U.S. patent application number 13/814127 was filed with the patent office on 2013-08-01 for system and a method for dispersing by circulation.
The applicant listed for this patent is Yutaka Hagata, Masaya Hotta, Yuu Ishida, Katsuaki Odagi. Invention is credited to Yutaka Hagata, Masaya Hotta, Yuu Ishida, Katsuaki Odagi.
Application Number | 20130194888 13/814127 |
Document ID | / |
Family ID | 43765196 |
Filed Date | 2013-08-01 |
United States Patent
Application |
20130194888 |
Kind Code |
A1 |
Hotta; Masaya ; et
al. |
August 1, 2013 |
SYSTEM AND A METHOD FOR DISPERSING BY CIRCULATION
Abstract
A system and a method for dispersing by circulating a mixture
that simplifies the structure of the part for sealing a shaft of a
dispersing device and lengthens the life of the device are
provided. The system for dispersing by circulating a slurry or
liquid mixture to disperse substances in the mixture comprises a
rotating and continuously dispersing device that disperses the
mixture, a tank that is connected to an outlet of the dispersing
device, a circulating pump that circulates the mixture, and a
piping that in series connects the dispersing device, the tank, and
the circulating pump. In the dispersing device the outflow of the
mixture is greater than the inflow so that an amount of the mixture
in the dispersing device is maintained at a level where a part for
sealing a shaft that is provided inside the dispersing device is
not immersed.
Inventors: |
Hotta; Masaya;
(Toyokawa-shi, JP) ; Hagata; Yutaka;
(Toyokawa-shi, JP) ; Ishida; Yuu; (Toyokawa-shi,
JP) ; Odagi; Katsuaki; (Toyokawa-shi, JP) |
|
Applicant: |
Name |
City |
State |
Country |
Type |
Hotta; Masaya
Hagata; Yutaka
Ishida; Yuu
Odagi; Katsuaki |
Toyokawa-shi
Toyokawa-shi
Toyokawa-shi
Toyokawa-shi |
|
JP
JP
JP
JP |
|
|
Family ID: |
43765196 |
Appl. No.: |
13/814127 |
Filed: |
December 3, 2010 |
PCT Filed: |
December 3, 2010 |
PCT NO: |
PCT/JP2010/071676 |
371 Date: |
April 9, 2013 |
Current U.S.
Class: |
366/132 |
Current CPC
Class: |
B01F 5/106 20130101;
B01F 7/00866 20130101; B01F 5/108 20130101; B01F 5/104 20130101;
B01F 3/1271 20130101; B01F 3/1221 20130101; B01F 7/00858
20130101 |
Class at
Publication: |
366/132 |
International
Class: |
B01F 5/10 20060101
B01F005/10 |
Foreign Application Data
Date |
Code |
Application Number |
Aug 5, 2010 |
JP |
2010-176779 |
Nov 15, 2010 |
JP |
2010-255170 |
Claims
1. A system for dispersing by circulating a slurry or liquid
mixture to disperse substances in the mixture, the system
comprising: a rotating and continuously dispersing device that
disperses the mixture; a tank that is connected to an outlet of the
dispersing device; a circulating pump that circulates the mixture;
and a piping that in series connects the dispersing device, the
tank, and the circulating pump; wherein an outflow of the mixture
from the dispersing device is greater than an inflow into the
dispersing device so that an amount of the mixture in the
dispersing device is maintained at a level where a part for sealing
a shaft that is provided inside the dispersing device is not
immersed.
2. The system of claim 1, wherein the dispersing device is placed
above the tank.
3. The system of claim 1, wherein a pump for increasing the outflow
from the dispersing device is provided in the piping between the
outlet of the dispersing device and an inlet of the tank.
4. The system of claim 1 or 3, wherein a decompressing pump that
decompresses the tank is provided in the tank.
5. The system of claim 1, wherein the dispersing device has a pair
of rotors, wherein the mixture flows through a hollow shaft to a
gap between the pair of rotors, and wherein the mixture is
dispersed when it is radially and outwardly discharged from outer
circumferences of the rotors through the gap between the pair of
rotors.
6. The system of claim 5, wherein the pair of rotors horizontally
face each other.
7. The system of claim 5, wherein the pair of rotors vertically
face each other.
8. The system of claim 7, wherein the mixture is made by mixing a
raw material and additives, wherein by the system the raw material
is circulated through the piping and the additives are added to the
raw material to be dispersed by the dispersing device, and wherein
in the dispersing device the raw material is supplied through a
hollow shaft of a lower rotor in the pair of rotors and the
additives are supplied through a hollow shaft of an upper rotor in
the pair of rotors.
9. The system of any of claims 5 to 8, further comprising: a
driving mechanism that drives at least one of the pair of rotors to
approach, or retract from, each other.
10. The system of claim 9, comprising: a controller that controls
the driving mechanism; wherein the controller adjusts the the gap
between the pair of rotors based on either a pressure detected by a
sensor of the mixture between the pair of rotors or a temperature
of the mixture discharged from the gap between the pair of rotors
detected by a sensor or both the pressure and temperature.
11. The system of claim 10, wherein the driving mechanism is a
servo cylinder.
12. The system of claim 1, wherein the dispersing device has a
rotor and a stator that face each other, wherein the mixture flows
through a hollow shaft to a gap between the rotor and the stator,
and wherein the mixture is dispersed when it is radially and
outwardly discharged from the outer circumferences of the rotor and
the stator through the gap between the rotor and the stator.
13. The system of claim 12, wherein the rotor and the stator
horizontally face each other.
14. The system of claim 12, wherein the rotor and the stator
vertically face each other.
15. The system of claim 14, wherein the mixture is made by mixing a
raw material and additives, wherein by the system the raw material
is circulated and the additives are added to the raw material to be
dispersed by the dispersing device, and wherein in the dispersing
device the raw material is supplied through a hollow shaft of the
stator that is located on the underside of the rotor and the
stator, and wherein the tank has a feeder that supplies the
additives to the raw material in the tank.
16. The system of any of claims 12 to 15, further comprising: a
driving mechanism that drives either the rotor or the stator or
both of them to approach, or retract from, each other.
17. The system of claim 16, comprising: a controller that controls
the driving mechanism; wherein the controller adjusts the size of
the gap between the rotor and the stator based on either a pressure
detected by a sensor of the mixture between the rotor and the
stator or a temperature of the mixture discharged from the gap
between the rotor and the stator detected by a sensor or both the
pressure and temperature.
18. The system of claim 17, wherein the driving mechanism is a
servo cylinder.
19. The system of claim 7 or 8, wherein in the dispersing device a
projection is formed in the outer circumference of the lower rotor
in the pair of rotors to lead the mixture downwardly.
20. The system of claim 19, wherein the projection in the lower
rotor that is shaped as a ring and formed in the outer
circumference of a back face of the lower rotor.
21. The system of claim 5, wherein faces of the pair of rotors that
face each other are made of ceramics.
22. The system of claim 5, wherein the pair of rotors comprise end
members that have respective faces facing each other and mounting
members that mount the end members wherein the end members can be
exchanged, and wherein the end members are made of ceramics and the
mounting members are made of metals.
23. The system of claim 5, wherein the pair of rotors comprise end
members that have respective faces facing each other, mounting
members that mount the end members wherein the end members can be
exchanged, and fixing screws that fix the end members to the
mounting members, wherein the fixing screws are screwed to the
mounting members from faces of the end members, the faces facing
each other, to fix the end members to the mounting members, wherein
the end members are made of ceramics, wherein recesses are formed
in the portions where the fixing screws are screwed in the end
members, and wherein the recesses are formed so that heads of the
fixing screws are located at positions which are deeper than
positions of the faces when the fixing screws are screwed to fix
the end members.
24. A method of dispersing by circulating a slurry or liquid
mixture to disperse substances in the mixture, wherein the mixture
is dispersed by a rotating and continuously dispersing device and
circulated through a piping that in series connects the dispersing
device, a tank that is connected to an outlet of the dispersing
device, and a circulating pump, and wherein an outflow of the
mixture from the dispersing device is greater than an inflow into
the dispersing device so that an amount of the mixture in the
dispersing device is maintained at a level where a part for sealing
a shaft that is provided inside the dispersing device is not
immersed.
25. (canceled)
26. (canceled)
27. (canceled)
28. (canceled)
29. (canceled)
30. (canceled)
31. (canceled)
32. (canceled)
33. (canceled)
34. (canceled)
35. (canceled)
36. (canceled)
37. (canceled)
38. (canceled)
39. (canceled)
40. (canceled)
41. (canceled)
42. The method of claim 24, wherein the dispersing device has a
pair of rotors, wherein the mixture flows through a hollow shaft to
a gap between the pair of rotors, wherein the mixture is dispersed
when it is radially and outwardly discharged from outer
circumferences of the rotors through the gap between the pair of
rotors, wherein the pair of rotors vertically face each other, and
wherein in the dispersing device a projection is formed in the
outer circumference of the lower rotor in the pair of rotors to
lead the mixture downwardly.
43. The method of claim 42, wherein the projection in the lower
rotor is shaped as a ring and formed in the outer circumference of
a back face of the lower rotor.
44. (canceled)
45. (canceled)
46. (canceled)
Description
TECHNICAL FIELD
[0001] The present invention relates to a system and method for
dispersing by circulating a slurry or liquid mixture to disperse
the substances in the mixture.
BACKGROUND ART
[0002] An exemplary system for circulating a slurry or liquid
mixture to disperse substances in a mixture is disclosed in
Japanese Patent Laid-open Publication No. 2004-267991. In a system
for dispersing by circulation like this, the following must be
considered in order to use a rotating and continuously dispersing
device. That is, in such a device, an O ring, an oil seal, a gland
packing, a mechanical seal, or the like is used for a part for
sealing a shaft that prevents the leakage of the mixture through
the axis. When preventing the leakage of a slurry that has a high
concentration, such as a concentration of solids over 40 to 50%,
often a mechanical seal is used.
[0003] However, there are problems in using a mechanical seal. The
structure of it is complicated, the seal is large, and its cost is
high. Moreover, if a mixture penetrates the seal and particulates
enter there, the sealing surface (shaft seal side) is damaged, to
deteriorate the performance. Therefore, there is also a problem in
that a double mechanical seal, which is especially expensive and
has a more complicated structure, will be needed.
