
12. The wall may consist of a relatively thin-walled, cylindrical
tube. Around the membrane or sack 16 is arranged a supporting space
17 axially limited by a wall or support to carry the container and
protect the sack 16. The support space 17 may be open at the bottom
or limited by a perforated plate 18, net or grid to permit the
passage of pressure medium from the outer pressure chamber 19 to
the supporting space 17.
The container 12 with supporting space 17 and sack 16 is lowered
into an outer pressure chamber for gaseous or hydraulic pressure
medium, such as hydraulic oil which is water repellent and
noncorrosive. The container 12 may be positioned or suspended in
the chamber 11 and the latter pressurized to 500--40,000 atm., for
example, 6000 atm. by means of a conventional pump and/or press
means 20.
Instead of a sack or membrane at the bottom, other walls of the
container, or all of these, may be flexible so that they can be
compressed until pressure equilibrium is achieved between the outer
and inner pressure spaces. It is also possible, as shown in FIG. 2,
to replace the membrane by a piston movable in a cylindrical space
21 sealing the bottom of the container 12. The shape of the
container is in principle immaterial.
When the container 12 has been filled with the object and pressure
medium, in this case heating element billet and water, and sealed
at 14 after air has been removed, it is lowered into the pressure
chamber 11 after which the pressure in the outer chamber is raised
to, for example, 6000 atm., and this pressure also operates on the
container 12 and its sack 16. The container 12 is compressed and
the sack space decreases so that pressure equilibrium is achieved
between the outer and inner pressure spaces. The container may
possibly also be heated to a certain extent. The bodies 13 are
compressed isostatically by the inner pressure and when the
pressure ceases in the chamber 11 the sack space expands again. As
an example of the degree of compression, it may be mentioned that
at a pressure of 6000 atm. the container (space and sack space) is
compressed to 84 percent of its original volume. The sack space
must therefore be at least 16 percent of the inner total
volume.
After the pressure medium has been poured into the container 12 the
total volume assumes its greatest value and during the isostatic
compressure it assumes its minimum volume. The object in the
container is isostatically compressed and becomes uniformly and
homogeneously compressed.
FIG. 3 shows a container 12 with a completely closed bottom 22
through which at least one tube 23 communicates with the sack space
and the container space. As can be seen, the sack 16 may also be
attached to some other part of the support space 17, for example,
around the perforated plate 18. The bottom 22 may also be provided
with channels at its periphery.
The method according to the above may also be used for the
manufacture of plastic bodies in which case a billet of base
material and curing agent is subjected to isostatic compression,
possibly also heat and is thus cured. Liquids may also be subjected
to isostatic pressure in order to undergo certain alterations. In
conclusion, the above method relates to the separation of two
different pressure media for the reasons given above.
The method and means according to the above can be varied in many
ways within the scope of the following claims.
* * * * *