U.S. patent number 3,834,624 [Application Number 05/374,014] was granted by the patent office on 1974-09-10 for apparatus for fluidizing powders.
This patent grant is currently assigned to Ceskoslovenska akademie ved. Invention is credited to Vladimir Bazant, Ratibor Majzlik, Jan Novosad, Vlastimil Smid.
United States Patent |
3,834,624 |
Novosad , et al. |
September 10, 1974 |
APPARATUS FOR FLUIDIZING POWDERS
Abstract
The apparatus comprises a vertical vessel provided with a
rotating gas-feed unit for maintaining powders in a fluidized
state. The rotating gas-feed unit is provided above the bottom of
the vessel with at least one tube extension terminating in a
nozzle. The gas-feed unit may contain a plurality of tube
extensions with nozzles, the tube extensions having different
lengths and being bent in such a way, that the longitudinal axis of
the nozzles forms an angle of 0.degree. - 90.degree. with respect
to a radial direction passing through the nozzle opening in the
direction of nozzle rotation and an angle of 0.degree. - 45.degree.
in the same plane in the direction towards the bottom of the
vessel. The vessel can be provided by several gas-feed units to
which mixer blades may be attached.
Inventors: |
Novosad; Jan (Praha,
CS), Bazant; Vladimir (Praha, CS), Smid;
Vlastimil (Praha, CS), Majzlik; Ratibor (Praha,
CS) |
Assignee: |
Ceskoslovenska akademie ved
(Praha, CS)
|
Family
ID: |
5388720 |
Appl.
No.: |
05/374,014 |
Filed: |
June 27, 1973 |
Foreign Application Priority Data
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|
|
|
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Jun 27, 1972 [CS] |
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4566-72 |
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Current U.S.
Class: |
239/214.15;
239/254; 239/251; 34/585 |
Current CPC
Class: |
B01J
8/1818 (20130101) |
Current International
Class: |
B01J
8/18 (20060101); B05b 003/02 (); F23d 011/04 () |
Field of
Search: |
;239/251,214.15,143,254
;34/57E,57D |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: King; Lloyd L.
Claims
What is claimed is:
1. Apparatus for fluidizing powders, comprising a vertical vessel,
a rotatable gas-feed unit journalled in bearings in the bottom of
the vessel, means for drivingly rotating the gas-feed unit, a
passage in the gas-feed unit for gas through flow independently
connected to a source of gas under pressure, the gas-feed unit
being provided within the vessel with a tube extension having a
nozzle, the longitudinal axis of the nozzle forming an angle of
from 0 to + 120.degree. in the direction of rotation of the nozzle
with respect to the radial direction passing through the nozzle
opening.
2. Apparatus according to claim 1, wherein the gas-feed unit has a
plurality of tube extensions having nozzles, the distances between
each of said nozzles and the axis of rotation of the gas-feed unit
being substantially different.
3. Apparatus according to claim 1, wherein the longitudinal axis of
the nozzle is inclined downwardly toward the bottom of the vessel
at a second angle with respect to the radial direction passing
through the nozzle opening in the range 0 to + 60.degree..
4. Apparatus according to claim 1, wherein at least two gas-feed
units are disposed in the vessel.
5. Apparatus according to claim 1, wherein the gas-feed unit is
provided with at least two passages for gas through-flow, each
passage being connected to an independent source of gas.
6. Apparatus according to claim 1, wherein the passage for gas
through-flow is provided with a plurality of tube extensions with
nozzles.
7. Apparatus according to claim 1, comprising a mixer blade
attached to the gas-feed unit and rotatable therewith.
Description
BACKGROUND OF THE INVENTION
1. Field of Invention
The subject of the invention is an apparatus for bringing powders
into a state of fluidization. The invention is especially concerned
with apparatus for introducing gases into fluidized beds of
cohesive powders.
2. Prior Art
Fluidized bed processes have gained great importance in modern
technologies. They are base on the ability of a gas stream to
suspend solid particles in the gas stream. A great advantage of
these processes is the great contact area between the gas and the
surface of the solid particle.
The choice of the type of the equipment for introducing gases into
fluidized beds depends on the type of particulate solid that is to
be fluidized. When it is necessary to fluidize a powder which has a
certain degree of cohesion, normal types of grids with gas inlets
opening from below are unsatisfactory since channels or cavities
form in the powder above the grid, the gas flowing through such
channels or cavities without coming into contact with the treated
material. Various studies have therefore been undertaken to
overcome these difficulties.
For example, Gelperin et al., in the book Fundamentals of
Fluidization, Chimia, Moscow 1967 describe a movable grid wherein
the grid usually rotates. These grides are usually designed in the
form of a plate provided with slots or openings forming gas inlets
and are situated near the bottom of the vessel, or are in the form
of a cone provided with openings and rotating around a vertical
axis.