DISCLOSURE OF INVENTION
[0004] The purpose of the present invention is to provide a system
and a method for dispersing a mixture by circulation that enables
the structure of the part for sealing a shaft of a dispersing
device to be simple and its life to be longer while dispersing the
mixture by circulating it.
[0005] The system for dispersing by circulating a mixture of the
present invention that disperses a slurry or liquid mixture by
circulating it comprises a rotating and continuously dispersing
device that disperses the mixture, a tank that is connected to the
outlet of the dispersing device, a circulating pump that circulates
the mixture, and a piping that connects in series the circulating
pump that circulates the mixture, the dispersing device, the tank,
and the circulating pump. In the system the outflow of the mixture
from the dispersing device is greater than the inflow into it, so
that the amount of the mixture in the dispersing device is
maintained at a level where the part for sealing a shaft that is
provided inside the dispersing device is not immersed. Herein, the
wording "the inflow of the mixture from the dispersing device is
greater than the inflow into the device" means that the amount (or
flow rate) of the mixture that flows out of the dispersing device
is at least the same as, or greater than, the amount (or flow rate)
of the mixture that flows into the dispersing device. The outflow
from the dispersing device is not necessarily always greater than
the inflow into it, but may be intermittently greater than the
inflow.
[0006] The method for dispersing by circulating a mixture of the
present invention that disperses a slurry or liquid mixture by
circulating it comprises the steps of dispersing a mixture by a
rotating and continuously dispersing device, dispersing the mixture
by circulation through a piping that connects in series the
dispersing device, a circulating pump that is connected to the
outlet of the dispersing device, and the dispersing device, so that
the amount of the mixture in the device is maintained at a level
where the part for sealing a shaft that is provided inside the
dispersing device is not immersed.
[0007] By the present invention, since no mixture penetrates the
part for sealing a shaft, the structure of that part can be
simplified, and the mixture can be properly dispersed by
circulating it. Further, since the life of the part for sealing a
shaft can be lengthened, the maintenance for the dispersing device
and the entire system can be reduced. Therefore, the present
invention achieves a simplified structure, simplified maintenance,
and a low cost.
[0008] The basic Japanese patent applications, No. 2010-176779,
filed Aug. 5, 2010, and No. 2010-255170, filed Nov. 15, 2010, are
hereby incorporated by reference in their entireties in the present
application.
[0009] The present invention will become more fully understood from
the detailed description given below. However, the detailed
description and the specific embodiments are only illustrations of
desired embodiments of the present invention, and so are given only
for an explanation. Various possible changes and modifications will
be apparent to those of ordinary skill in the art on the basis of
the detailed description.
[0010] The applicant has no intention to dedicate to the public any
disclosed embodiment. Among the disclosed changes and
modifications, those which may not literally fall within the scope
of the present claims constitute, therefore, a part of the present
invention in the sense of the doctrine of equivalents.
[0011] The use of the articles "a," "an," and "the" and similar
referents in the specification and claims are to be construed to
cover both the singular and the plural, unless otherwise indicated
herein or clearly contradicted by the context. The use of any and
all examples, or exemplary language (e.g., "such as") provided
herein is intended merely to better illuminate the invention, and
so does not limit the scope of the invention, unless otherwise
stated.
BRIEF EXPLANATION OF THE DRAWINGS
[0012] [FIG. 1] FIG. 1 is a schematic diagram that illustrates a
system for dispersing by circulating a mixture of the present
invention.
[0013] [FIG. 2] FIG. 2 is a schematic sectional drawing of the
dispersing device of the system for dispersing by circulating a
mixture of FIG. 1.
[0014] [FIG. 3] FIG. 3 is a schematic diagram illustrating another
embodiment of the system for dispersing by circulating a mixture of
the present invention.
[0015] [FIG. 4] FIG. 4 is a schematic diagram illustrating yet
another embodiment of the system for dispersing by circulating a
mixture of the present invention.
[0016] [FIG. 5] FIG. 5 is a schematic sectional drawing of the
dispersing device that constitutes the system for dispersing by
circulating a mixture of FIG. 4.
[0017] [FIG. 6] FIG. 6 is a sectional drawing of the rotors that
illustrates another embodiment of the dispersing device that
constitutes the system for dispersing by circulating a mixture,
wherein ceramic members are used for the facing surfaces of a pair
of the rotors.
[0018] [FIG. 7] FIG. 7 is a schematic diagram illustrating another
embodiment of the system for dispersing by circulating a mixture of
the present invention, wherein a driving mechanism is provided for
driving a rotor or stator of the dispersing device.
[0019] [FIG. 8] FIG. 8 is a schematic sectional drawing of the
dispersing device that constitutes another embodiment of the system
for dispersing by circulating a mixture of the present invention,
wherein the dispersing device has a buffering section.
[0020] [FIG. 9] FIG. 9 is a schematic sectional drawing of the main
part of the dispersing device in FIG. 8.
[0021] [FIG. 10] FIG. 10 is a schematic sectional drawing showing
the modification of the dispersing device that has a buffering
section, which dispersing device is yet another embodiment of the
dispersing device that constitutes the system for dispersing by
circulating a mixture of the present invention.
BEST MODE FOR CARRYING OUT THE INVENTION
[0022] Below, a system 30 for dispersing by circulating a mixture
of the present invention is discussed with reference to the
drawings. Though the system 30 for dispersing by circulating a
mixture that disperses a slurry mixture 31 by circulating it (also
called "solid-liquid dispersion" or "slurrying") is below
discussed, the present invention is not limited to this. It has an
effect on dispersing a liquid mixture by circulating it (also
called "liquid-liquid dispersion" or "emulsification"). Herein
"dispersion" means dispersing substances in the mixture, i.e.,
mixing them so that each substance in the mixture is dispersed
uniformly. Moreover, a device or method for "dispersing by
circulating a mixture" includes one for dispersing by circulating a
mixture and by adding additives.
[0023] As shown in FIG. 1, the system 30 for dispersing by
circulating a mixture comprises a rotating and continuously
dispersing device 3 that disperses the mixture 31. It comprises a
tank 1 that is connected to the outlet of the dispersing device 3
and a circulating pump 2 that is connected to the outlet of the
tank 1 to circulate the mixture 31. It also comprises a piping 32
that connects in series the dispersing device 3, the tank 1, and
the circulating pump 2. In the dispersing device 3, the outflow is
greater than the inflow, so that the amount of the mixture 31 in
the dispersing device 3 is maintained at a level where the part 16
for sealing a shaft (refer to FIG. 2) that is provided in the
dispersing device 3 is not immersed.
[0024] At first the fluid that circulates through the tank 1, the
dispersing device 3, and the piping 32 is a raw material. It
gradually becomes a mixture in which additives are dispersed as it
goes through the dispersing device 3. Finally it becomes a
processed mixture that has been dispersed. In the above and
following discussion both the first "raw material" and the
"mixture" that is being processed are called a "mixture."
[0025] As shown in FIGS. 1 and 2, the system 30 for dispersing by
circulating a mixture has a rotating and continuously dispersing
device 3 in which the mixture is supplied from the hollow portion
of a rotating hollow shaft. The mixture is supplied to the
dispersing device 3 by the circulating pump 2. The rate of the
discharged mixture (also called "the outflow") Q.sub.out that is
discharged from a rotor cover 19, which is the casing of the
dispersing device 3, is made to be greater than the rate of the
supplied mixture (also called "the inflow") Q.sub.in that is
supplied by the circulating pump 2. Thus no mixture accumulates
within the rotor cover 19. Further, no mixture reaches the part 16
for sealing a shaft by using the centrifugal force of the rotors 13
and 14.
[0026] Below, the system is discussed in detail. As shown in FIGS.
1 and 2, the discharging port of the tank 1, which is a storage
tank for the mixture, is connected to the circulating pump 2. The
circulating pump 2 conveys and circulates the mixture. A feeder 6
that is provided on the piping for the circulation adds additives 5
(in the form of a fluid or powder) stored in a hopper 4 to the
mixture (a raw material at first) that circulates. The mixture,
after the additives are added, is supplied to the rotating and
continuously dispersing device 3 that is installed above the tank 1
in the vertical direction.
[0027] The rotors 13 and 14 of the dispersing device 3 are
constituted so that they rotate in reverse directions. The rotors
13 and 14 cause the additives to be uniformly dispersed in the raw
material. The mixture that has been processed for being dispersed
between the rotors 13 and 14 of the dispersing device 3 is returned
to the tank 1 by gravity, without accumulating in the rotor cover
19 of the dispersing device 3. The mixture in the tank 1 is
prevented from being segregated, by stirring it by an agitator
7.
[0028] As the feeder 6 for the raw material of the additives 5, a
screw feeder, a rotary valve, a plunger pump, etc., can be suitably
used. The feeder 6 may be placed at an arbitrary position in the
piping 32. It may be placed on the tank 1, etc.
[0029] A vacuum pump 8 is connected to the tank 1. When the amount
that is discharged from the dispersing device 3 is too low, the
vacuum pump 8 can decompress the tank 1 to assist the discharge.
Further, the decompression by the vacuum pump 8 may serve for
degassing the mixture when air bubbles mix with the mixture.
[0030] In the system 30 for dispersing by circulating a mixture,
the valve 9 is normally open and the valves 10 and 11 are normally
closed, when the system is operating. When the dispersion is
completed, the valve 9 is closed and the valve 10 is opened.
Thereby, the processed mixture can be discharged through the valve
10 to then be recovered. Further, the mixture that remains in the
dispersing device 3 or the piping 32 may be discharged by opening
the valve 11 and recovered. The valve for discharging or recovering
the mixture can be placed at an arbitrary place in the tank or the
piping.
[0031] Next, with reference to FIG. 2, the flow of the mixture in
the rotors portion of the dispersing device 3 is discussed. First,
the mixture from the circulating pump 2 is supplied to a gap (a
shearing part) between a pair of rotors 13 and 14 that rotate
through the center of the hollow shaft that is rotated by the
electric motor M, which is shown in FIG. 1. The mixture that has
been supplied is radially discharged by the centrifugal force from
the outer circumferences of the rotors through the gap between the
pair of rotors 13 and 14. When doing so, a shearing force is
applied to the mixture by the rotors 13 and 14, and thus the
mixture is dispersed. The mixture that is discharged from the
rotors 13 and 14 collides with the inner wall of the rotor cover 19
and flows down on it to be discharged from a discharging port 22
that is located in the lower portion.
