U.S. patent number 3,573,460 [Application Number 04/578,884] was granted by the patent office on 1971-04-06 for ion chamber detector for submicron particles.
This patent grant is currently assigned to General Electric Company. Invention is credited to George F. Skala.
United States Patent |
3,573,460 |
Skala |
April 6, 1971 |
**Please see images for:
( Certificate of Correction ) ** |
ION CHAMBER DETECTOR FOR SUBMICRON PARTICLES
Abstract
This invention relates to gas analyzing apparatus and more
particularly to an improved ion chamber apparatus for detecting the
presence of submicron size particles entrained in a gaseous
carrier.
Inventors: |
Skala; George F. (Scotia,
NY) |
Assignee: |
General Electric Company
(N/A)
|
Family
ID: |
24314704 |
Appl.
No.: |
04/578,884 |
Filed: |
September 12, 1966 |
Current U.S.
Class: |
250/381; 250/383;
313/7; 313/54; 324/469; 436/7 |
Current CPC
Class: |
G01N
27/66 (20130101); G08B 17/113 (20130101); H01J
41/08 (20130101) |
Current International
Class: |
H01J
41/08 (20060101); G01N 27/64 (20060101); G01N
27/66 (20060101); H01J 41/00 (20060101); G08B
17/113 (20060101); G08B 17/10 (20060101); G01n
005/00 () |
Field of
Search: |
;250/86.6 (FT)/
;250/43.5 (R)/ ;324/33 ;313/7,54 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Borchelt; Archie R.
Assistant Examiner: Frome; Morton J.
Claims
I claim:
1. An apparatus for detecting submicron particulates in a gaseous
carrier, said apparatus comprising;
a. a mixing and gas ionizing section, which section includes means
defining a delay volume for receiving the particulate bearing gas,
and which also includes a source of radiation to effect ionization
of the gaseous carrier, and
b. a detector section operably joined to said section (a) to
receive the ionized gas and entrained particulates therefrom, said
detector section including spaced electrodes having an applied
voltage and between which current flow occurs by means of the
ionized gas to produce a variable signal the magnitude of which is
proportional to the amount of entrained particulates wherein said
mixing and gas ionizing section comprises an elongated body having
a substantially greater longitudinal dimension than transverse
dimension and where said source of radiation is substantially
uniformly distributed over the length of said elongated body.
Description
The ability to detect gas borne submicron particulates is often of
significant value in many industrial and domestic situations,
since, for example, it makes possible the construction of safety
and alarm equipment. More specifically, articles such as air
pollution detecting devices and fire detecting and signaling
apparatus are of obvious value in both home and industry.
Unfortunately, many of the detecting devices currently available
are expensive, difficult to operate and often erratic in
behavior.
It is a principal object of this invention to provide an improved
ion chamber apparatus for detecting the presence and of submicron
particulates entrained in a gaseous carrier which is relatively
cheaper and more dependable in operation than those known in the
art.
An additional object of this invention is to provide an improved
detector of submicron gas borne particulates which includes a
mixing-ionizing chamber and a detector section which is operably
joined to the mixing-ionizing section but separate therefrom.
Other objects and advantages of this invention will be in part
obvious and in part explained by reference to the accompanying
specification and drawings:
FIG. 1 is a cross-sectional view through an improved ion chamber
apparatus according to this invention; and
FIG. 2 is a graph showing the detection characteristics of the
apparatus as a function of time versus ion chamber current and
sample current.
Generally, the ion chamber apparatus of this invention for
detecting submicron particulates entrained in a gaseous carrier
comprises a mixing and gas ionizing section where incoming gas
carrying the particulate material is thoroughly mixed and subjected
to a source of radiation, the radiation effecting ionization of the
gaseous carrier. Operatively connected to the mixing gas ionizing
section is a detector section including a pair of spaced electrodes
which are electrically biased so that current will be transported
from one electrode to the other by means of the ionized gas. A
suitable amplifying and recording or signaling device is connected
to the electrodes to indicate the degree of current flow occurring
at any given time.
The construction of the ion chamber apparatus can best be seen by
referring to FIG. 1 of the drawings where the numeral 10 indicates
an elongated cylindrical body 10 closed at opposite ends by end
caps 11 and 12. It is apparent that although the body 10 is
described as cylindrical, that any other cross-sectional geometry
would be as effective. An inlet port 13 is provided through the end
cap 11 and similarly end cap 12 is provided with an outlet opening
14. Within the volume defined by body 10 is an elongated container
15 which defines a delay volume 18 for receiving particulate
bearings gas. This section formed by the body 15 is one in which
thorough mixing of the incoming gas and carried particulates can
take place as the gas is ionized by means of a source of radiation
located within container 15. It will be noted that the end of body
15 adjacent inlet opening 13 is closed by an end cap 16 having a
generally cup-shaped diffusion baffle 17 which causes the incoming
air and the entrained particulates to enter the delay volume 18 in
a turbulent fashion through the openings 19.
