U.S. patent number 3,575,055 [Application Number 04/866,906] was granted by the patent office on 1971-04-13 for apparatus for automatically sampling solids.
This patent grant is currently assigned to Continental Carbon Company. Invention is credited to Audis H. Thornton, Jr..
United States Patent |
3,575,055 |
Thornton, Jr. |
April 13, 1971 |
**Please see images for:
( Certificate of Correction ) ** |
APPARATUS FOR AUTOMATICALLY SAMPLING SOLIDS
Abstract
A sampling apparatus for automatically sampling solids at
regulated time intervals from a conduit carrying said solids
comprising a base member affixed over an opening in the conduit and
having a sampling tube extending through the member and the conduit
and into the path of guide vanes mounted on said base member. The
sampling tube has a butterfly valve to form a sampling chamber in
the upper end and the lower end communicates into a sample
accumulator. The apparatus has a pneumatic system with a line to
purge the sample chamber before the sampling operation and lines to
activate a power cylinder to operate the butterfly valve, and this
system is controlled by an electrical system for timing and
sequential activation of the components to obtain and transfer
samples to the accumulator.
Inventors: |
Thornton, Jr.; Audis H. (Lake
Charles, LA) |
Assignee: |
Continental Carbon Company
(Houston, TX)
|
Family
ID: |
25348693 |
Appl.
No.: |
04/866,906 |
Filed: |
October 16, 1969 |
Current U.S.
Class: |
73/863.43;
73/863.57 |
Current CPC
Class: |
G01N
1/20 (20130101) |
Current International
Class: |
G01N
1/20 (20060101); G01n 001/20 () |
Field of
Search: |
;73/422,422 (TC)/ |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Prince; Louis R.
Assistant Examiner: Yasich; Daniel M.
Claims
I claim:
1. An apparatus for automatically sampling solids from a gravity
conveyor conduit which comprises:
a base member adapted to be affixed in an opening of said conveyor
conduit, said member having an aperture;
a plurality of guide vanes affixed to said base member above said
aperture on the side of said base member communicating with the
interior of said conveyor conduit;
a sampler tube having a first end affixed through the aperture of
said base member with valve means forming a sample chamber in the
upstream end adapted to communicate through said tube and the
second end of said tube extending into a sample accumulator;
a sample chamber purge means connected to said chamber;
a power means affixed to said base member on the side exterior of
said conveyor conduit and connected to the valve means in said
sampler tube;
an activation means communicating with said power means; and
a control means for said sample chamber purge means and said
activation means.
2. The apparatus of claim 1 wherein the first end of said sampler
tube is cut at an angle to have a substantially horizontal cross
section with the shortest side of said tube being mounted flush
with said base member.
3. The apparatus as set forth in claim 1 wherein the sampler tube
valve means is a butterfly valve.
4. The apparatus of claim 1 wherein the power means is a pneumatic
power cylinder affixed to said base member with the piston thereof
having a rod connected to actuate the valve in said sampler
tube.
5. The apparatus of claim 1 wherein the sample chamber purge means
is a pneumatic line extending from a pressurized gas source through
the wall of the said sampler tube into the lower portion thereof
with said pneumatic line having a pressure regulator upstream of a
valve controlled by a single-stage solenoid means.
6. The apparatus of claim 5 wherein the activation means is a
pneumatic line extending from a compressed gas source through a
pressure regulator and valve means to said power means.
7. The apparatus of claim 6 wherein the control means are
electrical lines extending from a timing means to operation means
for the valve means of said activation means and the valve of said
sample chamber purge means.
8. The apparatus of claim 7 wherein said operation means are
solenoids.
9. The apparatus of claim 7 wherein the valve means of said
activation means is a two-way valve and the operation means thereof
is a double-stage solenoid.
10. The apparatus of claim 7 wherein the timing means is an
electronic timer preset to sequentially operate to transmit
electrical signals to said control means.
Description
BACKGROUND OF THE INVENTION
1. Field of the Invention
The present invention relates to the automatic sampling of solids,
such as pelletized carbon black product, as the same is being
passed through a conveyor conduit at some stage in the intermediate
handling or processing of the solid particles. The apparatus is
assembled and installed in such a manner as to provide the
automatic withdrawal of small sample portions at regular time
intervals in order that a composite sample of the solids stream
being moved through the conveyor can be obtained.
The apparatus is particularly applicable to the manufacture of
materials in continuous processes wherein there are at various
stages solid particles to be tested for quality. A particularly
useful application of the present apparatus is in the accumulation
of samples of pelletized carbon black as the same is being passed
from the final processing stage to storage, said black having been
prepared as a suspension of carbon particles in a gaseous effluent
with the particles being separated, pelletized and dried before the
transfer to storage.