[0032] The rotors 13 and 14 have shapes that prevent the mixture
that flows from the rotor cover 19 from splashing the rotating
shafts 20 and 21. That is, projections 13c and 14c for protecting
the shaft are formed in the outer circumferences of the back faces
13b and 14b that are the reverse faces of the faces 13a and 14a
that face each other. Further, members 24 and 25 for protecting the
seal are provided in the circumference of the part 16 for sealing a
shaft, such as an oil seal. The members 24 and 25 for protecting
the seal have respective projections 24c and 25c for protecting the
shaft. The members 24 and 25 for protecting the seal are integrally
formed in members 18 for fastening the seal that fasten the
respective parts 16 for sealing. However, they may be formed as
other parts.
[0033] The projections 13c, 14c for protecting the shafts are
upward projections that are shaped as rings in the outer
circumferences of the back faces 13b, 14b. They cause the mixture
to radially and outwardly fly from the inner wall of the rotor
cover 19 by applying a centrifugal force to the mixture that flowed
and fell through the members 24, 25 for protecting the seals. Thus
the rotating shaft 20 is prevented from contacting a liquid (being
splashed or being adhered to).
[0034] The projections 24c, 25c for protecting the shafts are
upward projections that are shaped as rings in the outer
circumferences of the ends of the members 24, 25 for protecting the
seals. They prevent the mixture that is introduced from the inner
wall of the rotor cover 19 from contacting the rotating shafts 20,
21.
[0035] The mixture that is prevented from flowing to the shafts 20,
21 by the projections 24c, 25c for protecting the shafts that are
formed as upward projections that are shaped as rings flows down
the members 24, 25 for protecting the seals. It flows out of the
discharging port 22 of the dispersing device 3 to the tank 1. In
FIG. 2, Q.sub.in denotes the flow of the mixture and Q.sub.out
denotes the flow of the mixture that has been dispersed and is
discharged to the tank 1.
[0036] The centrifugal force to move the mixture radially and
outwardly is generated in the rotors 13, 14 by the rotation. The
member 18 for fastening the seal has a shape so as to prevent the
mixture from reaching the shafts, even if the mixture flows from
the rotors 13, 14 or the rotor cover 19, as discussed above. Since
the rate of the mixture (the rate of the outflow) that flows out of
the discharging port 22 is constituted so that it is greater than
the rate of the mixture that is supplied from the circulating pump
2, the mixture does not accumulate in the rotor cover 19. For
having the rate of the mixture that flows out (outflow) be greater,
the diameter of the piping may be enlarged, for example. The
dispersing device 3 is equipped with a bearing 15 and a plug 17 for
preventing the mixture from flowing back.
[0037] The viscosity of the mixture or the raw material may be so
high that it becomes difficult to have a sufficient amount flow
through the discharging port of the rotor cover 19 only by means of
gravity, due to the fluid resistance. If the amount of the mixture
supplied from the circulating pump 2 is regularly greater than the
amount of it discharged out of the rotor cover 19, the air in the
tank 1 in FIG. 1 may be evacuated by the vacuum pump 8 so that the
tank 1 is in a vacuum. Thus the discharge from the rotor cover is
accelerated. The vacuum pump 8 also functions to reduce the air
bubbles mixed in the liquid. It may make the tank a vacuum for that
purpose. In this case, it is necessary to install a seal that
maintains a vacuum at the seal portions of the rotating shafts.
Thus, the vacuum pump 8 functions as a decompressing pump that
decompresses the tank 1.
[0038] Further, if the amount of the mixture Q.sub.out that flows
out of the rotor cover 19 is not great enough even though the tank
1 is decompressed, a pump 12 may be connected between the
discharging port 22 of the rotor cover 19 and the raw-material
returning port of the tank 1, as shown in FIG. 3, to force the
mixture to be discharged. That is, FIG. 3 illustrates the
modification of the system 30 for dispersing by circulating a
mixture as in FIG. 1. That system is denoted as the system 40 for
dispersing by circulating a mixture. Since the structure of the
system 40 is the same as that of the system 30 except for the pump
12, the same symbols are used, and duplicate explanations are
omitted. The pump 12 is placed in the piping between the outlet of
the dispersing device 3 and the inlet of the tank 1. The pump 12
increases the outflow of the mixture from the dispersing device 3.
Since the amount of the mixture Q.sub.out that flows out of the
rotor cover 19 is determined by the capability of the pump 12,
regardless of the effect of gravity in this case, the dispersing
device 3 need not be installed above the tank 1.
[0039] The dispersing device 3 need not have its shafts horizontal.
As shown in FIG. 4, it may be a dispersing device that is
positioned vertical. That is, FIG. 4 illustrates the modification
of the system 30 for dispersing by circulating a mixture shown in
FIG. 1. That system is denoted as the system 50 for dispersing by
circulating a mixture. The dispersing device 3 that is discussed
above may be used for the system 50 for dispersing by circulating a
mixture as in FIG. 4. However, the rotating and continuously
dispersing device 51 that is shown in FIG. 5 may be suitable. Since
the structures of the system 50 and the dispersing device 51 are
the same as those of the system 30 and the dispersing device 3,
respectively, except for the matters that are discussed below, the
same symbols are used for the same members, and duplicate
explanations are omitted. In the system 50, by adding the pump 12
that is discussed with reference to FIG. 3, the same effect can
also be achieved.
[0040] That is, the system 30 for dispersing by circulating a
mixture of FIG. 1 and the system 50 for dispersing by circulating a
mixture of FIG. 4 have in common the fact that the dispersing
devices 3, 51 have respective pairs of rotors 13, 14 and 53, 54 and
the pairs of rotors 13, 14 and 53, 54 disperse the mixture by
discharging it from the gaps between the rotors 13, 14 and 53, 54
radially and outwardly. The difference between the system 30 of
FIG. 1 and the system 50 of FIG. 4 is that the dispersing device 3
of FIG. 1 has its pair of rotors 13, 14 horizontal whereas the
dispersing device 51 of FIG. 4 has its pair of rotors 53, 54
vertical. An advantage of the system 30 of FIG. 1 may be that the
size of the system in the vertical direction can be made smaller.
Below the structure and advantages of the system 50 of FIG. 4 are
discussed in detail.
[0041] In the system 50 for dispersing by circulating a mixture as
in FIG. 4, the mixture may be supplied from any part of the hollow
portion of the hollow shaft of the upper rotor 53 and the lower
rotor 54. However, for example, if it will be supplied from the
hollow portion of the hollow shaft of the lower rotor 54 by a pump,
then the additives 5 can be supplied from the shaft of the upper
rotor. In this case, a hopper 55 that stores the additives 5 may be
provided above the dispersing device 51.
[0042] As shown in FIG. 5, the rotors 53, 54 of the dispersing
device 51 are constituted like the dispersing device 3 so that they
rotate in reverse directions. The rotors 53, 54 cause the additives
to be uniformly dispersed in the raw material. The raw material
that has been dispersed between the rotors 53, 54 of the dispersing
device 51 is returned to the tank 1 by gravity without it
accumulating in the rotor cover 19 of the dispersing device 51.
[0043] Next, with reference to FIG. 5, the flow of the raw material
and the additives in the dispersing device 51, which is an example
of a vertical device, is discussed. First, the raw material that
has been supplied to the device is supplied to the gap (the
shearing part) between the pair of rotating rotors 53, 54 through
the center of the hollow shaft that is rotated by the electric
motor, which is not illustrated. The supplied raw material is
radially discharged by the centrifugal force from the outer
circumferences of the rotors 53, 54 after passing through the gap
between the pair of rotors 53, 54. By doing so, the raw material is
subject to a shearing force from the rotors 53, 54, and is
dispersed. The raw material discharged from the rotors 53, 54
collides with the inner wall of the rotor cover 19. Then it flows
down the wall and is discharged from the discharging port 22 that
is located in the lower portion.
[0044] Since the additives 5 in the hopper 55 are drawn into the
piping by the negative pressure that is generated by the rotation
of the rotors 53, 54 or the by the evacuation of the air in the
tank by a vacuum pump, the feeder 6 for additives in FIG. 4 will
become unnecessary if the additives are supplied at a sufficient
rate by that operation.
[0045] The rotors 53, 54 are configured to prevent the mixture that
flowed from the rotor cover 19 from splashing the rotating shafts
20, 21. That is, the projection 54c for protecting the shaft is
formed in the outer circumference of the back face of the lower
rotor 54 of the pair of rotors 53, 54. More specifically, the
projection 54c for protecting the shaft is formed in the outer
circumference of the back face 54b of the lower rotor 54, which
back face is the reverse face of the face 54a that faces the upper
rotor 53.
[0046] The projection 54c for protecting the shaft is an upward
projection that is shaped as a ring along the outer circumference
of the back face 54b. It can prevent the mixture from contacting
(splashing or adhering) the rotating shafts 20, 21 by causing the
mixture that has flowed from the rotor cover 19, etc., to the outer
circumferences 53d, 54d of the rotors 53, 54, to flow into a
circumferential groove 56 (by leading the mixture downward). The
mixture that has been prevented by the projection 54c from flowing
to the shaft 20 is led to the discharging port 22 through the
circumferential groove 56 of the rotor cover 19. It flows out of
the discharging port 22 to the tank 1. In FIG. 5, Q.sub.in denotes
the flow of the mixture and Q.sub.out denotes the flow toward the
tank 1 of the mixture that has been dispersed. F.sub.T denotes the
flow of the additives and F.sub.K denotes the flow of the mixture
of the raw material and the additives.
[0047] The dispersing device 3 and the dispersing device 51, which
are discussed with reference to FIG. 2 and FIG. 5, respectively,
are configured to have respective pairs of rotors 13, 14 and 53, 54
that rotate in reverse directions. However, the dispersing device
that constitutes the system 30, 40, 50 for dispersing by
circulating a mixture, is not limited to that device. That is, the
dispersing device in which either of a pair of rotors is changed to
a stator that does not rotate may be used. Specifically, that
dispersing device has a rotor and a stator that face each other.