The construction shown in FIG. 1 has the inner surface of the body
15 coated with a suitable radiation source indicated by the numeral
25. Although it would be possible to have a more concentrated
source of radiation, it is highly preferred that it be spread along
the length of the delay volume 18 so that more uniform and complete
radiation of all the gas can be effected. Tests have shown that
concentrated sources of radiation will work, but the results are
less accurate than those obtained with a radiation source extending
some appreciable distance along the axis of the delay volume
container 15, probably because of incomplete dispersion of the ions
from the concentrated source.
The outlet end of delay volume 18 is closed by end cap 26 which has
openings 27 through which the gas flows into the detector section,
indicated generally by the numeral 30. The detector section
comprises an outer electrode 31 which has the openings 27 for
admitting the gas-particulate mixture, an outlet opening 32 and a
centrally located electrode 33 which is connected to an appropriate
voltage source 34. The gas, after flowing between outer electrode
31 and central electrode 33, exits through the openings 35 and on
out through outlet opening 14 in end cap 12.
The outer electrode 31 is electrically connected to a suitable
sensing and amplifying device such as an electrometer (not shown)
by means of the wires 36.
The present device makes use of the fact that submicron particles
can be detected by their influence on the output current of an ion
chamber arranged to collect the small ions produced by a low level
radiation source in the gas stream containing the particles. When
no particles are present, almost all the ions are collected,
resulting in maximum output current of a magnitude determined by
the strength of the radiation source and the ionization properties
of the gas stream. With particles present, some of the ions combine
with them and because the particles are much larger than the ions,
the mobility of the resultant charged particle is less, only a few
being collected in the ion chamber. The result is a decrease of the
output current of the ion chamber, this decrease being a function
of the particle concentration and particles size. The construction
shown in FIG. 1 of the drawings is particularly applicable for use
in connection with, for example, a hydrogen-cooled generator. By
appropriately coating parts of the generator subject to hot spots
with a vaporizable material, a portion of the cooling hydrogen can
be cycled through the ion chamber detecting apparatus and a
determination made as to whether or not any vaporization has in
fact occurred. An advantage of this type of detector for this
application is that the hydrogen can be passed through the detector
and returned to the generator, using the small pressure
differential available within the generator, without the addition
of any pumps or blowers. For a more complete description of this
one area of utility, reference is made to the copending application
of Lloyd P. Grobel and Chester C. Carson, entitled "OVERHEATING
DETECTOR FOR GAS COOLED ELECTRIC MACHINE," Ser. No. 578,855
assigned to the same assignee as the present invention and filed of
even date herewith.
To indicate the fashion in which the apparatus functions, a
detector as shown in FIG. 1 was constructed with the delay volume
18 being 1120 cm.sup.3. An alpha source was distributed along the
walls of the delay volume, in this particular instance the
radiation source being thorium 232 which produces 3,99 Mev. alphas,
total activity on the order of 0.36 micro-Curies. While an alpha
source was used in the present instance, the apparatus is not
limited to this type but can utilize any source of ionizing
radiation.
To test the efficacy of the present apparatus, tests were conducted
on thermal particulate properties of various plastic materials in a
hydrogen atmosphere at pressure up to four atmospheres. The
particular type of thermal plastic used is not important to this
invention since the selection of the proper thermal plastic would
reside in the degree of temperature sensitivity required or sought
by the user. The materials were coated on a metal strip which was
then heated by passing a current through it so that the hydrogen
passing over the heated strip would entrain any volatilized
material and carry it on into the ion chamber.
The manner in which the apparatus function can be seen best is by
reference to FIG. 2 of the drawings. Here, the curve 40 shows how
the current passing through the sample was increased gradually over
a period of about 16 minutes. The curve 41, by way of comparison,
shows the decrease in ion chamber current occurring with the
increase in time and as a function of the amount of material
volatilized from the coated metal specimens. It can be seen that
during the initial 4 or 5 minutes almost maximum ion chamber
current was obtained showing that at the temperatures then present
in the sample little or no volatilization of coating material had
occurred. However, after that time there was a significant and
continuing drop in the ion chamber current as more and more thermal
particulates were introduced into the gaseous hydrogen flowing past
the sample. It is obvious by comparing these curves that the
apparatus functions well as a detector of gas borne particulate
materials.
Although the present invention has been described in connection
with preferred embodiments, it is to be understood that
modifications and variations may be resorted to without departing
from the spirit and scope of the invention, as those skilled in the
art will readily understand. Such modifications and variations are
considered to be within the purview and scope of the invention and
the appended claims.
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