2. Description of the Prior Art
The body of prior art in the field of sampling apparatus is
substantial. The sampling of a stream of moving solids is basically
accomplished by manually inserting a container into the stream in
order to obtain a "grab" sample; by inserting a probe in order to
withdraw a portion of the material in a manner not dissimilar to
the "grab" sample technique; and withdrawing a portion of the
material flowing through a conduit by the application of a vacuum
force to the materials in order to obtain the sample.
SUMMARY OF THE INVENTION
The invention of this present application comprises an apparatus
for automatically sampling solids from a gravity conveyor conduit,
having a base member affixed within an opening in the wall of the
conveyor conduit. The base member has an aperture through which a
sampler tube is extended and affixed in alignment with a plurality
of guide vanes affixed to the base member. A valve is set within
the upper portion of the sampler tube in order to form a sample
chamber in the upstream end of the tube and the downstream end of
the tube extends into a sample accumulator or a tank. A power means
is affixed to the base member and connected to the valve in order
to operate the same within the sampler tube and there is a purge
means connected to the sample chamber. An activation means, such as
a pneumatic system, operates to cause the power means to function
and the activation means is in turn subject to a control means,
such as an electrical system tied in with a timing means in order
to obtain the requisite sequential action for automatic
sampling.
BRIEF DESCRIPTION OF THE DRAWING
The annexed drawing sets forth in detail illustrative views of the
invention wherein like reference numerals designate like parts as
follows:
FIG. 1 represents a side elevation of a sampling apparatus of the
present invention partially in section and including a schematic
diagram of the control and activation means;
FIG. 2 represents a view of the apparatus taken along line 2-2 of
FIG. 1; and
FIG. 3 represents a view of the apparatus taken along line 3-3 of
FIG. 1.
DESCRIPTION OF PREFERRED EMBODIMENT
The present invention may be readily understood from the following
detailed description and by reference to the drawing, particularly
FIG. 1. The apparatus of the present invention is installed in a
conveyor conduit 10 wherein feed of the solid particles is by
gravity fall, said apparatus being inserted in the opening 12 of
the downfall conduit.
The base member 14 of the automatic sampling apparatus has at least
two guide vanes 16 affixed to the side of the member which extends
into the conduit. The better view of the alignment of the vanes 16
is set forth in FIG. 3. These vanes are illustrated to be two in
number; however, it is understood that the nature of the conduit
may require that additional vanes be installed in order that the
most representative sample flow of product particles is diverted
across the aperture 18 of the base member 14.
Extending through the aperture 18 is a sampling tube 20 which is
preferably cut at such an angle so that the cross section of the
upper end of the tube is substantially horizontal and the shortest
side of the tube abuts and is affixed against the base member 14.
The sampling tube has in the upstream end a valve such as butterfly
22 which thus forms a sample chamber 24 in the upstream end of said
tube when the valve is in the closed position. At the backside of
valve 22, the requisite pivot bar, as illustrated in FIG. 2, is
securely affixed to said valve and in communication with the
requisite connection means described more completely hereinbelow.
The pivot bar 25 extends through the sidewalls of sampling tube 20
and is sealably affixed therein by packing gland 26.
The base member 14 has affixed at one end on the outside, or side
exterior of said conveyor conduit, a support member 28 adapted to
receive and retain pneumatic power cylinder 30 by bolt means 32.
The power cylinder includes a piston rod 34 connected to the piston
within said cylinder and the same is enclosed by piston seal 36.
The piston rod 34 at its end has a bracket member 38 attached to
toggle 40 by connection means 42 and said toggle is likewise
affixed by connection means 44 to pivot bar 25 described
hereinabove.
This unit comprises the power means which is affixed to the
backside of base member 10 and is utilized to cause withdrawal of
the sample from the conduit through the sampling tube.
The apparatus includes an activation means for the above power
means comprising the cylinder, piston, piston rod and connections,
particularly pneumatic connections 46 extending cylinder the upper
portion and the lower portion of pneumatic cylinder 30 and these
pneumatic connections 46 are in turn connected with flexible
conduits 48. The flexible pneumatic conduits 48 are attached to
pneumatic connections 50 tied in respectively to the pneumatic
lines 66 and 68 described below.
The activation means comprises a main gas line 52 connected to a
source of compressed gas (not shown) and the main gas line 52 is
split to a pneumatic power cylinder control line 54 having a
pressure regulator 56 inserted in the line upstream of a two-way
valve 58 which is connected to a pneumatic cylinder line 66
extending to the pneumatic connection 50 communicating with the
upper end of power cylinder 30 and a second pneumatic cylinder line
68 communicating with pneumatic connection 50 and the lower end of
power cylinder 30.