The mixture flows to the gap between the rotor and the stator
through the hollow shaft. It is dispersed when it is radially and
outwardly discharged from the gap.
[0048] In the dispersing devices 3 and 51 in FIG. 2 and FIG. 5,
respectively, the pair of rotors may be configured to have the
faces that face each other be formed of ceramics. By using ceramics
for the faces, the resistance to wear improves so that durability
improves when applying a high shearing force to the mixture. Now, a
pair of rotors 61 and 62 that are applicable to the dispersing
devices 3, 51 are discussed with reference to FIG. 6. Namely, the
rotors 61, 62 that use the ceramics as discussed below can be used
instead of the rotors 13, 14, 53, 54. The system 30, 40, 50 for
dispersing by circulating a mixture that is equipped with the
dispersing devices 3, 51 to which those rotors are applied can
simplify the maintenance. Thus the cost may be reduced by that
simplification.
[0049] As shown in FIG. 6, a pair of rotors 61, 62 comprise end
members 63, 64 that have respective faces facing each other,
mounting members 65, 66 that exchangeably have mounted the end
members 63, 64 on them, and the fixing screws (such as bolts) 67,
68 that fix the end members 63, 64 to the mounting members 65, 66.
The end members 63, 64 are made of ceramics. The mounting members
65, 66 are made of metal, etc. Though the end members 63, 64 and
the mounting members 65, 66 may be fixed by adhesion, etc., fixing
them by the fixing screws 67, 68 achieves the following advantages.
The pair of rotors 61, 62 in which the end members 63, 64, which
are ceramic members, can be mounted and demounted by the fixing
screws 67, 68, facilitate the exchange of them compared with using
adhesion. Thus the maintenance can be simplified. Thus the cost may
be reduced by that simplification.
[0050] Further, the pair of rotors 61, 62 shown in FIG. 6 have the
following features. That is, the fixing screws 67, 68 are screwed
to the mounting members 65, 66 from the faces 63a, 64a of the end
members 63, 64, which faces 63a, 64a face each other, to fix the
end members 63, 64 to the mounting members 65, 66. The recesses
63b, 64b are formed in the portions where the fixing screws 67, 68
are screwed in the end members 63, 64. The recesses 63b, 64b are
formed so that the heads 67a, 68a of the fixing screws 67, 68 may
be located at positions which are at the lower end of the
predetermined gaps G1, G2 from the faces 63a, 64a of the end
members 63, 64, which faces 63a, 64a face each other, when the
fixing screws 67, 68 are screwed to fix the end members 63, 64. The
predetermined gaps G1, G2 are determined so that the heights H1 and
H2 of the respective heads of the fixing screws 67, 68 comply with
the equations 0.5.times.H1<G1<1.5.times.H1 and
0.5.times.H2<G2<1.5.times.H2, respectively.
[0051] Thus, the pair of rotors 61, 62 have the feature wherein the
depths of the heads 67a, 68a of the fixing screws 67, 68 (i.e., the
depths at the tips of the heads 67a, 68a from the faces 63a, 64a of
the end members 63, 64) are greater than those that are usually
assumed. Because of this feature the solid parts in the mixture
fill in (are deposited in) the crevice (space) between the heads
67a, 68a of the fixing screws 67, 68 and the recesses 63b, 64b of
the end members 63, 64. The filled (deposited) solid parts contact
the slurry mixture, etc., that flows outside of the recesses 63b,
64b, i.e., the positions where the fixing screws 67, 68 are
screwed. However, since it does not flow in the recesses 63b, 64b,
it protects the heads 67a, 68a. In FIG. 6 S.sub.S denotes the
deposited solid parts and S.sub.L denotes the mixture that can
flow.
[0052] In other words, the pair of rotors 61, 62, which have that
feature, can prevent wear of the heads 67a, 68a of the fixing
screws 67, 68 by the solid parts since the heads 67a, 68a are
located at the predetermined depth G1, G2, and the solid parts are
deposited on them.
[0053] By using the pair of rotors 61, 62, the slots or holes for
screwing the fixing screws 67, 68, such as plus slots, minus slots,
hexagon sockets, etc., are prevented from being crushed. Thus
trouble can be prevented. Further, any mixing with the mixture of
metal dust (contamination) generated by the wear of the heads 67a,
68a can be prevented.
[0054] In the pair of rotors 61, 62, if 0.5.times.H1>G1 or
0.5.times.H2>G2, then the effects achieved by the deposited
solid parts would be small. If G1>1.5.times.H1 or
G2>1.5.times.H2, then the recesses 63b, 64b of the end members
63, 64 would become too large, such that the strengths would be
low, or the amount of the deposited solid parts would be too large
such that its removal would become troublesome. As a result, the
range discussed before is proper.
[0055] By using the rotors 61, 62 instead of the rotors 13, 14, 53,
54, which rotors 61, 62 are made of ceramics and have the same
characteristic structure as that of the dispersing device 3, 51,
replacing the ceramic parts can be simplified and foreign
substances can be prevented from mixing. Also, the dispersing
device using the rotors 61, 62 has the effects (increasing
durability, facilitating maintenance, and reducing costs) achieved
by using ceramics. By constituting the system 30, 40, 50 for
dispersing by circulating a mixture with the rotors 61, 62, the
effects by the rotors 61, 62 can be achieved as well as the effects
that were discussed before and will be discussed below. FIG. 6
illustrates an example where the hollow shaft for introducing the
mixture is attached to the rotor 62 (the through-holes 64c, 66c are
formed in the end member 64 and the mounting member 66 of the rotor
62). However, the hollow shaft may be attached to the rotor 6.
Further, the hollow shafts may be attached to both rotors.
[0056] In FIGS. 1, 3, and 4, and FIG. 7, which is below referred
to, M denotes an electric motor and P denotes a pump. The pump P
for the systems 30, 40, and 50 is preferably a pump without a part
for sealing a shaft, as, for example, a tube pump or a hose pump.
If the pump has a part for sealing a shaft that contacts liquid,
that part may deteriorate.
[0057] As seen from the above discussion, the system 30, 40, 50 for
dispersing by circulating a mixture, to which the present invention
is applied, has the features wherein it has the dispersing devices
3, 51, the tank 1, the circulating pump 2, and the piping 32, and
the outflow of the mixture is greater than the inflow so that the
mixture in the dispersing device is maintained at a level where no
part for sealing a shaft 16 is immersed. The method for dispersing
by circulating a mixture, to which the present invention is
applied, has the features for a method for dispersing by
circulating a slurry or liquid mixture wherein the mixture 31 is
dispersed by the rotating and continuously dispersing device 3.
When it is circulated through the piping 32 that connects in series
the device 3, the tank 1 that is connected to the outlet of the
device 3, and the circulating pump 2, then the outflow of the
mixture is greater than the inflow, so that the mixture in the
device is maintained at a level where no part for sealing a shaft
16 is immersed.
[0058] The system 30, 40, 50 for dispersing by circulating a
mixture can simplify the structure of the part for sealing a shaft
of the dispersing device to disperse the mixture, since no mixture
reaches that part. Since the life of the part for sealing a shaft
can be prolonged, the maintenance of the dispersing device or the
entire system can be reduced. Thus, the system and the method
achieve the simplification of the structure, simplification of the
maintenance, and reduction of the cost.
[0059] The system 30, 40, 50 for dispersing by circulating a
mixture causes the mixture to not reach the shaft seals of the
rotating and continuously dispersing machine. Further, for using
the rotating and continuously dispersing device to which the
mixture is supplied from the hollow portion of the rotating hollow
shafts, the system prevents the mixture from reaching the part for
sealing the shaft, by using the rotations (centrifugal forces) of
the shafts or the rotors and by controlling the inflow of the
mixture into the rotors and outflow from the rotors. Thus no
mixture reaches the part for sealing the shaft that seals the
inside and the exterior of the casing (the rotor cover 19) that
stores the rotor. By using the system, since no liquid reaches the
part for sealing the shaft, the shaft seal can be simplified and
its cost is reduced. Or the life of the shaft seal can be
prolonged.
[0060] The system may also have a feature wherein the pump 12 shown
in FIG. 3 is used to transfer liquid to discharge the mixture from
the rotor cover 19. It may also have a feature wherein the amount
of the mixture to be discharged from the rotor cover 19 increases
by decompressing the tank 1 by the vacuum pump 8, for example.
Further, the system 50 may have a feature wherein the rotating
shaft of the dispersing device is installed in a vertical direction
so that the mixture (the raw material at first) from the axial
center of the lower rotor and the additives are supplied from the
axial center of the upper rotor.
[0061] Thus, since, unlike the prior-art system, the system 30, 40,
50 for dispersing by circulating a mixture avoids causing the
mixture from reaching the part 16 for sealing the shaft so as to
thereby saturate the dispersing device with the mixture, a shaft
seal that has a simple structure and a low cost can, be used.
Further, its life can be prolonged.
[0062] In the system 30, 40, 50 for dispersing by circulating the
mixture or the dispersing device 3, 51 in it, a driving mechanism
for moving at least one rotor of the pair of rotors may be provided
so that that one rotor is moved closer to or away from the other
rotor. The driving mechanism is provided in the system for
dispersing by circulating a mixture to prevent the failure of the
devices or the piping due to the increased pressure in the piping
caused by clogging the gap between the pair of rotors or the rotor
and the stator of the dispersing device. The specific structure,
functions, and effects of it are in detail discussed by referring
to the system 130 for dispersing by circulating a mixture as in
FIG. 7.
[0063] Next, with reference to FIG. 7, the system 130 for
dispersing by circulating a mixture, to which the present invention
is applied, is discussed. The system 130 for dispersing by
circulating a mixture has been discussed as one that disperses the
slurry mixture 131 by circulating it like the system 30, 40, 50 for
dispersing by circulating a mixture. However, it is not limited to
this.
[0064] As shown in FIG. 7, the system 130 for dispersing by
circulating a mixture comprises a rotating and continuously
dispersing device 151 that disperses a mixture 131, a tank 101 that
is connected to the outlet of the dispersing device 151, the
circulating pump 102 that is connected to the outlet of the tank
101 to circulate the mixture 131, and the piping 132 that connects
in series the dispersing device 151, the tank 101, and the
circulating pump 102. The dispersing device 151 has the rotor 153
and the stator 154. In the dispersing device 151 the outflow of the
mixture is greater than the inflow, so that the amount of the
mixture 131 in the dispersing device 151 is maintained at a level
where the part for sealing a shaft in the dispersing device 151 is
not immersed. Though the part for sealing a shaft is not
illustrated for the dispersing device 151, the part for sealing a
shaft that is similar to the part 16 in FIG. 5 is provided to the
rotor 153.
[0065] Like the operation discussed with reference to FIG. 1, at
first the fluid that circulates through the tank 101, the
dispersing device 151, and the piping 132, is a raw material. It
gradually becomes a mixture in which additives are dispersed as it
goes through the dispersing device 151. Finally it becomes a
processed mixture that has been dispersed. In the above and
following discussion both the first "raw material" and the
"mixture" that is being processed are called a "mixture."
[0066] The system 130 for dispersing by circulating a mixture has a
rotating and continuously dispersing device 151 in which the
mixture is supplied from the hollow portion of a rotating hollow
shaft. The mixture is supplied to the dispersing device 151 by the
circulating pump 102. The rate of the discharged mixture (also
called "outflow") Q.sub.out that is discharged from a rotor cover,
which is a casing of the dispersing device 151, is made to be
greater than the rate of the supplied mixture (also called
"inflow") Q.sub.in that is supplied by the circulating pump 102.
Thus no mixture accumulates within the rotor cover. Further, no
mixture reaches the part for sealing a shaft. The dispersing device
151 may be changed to have a pair of rotating rotors. By doing so,
the centrifugal force of the rotors is effectively used and the
effect of preventing the mixture from reaching the part for sealing
is achieved.
[0067] The system 130 for dispersing by circulating the mixture
comprises a driving mechanism 171 for moving at least the rotor 143
or the stator 154 of the dispersing device 151, to move one closer
to or away from the other. It also comprises a controller 180 that
controls the driving mechanism 171. The driving mechanism 171 may
be, for example, a servo cylinder. It moves up and down a unit that
includes the rotor 153, a rotating shaft for the rotor 153, and a
motor M for rotating them, so that the gap between the rotor 153
and the stator 154 is enlarged or narrowed. The system 130 for
dispersing by circulating the mixture that comprises the driving
mechanism 171 can prevent the failure of the devices, such as the
pump, or the piping (especially a fitting) if the pressure in the
piping has been or may be increased by clogging the gap between the
rotor 153 and the stator 154.
[0068] The controller 180 adjusts the gap between the rotor 153 and
the stator 154 based on both the detected pressure of the sensor
173 that detects the pressure of the mixture between the rotor and
the stator and the detected temperature of the sensor 174 that
detects the temperature of the mixture discharged from the gap
between them. The controller 180 may adjust it based on the
detection of either the pressure sensor 173 or the temperature
sensor 174.
[0069] The pressure sensor 173 is placed at the position where the
pressure becomes the highest in the piping 132. For example, as
shown in FIG. 7, it is placed before the point where the additives
are added to the dispersing device 151. If a servo cylinder is used
for the driving mechanism 171, the load cell that is provided at
the tip of the cylinder may be used for a pressure sensor.
Alternatively, the pressure sensor placed in the servo cylinder may
be used for that.
[0070] As shown in FIG. 7, the temperature sensor 174 is attached
to the piping 132 at a point just after the outlet of the
dispersing device 151, to detect the temperature of the mixture
that is discharged from the dispersing device 151. Further, the
temperature sensor 175 that detects the temperature of the bearing
portion of the rotor 153 is provided in the system 130 for
dispersing by circulating a mixture. By preliminarily measuring the
relation between the detection by that sensor 175 and the gap
.delta. to store it in the controller 180, the controller 180
adjusts the gap .delta. by operating the drive unit 171 to drive
the rotor 153 in the axial direction based on the detection by the
temperature sensor 175. Thus the pressure can be prevented from
increasing.
[0071] Below further details are discussed. As shown in FIG. 7, the
discharging port of the tank 101 that stores the mixture is
connected to the circulating pump 102. The circulating pump 102
delivers and circulates the mixture. The feeder 106 that is located
above the tank 101 adds the additives 105 (a liquid or powder) that
are stored in the hopper 104 into the mixture (the raw material at
first) that circulates. The mixture to which the additives have
been added is supplied in the rotating and continuously dispersing
device 151 installed above the tank 101 in the vertical
(perpendicular) direction.
[0072] The dispersing device 151 has the rotor 153 and the stator
154 that are arranged so as to perpendicularly face each other. The
dispersing device 151 has a perpendicular axis such that the rotor
153 is located in the upper part and the stator 154 is located in
the lower part. They may be substituted by a pair of rotors that
rotate in reverse directions. Further, the axis is horizontally
arranged so that the rotor and the stator horizontally face each
other. The rotor 153 and the stator 154 cause the additive to be
uniformly dispersed in the raw material. The mixture that has been
dispersed between the rotor 153 and the stator 154 of the
dispersing device 151 is returned to the tank 101 by gravity,
without accumulating in the rotor cover of the dispersing device
151. The mixture in the tank 101 is prevented from being
segregated, by stirring it by the agitator 107.
[0073] For the feeder 106 of the additives 105, a screw feeder, a
rotary valve, a plunger pump, etc., can be suitably used. The
position to place the feeder 106 may be on the piping 132 for the
circulation, that is, any place in the piping 132 can be
arbitrarily chosen.
[0074] The vacuum pump 108 is connected to the tank 101. When the
amount of the discharge from the dispersing device 151 is low, it
can decompress the tank so as to assist discharging the mixture
from the dispersing device 151. Further, the decompression by the
vacuum pump 108 is also used for degassing the mixture when air
bubbles mix with it.
[0075] When the system 130 for dispersing by circulating a mixture
is operating the valve 109 is normally open and the valves 110, 111
are normally closed. Thereby the processed mixture can be
discharged through the valve 110 and then collected. Further, the
mixture that remains in the dispersing device 151 or the piping 132
may be discharged and recovered by opening the valve 111. The valve
for discharging or recovering the mixture can be placed at an
arbitrary place in the tank or the piping.
[0076] Since the flow of the mixture in the rotor of the dispersing
device 151 is the same as that of the dispersing device 51 that is
discussed with reference to FIG. 5, a duplicate explanation is
omitted. The mixture is supplied to the gap between the rotor 153
and the stator 154 through the center of the hollow shaft 154a that
is located in the lower part of the stator 154. It is radially
discharged by the centrifugal force from the outer circumference of
them through the gap. When doing so, the mixture is dispersed by a
shearing force and is discharged along the inner wall of the rotor
cover.
[0077] The rotor 153 and the stator 154 of the dispersing device
151 may have the same shape as the rotors 53 and 54 that are
discussed with reference to FIG. 5. That is, though the stator 154
is shown to be flat in FIG. 7, the projection 54c for protecting
the shaft may be formed on it like the rotor 54 of FIG. 5. In this
case the same effect as that of the dispersing device 51 that has
the rotor 54 can be achieved. Further, in the dispersing device
151, the faces of the rotor 153 and the stator 154 that face each
other may be made of ceramics like those discussed with reference
to FIG. 6.
[0078] As seen from the above discussion, the system 130 for
dispersing by circulating a mixture, to which the present invention
is applied, comprises the dispersing device 151, the tank 101, the
circulating pump 102, and the piping 132. It has the feature
wherein the outflow of the mixture is greater than the inflow so
that the amount of the mixture in the dispersing device 151 is
maintained at a level where no part for sealing a shaft in the
dispersing device 151 is immersed. The method for dispersing by
circulating a mixture, to which the present invention is applied,
has the features for a method for dispersing by circulating a
slurry or liquid mixture wherein the mixture 131 is dispersed by
the rotating and continuously dispersing device 151. When it is
circulated through the piping 132 that connects in series the
device 151, the tank 101 that is connected to the outlet of the
device 151, and the circulating pump 102, the outflow is greater
than the inflow, so that the mixture in the device 151 is
maintained at a level where no part for sealing a shaft 16 is
immersed.
[0079] The system 130 for dispersing by circulating a mixture can
simplify the structure of the part for sealing a shaft of the
dispersing device to disperse the mixture, since no mixture reaches
that part. Since the life of the part for sealing a shaft can be
prolonged, the maintenance of the dispersing device or the entire
system can be reduced. Thus, the system and the method achieve the
simplification of the structure, simplification of the maintenance,
and reduction of the cost.
[0080] The system 130 for dispersing by circulating a mixture
avoids causing the mixture from reaching the shaft seals of the
rotating and continuously dispersing machine. Further, for using
the rotating and continuously dispersing device to which the
mixture is supplied from the hollow portion of the rotating hollow
shafts, the system prevents the mixture from reaching the part for
sealing the shaft by using the rotations (centrifugal forces) of
the shafts or the rotor and by controlling the inflow into, and
outflow from, the rotor. Thus no mixture reaches the part for
sealing the shaft that seals the inside and the exterior of the
casing (the rotor cover) that stores the rotor. By using the
system, since no liquid reaches the part for sealing the shaft, the
shaft seal can be simplified and its cost is reduced. And the life
of the shaft seal can be prolonged. Further, in the system 130 for
dispersing by circulating a mixture, a pump may be provided between
the dispersing device 151 and the tank 101 like the pump 12 that is
discussed with reference to FIG. 3. By using that pump or the
vacuum pump 108, the mixture in the dispersing device can be
prevented from saturating the device. Thus the life of the part for
sealing the shaft can be prolonged.
[0081] Further, the system 130 for dispersing by circulating a
mixture achieves its characteristic effects by having a driving
mechanism 171. Before discussing the characteristic effects by
doing so, the problem that would occur in the system 130 for
dispersing by circulating a mixture that has no mechanism 171 is
discussed. That is, a problem in the system for dispersing by
circulating a mixture that has no driving mechanism, failures of
the devices or the piping due to an abnormal increase of the
internal pressure in the piping may be considered. The most
probable cause to abnormally increase the internal pressure in the
piping, may be the plugging of the solid parts at the part where
the fluid resistance is at the maximum, i.e., the gap between the
rotor and the stator (corresponding to the gap .delta. in FIG. 7)
or between the pair of rotors. For example, to prevent the plugging
of the solid parts so as to protect the devices and the system, an
upper limit for the pressure may preliminarily be set, and the
pressure at the point where the maximum pressure is generated by a
pressure sensor is detected. The system may be configured so that,
if that pressure exceeds the upper limit, the operation is stopped.