The apparatus includes a sample chamber purge means which is a
pneumatic line 60, also connected to the main gas line 52, and
having a pressure regulator 62 interposed in the line 60 ahead of a
valve 64 which communicates downstream through pneumatic line 70.
Pneumatic line 70 extends through pneumatic connection 72 extending
through opening 74 of the sampling tube 20 into the bottom portion
of sample chamber 24.
The control means for the apparatus of the subject invention
comprises a timing means 76, such as an electronic timer, which is
connected by electrical line 78 to a double-stage solenoid means 80
and by electrical line 82 to a single-stage solenoid means 84. The
solenoid means 80 is a double-stage solenoid capable of operating
the two-way valve 58 interposed between pneumatic lines 56 and
pneumatic lines 66 and 68. The solenoid 84 is connected to the
single valve 64 interposed between pneumatic lines 60 and 70 as
part of the sample chamber purge system.
The base member 14 is inserted through opening 12 of the solid
products conveyor conduit 10 and held in place by welds 86.
The sample withdrawn from the conduit 10 is passed through the tube
20 and into an appropriate sample accumulator 88. Referring to FIG.
2, the apparatus illustrated is previously referred to in the above
description and provides detail as to the assembly and linkage
required for the power means of power cylinder 30 and the valve 22.
The counterpart FIG. 3 is the view of appurtenances to the base
member 14 from the interior of conduit 10 illustrating the vanes
16, and particularly shows the butterfly valve 22 in an open
position within tube 20 extending through aperture 18 of the base
member.
The materials used in conjunction with the subject apparatus should
be capable of withstanding any erosive and corrosive
characteristics of the solid particles contacting the same in order
to provide essentially a self-cleaning and corrosion resistant
apparatus. In actual use in a carbon black manufacturing facility
it has been determined that the apparatus can be suitably installed
in a downfall conduit having an angle of approximately 30.degree.
from vertical and in this application it was necessary to utilize
stainless steel pipe for tube 20, the same having an outside
diameter of 2 inches with the butterfly valve 22 being affixed
downstream of the upper end of the pipe by a distance sufficient to
provide a sample chamber 24 capable of holding approximately 150
cubic centimeters of pelletized carbon black. The pressurized gas
in the carbon black system was air and the same was from a source
at 80 to 90 p.s.i. pressure, with the pressure regulators capable
of reducing the same to 25 p.s.i. pressure in regulator 56 of the
activation means for the power cylinder 30, while the regulator 62
in line 60 was set to operate at the pressure of 80 to 90 p.s.i. in
order to appropriately purge the sample chamber 24. The materials
actually contacted by the product, i.e., the base member 14, vane
16, sample tube 20 and components included therein, together with
the sample accumulator 88, are desirably of such material as to
resist deterioration upon contact with the solids, i.e., stainless
steel in the case of carbon black.
The installation of the present sampling apparatus in a conveyor
conduit is particularly adapted to a gravity fall conduit and the
same must be one in which the angle of the conduit is not such as
to cause bridging. The apparatus will function adequately in a
vertical conduit with the installation of the appropriate guide
vanes; however, it is desirable for the conduit to have an
inclination in the range 45.degree. to 85.degree. from horizontal,
preferably 60.degree. to 70.degree. horizontal.
The operation of the apparatus of the present invention through one
cycle is that the timer 76 transmits a control impulse to solenoid
84 which opens valve 64 for a limited period of time in the order
of 1 second to allow a jet of compressed gas to be transmitted into
the sample chamber 24 to blow any accumulated solids therefrom, and
the solenoid is then activated to close valve 64 and cut off the
air pressure. In a limited time, approximately 1 minute, the timer
76 transmits a control impulse to solenoid 80 which activates valve
58 to open and pass a jet of compressed gas into power cylinder 30
for movement of the piston and piston rod 34 to open the valve 22
and allow the sample to be recovered from sample chamber 24 through
the tube 20 into the sample accumulator 88. After a short time,
approximately 1 second, a second impulse is transmitted from the
timer 76 to the solenoid 80 to activate valve 58 and divert the
pneumatic gas stream to cylinder 30 to close the butterfly valve 22
thus completing the cycle.
This cyclical process is repeated at sufficient intervals to
provide the requisite number of samples required for the period. In
the above carbon black manufacturing situation the cyclical process
was repeated every 16 minutes to provide approximately 85 samples
in a 24 hour period, thus having a cumulative and composite sample
of approximately 5 gallons of solid product for recovery and
analysis on a daily basis.
Having thus described and disclosed my invention what is claimed is
set forth below.
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