However, in so configuring the system a certain time is required to
restart the system, to thereby lose time. Thus it is desirable to
prevent the pressure from increasing prior to it reaching the upper
limit, i.e., removing the plugging in the gap between the rotor and
the stator or the pair of rotors.
[0082] The methods of solving the plugging of the solid parts in
the gap between the rotor and the stator or in the pair of rotors
include first broadening the gap, or, second, increasing the rotor
speed, or, third, decreasing the pumping rate. That is, if the
detected pressure exceeds the predetermined threshold, the gap is
broadened to allow the plugged solid parts to flow, as in the first
method, for example. For the second method, the speed of the rotor
is increased so as to increase a shearing force to thereby destroy
the solid parts that are plugged at the gap. For the third method,
the pumping rate is reduced, to decrease the pressure in the piping
so that more time is available until the plugged solid parts are
removed by destroying them by the shearing force generated by the
original speed of the rotation of the rotors. Among these methods,
the first one is the most direct, and the best in view of removing
the plugging. Thus the system 130 for dispersing by circulating a
mixture adopts it. The second and third methods are essential for
destroying the plugged solid parts. However, if the plugged solid
parts have a high strength, they may not be immediately destroyed
so as to be removed. Herein, the functions and effects are
discussed assuming the first method is used. However, the second or
third method may be used instead of, or in addition to, the first
method. That is, after the gap is broadened to allow the plugged
solid parts to flow and to end the increase of the pressure, then,
if necessary, the speed of the rotation is increased, or the flow
rate is decreased. Then the gap, the rotating speed, or the flow
rate is gradually returned to the original setting (the value for
the normal operation) during the circulating operation. This is an
efficient way. The controller 180 should control the operation.
[0083] As discussed above, the system 130 for dispersing by
circulating a mixture has the driving mechanism 171, which is a
servo cylinder, which adjusts the gap .delta. between the rotor 153
and the stator 154. The system 130 for dispersing by circulating a
mixture can disperse the slurry mixture that has a high
concentration and a high viscosity. The motor M is connected to the
upper disk member to constitute the rotor 153. The upper unit,
which includes the rotor 153, is moved up and down by the driving
mechanism 171 (a servo cylinder) to adjust the gap .delta. between
the rotor 153 and the stators 154. To improve the endurance against
the slurry, the lower disk member is constructed to be the stator
154, which has no part for sealing a shaft (since no part rotates,
no part for sealing a shaft is needed). The slurry mixture that is
being dispersed is supplied to a dispersing part (between the rotor
153 and the stators 154) through the center shaft of the stator
154. The pressure is detected by the pressure sensor 173 that is
placed at the position where the pressure rises most. However, the
pressure sensor may be placed within the driving mechanism 171 (a
servo cylinder), or the pressure may be detected by a load cell
that is provided at the tip of the cylinder. The control of the
rate that the rotor rotates or the rate that the pump pumps may be
carried out by the controller 180 via inverters that are connected
to respective driving motors.
[0084] For the dispersing process in the system 130 for dispersing
by circulating a mixture, if the characteristics of the mixture can
be predicted, the efficiency is improved by preliminarily
constructing the program that controls the gap .delta. between the
rotor 153 and the stator 154, the rotating speed, the flow rate,
etc. For example, in the process of circulating a liquid raw
material, gradually adding powdery additives into it, and producing
the slurry mixture, the solid parts may clump in the early stages
of the operation, to thereby plug the gap between the rotor and the
stator. In this case, for the early stages of the operation, the
gap is preliminarily broadened, and the speed of the rotation is
increased. No possibility of the gap being plugged can occur after
the powdery additives are added, and clumped solid parts are
destroyed during the circulation of the liquid raw material and the
powdery additives to thereby stabilize the characteristics of the
slurry. In this stage the gap and the speed of the rotation are
returned to the original settings (the values for the normal
operation), to carry out the desired dispersion. In this case,
since reducing the flow means a reduction in the amount of the
liquid to pass through the shearing (dispersing) portion, the time
for the process is lengthened. Thus this method is not necessarily
carried out.
[0085] In the step of producing the slurry in the system 130 for
dispersing by circulating a mixture, when the powdery additives are
added multiple times, then the optimal gap between the rotor and
the stator, the optimal speed of the rotation, and the optimal flow
rate, may differ each time. Thus the program for controlling the
operation is prepared so as to achieve an efficient dispersing
operation.
[0086] Further, in the step of discharging the dispersed mixture
after finishing the dispersion in the system 130 for dispersing by
circulating a mixture, efficient processing can be achieved by
controlling the operation. The step of discharging the mixture
follows the step of dispersing it without stopping the operation.
At this time, the valve 109 is closed and the valves 110, 111 are
open. Thus the mixture (a product) can be discharged through the
valves 110, 111 to then be recovered. To prevent excessive
dispersing, the dispersing device 151 is stopped, i.e., the rotor
153 is stopped. Thus the mixture (a product) between the rotor 153
and the stator 154 is subject to a large fluid resistance and it is
hard to discharge it. At this time, by broadening the gap, the flow
resistance can be reduced, to accelerate the discharging. This
effect is great for a mixture having a high viscosity or for a
dispersing device in which a buffer is formed in the rotor or the
stator (below discussed with reference to FIGS. 8, 9, and 10),
since the amount of the mixture to be discharged is large.
[0087] In a disk-type dispersing device, such as the dispersing
device 151, the members that face each other in the rotor 153 and
the stator 154 may generate heat by friction, since they generate a
large shearing force to disperse the mixture by high-speed
rotation. The gap between the rotor 153 and the stator 154 may
decrease due to the thermal expansion of the facing members,
shafts, and their associated parts.
[0088] If the gap between the rotor 153 and the stator 154
decreases, the flow resistance increases, to thereby cause an
abnormal increase in the pressure. Thus the temperature of the raw
material is detected as well as the pressure to be used for
predicting and preventing any increase in the pressure. Thus the
safety of the system can be improved. Since the portion where the
temperature in the raw material rises most is the gap between the
rotor 153 and the stator 154 and that portion rotates at a high
speed, detecting the temperature is difficult. However, by placing
the temperature sensor 174 in the piping just after that portion,
the temperature that is almost the same as the highest one can be
detected.
[0089] If necessary, the temperature at the bearing may be detected
by the temperature sensor 175. By preliminarily investigating the
relationship between the temperature and the gap between the rotor
153 and the stator 154, the decrease in the gap due to the increase
in the temperature can be corrected by a means such as a servo
cylinder (the driving mechanism 171), to maintain the proper gap.
Thus the increase in the pressure can be prevented. Though the
purpose of this control is to prevent any increase in the pressure,
it also prevents any increase in the temperature.
[0090] Further, controlling the operation based on detected
temperatures can be also used for these two purposes: The first
purpose considers the fact that the decrease of the gap by thermal
expansion causes an overload by the contact of the rotor 153 with
the stator 154 (or a pair of rotors), an abnormal noise (a noise),
or a failure of the parts that face each other (disk members). That
is, the first purpose is to prevent these troubles and to properly
control the gap. The second purpose is to better control the
operation for controlling the temperature to prevent the raw
material from deteriorating due to the rise of the temperature,
etc. That is, if the detected temperature of the mixture exceeds a
predetermined value, then, regardless of the pressure, the gap
between the rotor 153 and the stator 154 is increased, and the
speed of the rotation of the rotor 153 is decreased, so that the
heat of the mixture generated by friction is reduced.
[0091] As discussed above, the system 130 for dispersing by
circulating a mixture that comprises the driving mechanism 171
prevents the mixture from plugging the gap .delta. between the
rotor 153 and the stator 154 in the dispersing device 151, and
prevents a failure of a device or piping due to the increase of the
internal pressure of the piping. The driving mechanism 171 may be
used not only in the dispersing device having a rotor and a stator,
but also in the dispersing device having a pair of rotors, such as
the dispersing devices 3, 51. It prevents the mixture from plugging
the gap between a pair of rotors, and prevents a failure of a
device or piping due to the increase of the internal pressure of
the piping.
[0092] Since in the system 130 for dispersing by circulating a
mixture the controller 180 is configured to adjust the gap (the gap
.delta.) between the rotor 153 and the stator 154 based on the
detection of the pressure sensor 173 or the detection of the
temperature sensor 174, or both of them, the condition of the
plugging in the mixture may be detected in advance. Thus plugging
the gap between the pair of rotors and a failure of a device or
piping can certainly be prevented.
[0093] Further, the driving mechanism 171 can be used for a
dispersing device that has a buffering section. The driving
mechanism 171 achieves an effect that is unique to the dispersing
device that has a buffering section, as well as achieving the
effects such as those discussed above. Next, the dispersing device
200 in FIGS. 8, 9, and 10 is discussed, as an example of a
dispersing device that has a buffering section.
[0094] Next, the dispersing device 200 that is suitably used for
the system 1 for dispersing by circulating a mixture and the method
for dispersing by circulation is in detail discussed with reference
to FIGS. 8, 9, and 10. The dispersing device 200 in FIG. 8 etc., is
a continuously dispersing device that efficiently disperses a
plurality of the powdery substances in a liquid or slurry (a
mixture of a powdery substance and a fluid). The dispersing device
200 certainly applies shearing energy to all the raw materials, and
incorporates the local dispersion by a shearing force and the
large-scale dispersion, to efficiently disperse.
[0095] In detail, as in FIGS. 8 and 9, the dispersing device 200
combines the first rotor 201 and second rotor 202, to thereby face
each other. It causes the raw material to pass through the gap
between the rotors 201, 202 radially and outwardly to disperse the
material. It comprises a first rotating device 208 for rotating the
first rotor 201 in a first direction R1 and a second rotating
device 209 for rotating the second rotor 202 in a second direction
R2 that is the reverse of the first direction R1. The port 220 for
discharging the raw material is formed at the center of the
rotation of the first rotor 201 or the second rotor 202.
[0096] Since, by constructing the dispersing device 200 in this
way, the first rotor 201 and the second rotor 202 rotate in reverse
directions, shearing energy can be certainly given to all the raw
materials, to efficiently disperse them.
[0097] In the dispersing device 200, as shown in FIG. 8, for
example, the gap 203 is formed in the outer circumference of the
port 220 for discharging the raw material between the flat surface
221 of the first rotor 201 and the flat surface 231 of the second
rotor 202. A buffering section 206, in which the gap between the
first rotor 201 and the second rotor 202 is larger than that of the
gap 203, is formed in the outer circumference of the gap 203. The
side 232 on the outer circumference that causes the gap between the
first rotor 201 and the second rotor 202 to be narrower than that
of the buffering section 206 is formed in the outer circumference
of the buffering section 206 in the second rotor 202.
[0098] By constructing the dispersing device 200 in this way, since
the gap carries out the local dispersion by shearing and the
buffering section carries out the large-scale dispersion, the
dispersing device 200 can achieve efficient dispersion.
[0099] Further, as shown in FIG. 8 for example, in the dispersing
device 200 the side 232 on the outer circumference is formed to be
parallel to the rotating shaft 208 of the first rotor 201 or
inclined toward the center of the rotation. By constructing the
dispersing device 200 in this way, since the side on the outer
circumference is formed in parallel with the first rotating shaft
or inclined toward the center of the rotation, no raw material
flows from the buffering section to the outer circumference, unless
the raw material flows into the buffering section at an amount that
exceeds the capacity of the buffering section. The raw material
accumulates in the buffering section. Therefore, since a new raw
material flows, at a high speed, from the gap into the material
that is accumulated in the buffering section to violently mix with
it, the material is more uniformly dispersed in the buffering
section.
[0100] As shown in FIG. 10, for example, the dispersing device 200
may have an overhang 262 that extends toward the center of the
rotation at the end of the side 232 on the outer circumference. By
constructing the dispersing device 200 in this way, since the end
of the side on the outer circumference is formed as an overhang
that extends toward the center of the rotation, no raw material
flows from the buffering section to the outer circumference, unless
the raw material flows into the buffering section at an amount that
exceeds the capacity of the buffering section. The raw material
accumulates in the buffering section. Therefore, since a new raw
material flows, at a high speed, from the gap into the material
that has accumulated in the buffering section to violently mix with
it, the material is more uniformly dispersed in the buffering
section.
[0101] As shown in FIG. 8, for example, the gap 203 is located
adjacent to the port 220 for discharging the raw material in the
dispersing device 200. By constructing the dispersing device 200 in
this way, the centrifugal force generated by the rotation of the
first rotor and the second rotor is applied to the raw material in
the gap to cause it to flow outside. Thus its flow velocity
increases so that a negative pressure is generated at the inner
side. Thus a raw material is suctioned through the port for
discharging it to the gap.
[0102] As shown in FIG. 8, for example, in the dispersing device
200 the second gap 204 is formed in the outer circumference of the
buffering section 206 between the flat face 223 of the first rotor
201 and the flat face 233 of the second rotor 202. The gap between
these faces of the second gap 204 is narrower than that of the gap
203. The second buffering section 207, in which the gap between the
first rotor 201 and the second rotor 202 is larger than that of the
second gap 204, is formed in the outer circumference of the gap
204. The second side 224 on the outer circumference that makes the
gap between the first rotor 201 and the second rotor 202 narrower
than the second buffering section 207, is formed in the outer
circumference of the second buffering section 207 in the first
rotor 201. Further, the third gap 205, which is narrower than the
gap 204, is formed in the outer circumference of the buffering
section 207 by the flat face 225 of the first rotor 201 and the
flat face 235 of the second rotor 202. By constructing the
dispersing device 200 in this way, since in addition to the gap and
the buffering section the second gap carries out the local
dispersion by shearing and the second buffering section carries out
the large-scale dispersion, it becomes a continuously dispersing
device that effectively and repeatedly disperses the raw material.
Further, since the third gap carries out a local dispersion by
shearing, it becomes a continuously dispersing device that more
effectively and repeatedly disperses the raw material.
[0103] As shown in FIG. 8 for example, in the dispersing device 200
the buffering section 206 is formed by an indented portion on the
first rotor 201, the side 232 on the outer circumference is formed
in the second rotor 202, the second buffering section 207 is formed
by an indented portion on the second rotor 202, and the second side
224 on the outer circumference is formed in the first rotor 201. By
constructing the dispersing device 200 in this way, since the
indented portions are alternatively formed in the first rotor and
the second rotor, the gap, the buffering section, the side on the
outer circumference, the second gap, the second buffering section,
and the second side on the outer circumference, are all formed.
Thus manufacturing the dispersing device that alternatively and
continuously carries out local dispersions by shearing and
large-scale dispersions for uniformly dispersing the material can
be facilitated.
[0104] Next, with reference to FIGS. 8, 9, and 10, the dispersing
device 200 is discussed in further detail. The dispersing device
200 combines two rotors that rotate at high speeds in reverse
directions. This causes the raw material to pass through the narrow
gap between them by centrifugal force so that multiple raw
materials are uniformly dispersed. As shown in FIG. 8, by coaxially
combining two rotors 201, 202 that have respective concaves and
convexes and vertically face each other, the concavities and
convexities are matched to alternatively form the narrow gaps 203,
204, 205 and broad spaces 206, 207. Herein, the narrow gaps 203,
204, 205 that generate high shearing forces are denoted as the
sections for generating shearing forces. The wide spaces 206, 207
where the raw materials are mixed, which spaces are larger than the
sizes of the sections for generating shearing forces, are denoted
as buffering sections. As shown in FIG. 9, the rotors 201, 202 are
connected to the hollow rotating shafts 208, 209, which are
supported via the bearing 215 by the bearing housing 216 that is
stiffly anchored (no way to anchor it is shown). They are rotated
by an electric motor (not shown) that is connected to a belt, a
chain, a gear, etc. They rotate in reverse directions R1, R2.
Herein, assume that the rotating shafts 208, 209 rotate clockwise
as seen from the ports 212, 214 for discharging the raw material,
respectively. The speeds of the rotation can be arbitrarily
determined depending on the intended raw material or the targeted
degree of dispersion. The raw material supplied to the ports 212,
214 for supplying raw materials flows through the hollow of the
rotating hollow shaft and is supplied to the gap between the two
rotors 201 and 202 from the port 220 for discharging the raw
material that is formed in the center of the rotation of the rotors
201, 202. In this embodiment the port for discharging the raw
material of the rotating hollow shaft 209 is closed by a plug 210a
to prevent the raw material from flowing in and out.
[0105] In the dispersing device 200, the outside diameter D of the
rotors 201, 202 in FIG. 8 is 200 mm, and the heights h1, h2 are 55
mm and 15 mm, respectively The gaps of the sections 203, 204, 205
for generating shearing forces can be adjusted to 0.05-2 mm. The
gaps of the sections 203, 204, 205 for generating shearing forces
are not necessarily constant, but may be suitably changed,
depending on the objects, the design of the shapes, and the sizes
of the rotors 201, 202. For example, the agglomerated particles of
the raw material are dissolved step by step by narrowing the gaps
of the parts 203, 204, 205 for generating shearing forces. Thus
uniformly dispersing the materials is facilitated. The angles
.alpha., .beta. of the sides 232, 224 on the outer circumference of
the buffering sections 206, 207 are 50 degrees and 70 degrees,
respectively. However, they are not limited to these angles. They
may be arbitrarily selected from acute or right angles depending on
the designs of the shapes and the sizes of the rotors 201, 202.
That is, the sides may incline toward the center of the rotation
(in the direction toward the rotating hollow shafts 208, 209) or
stand parallel to the rotating hollow shafts 208, 209. The speeds
of the rotation can be set at 0-1,720 rpm by an inverter control in
this dispersing device. However, they may be suitably changed by
any electric motor, a pulley, a gear, etc., that is selected.
[0106] Now, with reference to FIG. 8, the structures of the
sections 203, 204, 205 for generating shearing forces and the
buffering sections 206, 207 are discussed. The face of the upper
rotor 202 that faces the lower rotor 202 is formed like the flat
face 221 in the outer circumference of the port 220 for discharging
the raw material. It is vertical to the rotating shaft. The
indented portion, which consists of the side on the inner
circumference 222, the flat surface 223 parallel to the flat
surface 221, and the side 224 on the outer circumference, is formed
in the outer circumference side of the flat surface 221. In the
outer circumference of the flat face 221 an indented portion is
formed by the side 222 on the inner circumference, a flat face 223
that is parallel to the flat face 221, and the side 224 on the
outer circumference. The side 224 on the outer circumference
extends toward the lower rotor 202 and beyond the flat surface 221.
At the end of it the flat surface 225 that is parallel to the flat
surface 221 is formed. On the face of the lower rotor 202 that
faces the upper rotor 201, the flat face 231 that in parallel faces
the flat face 221 is formed. The flat surface 231 extends toward
the outer circumference and beyond the side 222 on the inner
circumference. The side 232 on the outer circumference is formed
toward the upper rotor 201 from the flat surface 231. The flat face
233 that in parallel faces the flat surface 223 is formed from the
end of the side 232 on the outer circumference. An indented portion
is formed in the outer circumference of the flat surface 233 by the
flat face 234 that is located in the inner side of the side 224 on
the outer circumference, and the flat face 235 that in parallel
faces the flat face 225.
[0107] By combining the upper rotor 201 and the lower rotor 202
that have those faces, the section 203 for generating shearing
forces is formed by the flat face 221 and the flat face 231, the
section 204 for generating shearing forces is formed by the flat
face 223 and the flat face 233, and the section 205 for generating
shearing forces is formed by the flat face 225 and the flat face
235. The buffering section 206 is formed as a portion that is
surrounded by the side 222 on the inner circumference, the flat
surface 223, the side 232 on the outer circumference, and the flat
surface 231. The buffering section 207 is formed as a portion that
is surrounded by the side 234 on the inner circumference, the flat
face 223, the side 224 on the outer circumference, and the flat
surface 235. Since the side 224 on the outer circumference extends
toward the lower rotor 202 and beyond the flat face 221 to form the
buffering section 207, the capacity of the buffering section 207
becomes large, to uniformly disperse the material in a larger
scale.
[0108] In the above embodiment the side 224 on the outer
circumference extends to the lower rotor 202, beyond the flat face
221. However, the side 224 may extend up to the same position as
the flat face 221, that is, the flat face 221 and the flat face 225
may be on the same level. By constructing the sections for
generating shearing forces and the buffering sections in this way,
since an indented portion is formed in the upper rotor 201 and a
projection is formed in the lower rotor 202 (a portion surrounded
by the side 232 on the outer circumference, the flat surface 233,
and the side 234 on the inner circumference), three sections 203,
204, 205 for generating shearing forces and two buffering sections
206, 207 can be formed. Thus manufacturing the dispersing device
that alternately and continuously carries out dispersions by local
shearing and larger-scale dispersions in a portion that is larger
than that for the dispersions by local shearing can be facilitated.
Further, the side 224 on the outer circumference may extend up to
the near side of the flat face 221.
[0109] The flat surfaces 221, 223, 225, 231, 233, and 235 are
explained as being perpendicular to the rotating shaft and parallel
to each other. However, they may be not vertical to the rotating
shaft or not parallel to each other. Further, the flat faces that
face each other to form the sections 203, 204, 205 for generating
shearing forces may not be parallel to each other. If the gaps
between the sections 203, 204, 205 for generating shearing forces
become narrower toward the outer circumference, the structure
dissolves the agglomerated particles of the raw material to make
them finer, step by step.
[0110] The buffering sections 206, 207 are the portions that store
liquid in order to mix the raw material that has been locally
dispersed at the sections 203, 204 for generating shearing forces.
They have large capacities. Thus, for example, the length L1 in the
radial direction of the flat face 231 for forming the buffering
section 206 is at least 0.5 or more times, normally one or more
times, of the length L2 in the radial direction of the flat face
that forms the section 203 for generating shearing forces by facing
the flat surface 221. The height of the buffering section 206 (the
sum of the size of the gap of the section 203 for generating
shearing forces plus the height of the side 222 on the inner
circumference) is at least three times, but normally five times or
more, the size of the gap 203.
[0111] In FIG. 8 the flow of the raw material is denoted by arrows.
Though for simplicity only one flow is shown, actually the same
type of flow occurs in every place in the space formed by the
rotors 201, 202. Now, FIG. 9 is also referred to again. When the
rotors 201, 202 are rotating, the raw material is supplied from the
port 212 for supplying raw materials of the swivel joint 211 that
is connected to the hollow shaft 208 and is prevented from rotating
(not shown). The raw material is supplied to the gap between the
two rotors 201, 202 from the port 220 for discharging the raw
material. It goes through the section 203 for generating shearing
forces, the buffering section 206, the section 204 for generating
shearing forces, the buffering section 207, and the section 205 for
generating shearing forces, which are formed by the two rotors 201,
202, in sequence along the direction of the centrifugal force. It
is discharged from the part 213 for discharging the raw material
located on the outer circumference of the rotors. Since the raw
material flows to the outer circumference by the centrifugal force
to have its velocity increased, the port 220 for discharging the
raw material becomes under a negative pressure. Thus the flow of
the raw material from the port 220 for discharging the raw material
is accelerated.
[0112] The cork 210 in the port for discharging the raw material of
the hollow shaft 209 may be removed to supply another raw material
from the port 214 for supplying the raw material to mix it between
the rotors with the raw material supplied from the port 212 for
supplying the raw material. However, to do so, the rotors and the
hollow shafts must be horizontally placed, or a pump for supplying
the raw material must be provided. That is because the negative
pressure at the port 220 for discharging the raw material is
usually not so low. Thus the raw material cannot be sucked to the
top of the hollow shaft 209.
[0113] In the dispersing device 200 the two rotating shafts are
driven by respective electric motors. However, they may be driven
by one electric motor by distributing the power by the gears, etc.
The rotating device is composed of these electric motors, a belt, a
chain, a gear, etc., and the hollow shafts 208, 209.
[0114] Next, with reference to FIG. 8, the process for dispersing
the raw material (the method of dispersing) by using the dispersing
device 200 alone is discussed. First, the raw material is subject
to a high shearing force when it passes through the section 203 for
generating shearing forces as the first step such that the
aggregated particulates of emulsified or fine powders are
dissolved. The raw material in which the aggregated particulates of
emulsified or fine powders have been locally dissolved or dispersed
or both by the high shearing force at the section for generating
shearing forces, is discharged from the section 203 for generating
shearing forces and then flows into the first buffering section
206. Since the side 232 on the outer circumference that narrows the
gap between rotors 201, 202 is formed in the outer circumference,
the raw material that has flowed into the buffering section 206
does not flow out of the buffering section unless the amount of the
raw material that has flowed into it exceeds its capacity. Thus the
raw material remains there. By the centrifugal force the raw
material in the buffering section 206 is pressed against the side
232 on the outer circumference in the buffering section 206.
However, since the side 232 on the outer circumference of the
buffering section 206 is inclined so as to resist the flow (as
shown in FIG. 8), the raw material needs to flow into the buffering
section 206 at an amount that exceeds its capacity to discharge it.
At this time the raw material that remains in the buffering section
206 then violently mixes with the raw material that flows into the
buffering section 206 at a high speed. Thus the raw material that
has been locally emulsified or dispersed is uniformly mixed in a
larger scale than is the local portion. Next, the raw material
passes the second section 204 for generating shearing forces and
the second buffering section 207 to be dispersed like in the first
section for generating shearing forces and the second buffering
section. It passes the third section 205 for generating shearing
forces as the last one to be further dispersed.
[0115] To uniformly mix the raw material, the raw material to be
supplied to the device is preferably dissolved in a premixing as a
previous process to emulsify or aggregate particles that are
smaller than the minimum gap of the section for generating shearing
forces. It is also preferably dispersed uniformly at the minimum
volume of the section for generating shearing forces (volume=the
area for shearing x the size of the gap). If no emulsified or
aggregated particles in a liquid is dissolved to the size that can
pass through the gap of the part 203 for generating shearing
forces, it is difficult for a droplet or an aggregated particle
that is larger than the gap of the part 203 to enter the gap when
it flows into the part 203, to thereby cause uneven dispersion or
plugging. Thus it may damage the device because of generation of an
excessive stress. The wording "dispersing uniformly at the minimum
volume of the section for generating shearing forces" means that,
when taking out the minimum volume of the raw material that has
been premixed, the ratios of a plurality of raw materials are
constant regardless of the fact that the emulsified or aggregated
particles are dissolved. For example, in FIG. 8 the minimum volume
of the section for generating shearing forces is that of the gap
203. It is approximately 0.3 ml when the gap is 0.1 mm. The
specific conditions discussed here are those for improving the
performance of the dispersing device 200. Though the dispersing
device 200 is suitably used for the continuously dispersing system,
these conditions do not need to be complied with.
[0116] The shape of the buffering section 206, 207 is not
necessarily limited to the shape in which the side 232, 224 on the
outer circumference inclines as shown in FIG. 8. To increase the
capacities of the buffering sections 206, 207, the overhang
sections 262, 254 that extend to the centers of the rotation
(hollow shafts 208, 209) may be provided at the ends of the sides
232, 224 on the outer circumferences of the buffering sections 206,
207, as shown in FIG. 10. Further, since the flat surface 263 of
the overhang section 262 that faces the flat face 223 of the upper
rotor 241 forms the section 204 for generating shearing forces, the
radial length of the section 204 becomes longer so as to carry out
a more localized dispersing. Similarly, the flat face 255 of the
overhang section 254 that faces the flat face 235 of the lower
rotor 242 forms the larger section 205 for generating shearing
forces so as to carry out a more localized dispersing.
[0117] Herein, the sections for generating shearing forces are
constituted of three steps and the buffering sections are
constituted of two steps. However, they are not necessarily limited
to this constitution. They may be arbitrarily constituted depending
on the raw material that is the object or the targeted degree of
dispersing.
[0118] By constructing the dispersing device 200 as discussed
above, it combines the first rotor and second rotor so as to face
each other so as to disperse the raw material by passing it through
the gap between the two rotors. It has the first rotating device
that rotates the first rotor in the first direction. It also has
the second rotating device that rotates the second rotor in the
second direction that is reverse to the first direction. The port
for discharging the raw material is formed at the center of the
rotation of the first rotor. Thus it can efficiently disperse the
raw material by efficiently applying shearing energy to all of
it.
[0119] The gap is formed in the outer circumference of the port for
discharging the raw material by the flat faces of the first rotor
and the second rotor. The buffering section, in which the distance
between the first rotor and the second rotor is larger than the
size of the gap, is formed in the outer circumference of the gap.
The side on the outer circumference that causes the gap between the
first rotor and the second rotor to be narrower than that of the
buffering section is formed in the outer circumference of the
buffering section in the first or second rotor. Thus mixing for
making uniform the raw material in a larger scale is carried out
after local mixing by shearing forces. By incorporating mixing for
making uniform the raw material in a larger scale with local mixing
by shearing forces, an efficient dispersing can be achieved.
[0120] The dispersing device 200, which is discussed with reference
to FIGS. 8, 9, and 10, has the driving mechanism 171 and the
controller 180 that adjust the gap between the rotor 201 and the
rotor 202. Since the driving mechanism 171 moves the rotor 201, the
plugging of a mixture in the gap .delta. between the pair of rotors
201, 202 or a failure of the device or piping caused by the
increase of the internal pressure can be prevented. Further, the
dispersing device has the other effects caused by the driving
mechanism 171, which effects are discussed above. Further, the
dispersing device 200, which has the driving mechanism 171, can
make it easy to discharge the mixture that accumulates in the
buffering section by widening the gap between the rotors 201, 202
after the operation is completed. The dispersing device 200 can be
used for the systems 30, 40, 50, and 130 for dispersing by
circulation, which are discussed above. The systems have an effect
for simplifying the structure of the part for sealing the shaft of
the dispersing device, since no mixture reaches the part for
sealing the shaft. This is a feature of the system for dispersing
by circulating the mixture. Thus, the systems achieve a suitable
dispersion by circulating a mixture, which is in addition to the
dispersing device 200 achieving a high shearing function for the
mixture.
* * * * *