Although this type of equipment has brought certain improvements,
it has not altogether overcome all the existing difficulties which
particularly occur when fine powders with a high degree of cohesion
are fluidized. The problem is in the inability of these types of
equipment to break up the firm channels and domes that have formed
in the powder. Another difficulty that appears in that the openings
in the grids are very often clogged with adhered material so that
the technological process is hindered or fails altogether.
SUMMARY OF THE INVENTION
The present invention has among its objects the provision of an
apparatus for introducing gases into fluidized beds which does not
have the above-mentioned disadvantages of the prior art, and
especially an apparatus wherein there are not formed in the treated
material cavities or channels through which gas can flow without
coming into contact with the treated material.
The above-mentioned objects are filled by this invention. In
accordance with the invention there is provided an apparatus for
fluidizing powders which comprises a vertical vessel provided by at
least one gas inlet and if need be also by a mixer, equipment for
heat supply and heat removal, and an inlet and discharge opening
for powder. The invention includes a gas-feed unit which is used
either singly or in multiple. Each gas-feed unit, which is
independently rotatably mounted in bearings in the bottom of the
vessel and connected to a driving means is provided with at least
one channel for gas flow independently connected to a source of gas
and provided by at least one tube extension with a nozzle. The
longitudinal axis of the nozzle in the direction of its rotation
forms with the radial direction passing through the nozzle's
opening the angle .beta. in the range 0 to .+-. 180.degree.,
conveniently 0 to + 90.degree., and the longitudinal axis of the
nozzle in the direction of the bottom of the vessel forms with
respect to the radial direction passing through the nozzle opening
the angle .alpha. in the range 0 to .+-. 60.degree., conveniently 0
to + 45.degree., the distances between nozzle openings and the axis
of rotation in every gas-feed unit in a given vessel being
different. If required the vessel can be provided by at least two
gas-feed units, at least one gas-feed unit can be provided by at
least two channels for gas through-flow independently connected to
sources of gas, and every channel for gas through-flow may be
provided by, for example, three tube extensions with nozzles. A
mixer can be attached to the gas-feed unit.
Powders having a considerable cohesion can be fluidized by the
above described device. The described design enables gas to be
introduced into the powder by a relatively small number of streams
with high kinetic energy; this prevents the formation of structural
domes in the cohesive powder. The walls of the domes which may
start to form are disrupted by the revolving gas stream so that
they break apart and the resulting falling powder is mixed by the
penetrating gas stream.
The slope of the longitudinal axis of the nozzle in the direction
of rotation and towards the bottom of the vessel causes the
rotating movement of the nozzle to provide the gas streaming from
the nozzle with additional kinetic energy and so the gas stream can
penetrate into the powder over a greater radial distance from the
axis of the gas-feed unit and thus can aerate and mix a greater
volume of material. By the repeated movement of the gas streams
ejected from the nozzles rotating at unequal distances from the
axis there is created a certain pulsation of the gas layers which
is transmitted to the fluidized material and this makes the
formation of cavities in the powder quite impossible. When gas is
introduced into the treated material by means of several gas-feed
units, by several channels for gas through-flow in every gas-feed
unit and when every channel for gas through-flow is provided with
three nozzles, or even by only one nozzle, then the gas being
introduced can be distributed almost evenly over the whole volume
of treated material. This also renders possible an exact control of
the whole fluidization process because the clogging of any nozzle
is immediately indicated by a lowering of gas flow rate or pressure
increase in the inlet piping. The clogged nozzle can then be easily
cleaned even during operation by simply connecting it temporarily
to a source of high pressure gas, by which the clogging is removed.
By attaching blades to the head of the gas-feed unit, the treated
material can be thoroughly mixed so that gas can be introduced and
evenly dispersed throughout even exceptionally cohesive
powders.
This invention can be utilized in may cases when classical methods
of fluidization fail. It can be used for the fluidization of
particulate solids containing a larger proportion of particles with
particle sizes under 100 microns which have a considerable
cohesion. Such processes are particularly efficient because such
fine materials have an exceptionally large specific surface. It
insures that no opening in the gas distributing device becomes
clogged. A particulate solid can be fluidized by a limited amount
of gas when the linear velocity of the gas is just over or even
just under the incipient fluidization velocity. The mixing effect
of the revolving gas streams and of mixer blades, when such blades
are attached to the rotating nozzles, aids in keeping the material
in movement.
The method and device according to this invention can, however, be
utilized even in cases when the particulate solid can be fluidized
by normal non-movable grids, since fixed grids for fluidized beds
of a large cross-section can be more expensive than the device
according to this invention to fit the same area.
A typical example of the utilization of the invention is for
reactors for the direct synthesis of methyl- or
phenyl-chlorosilanes from silicon and methylchloride or silicon and
chlorobenzene. The reason is that it is very advantageous to
conduct this synthesis with very small particles of silicon, most
conveniently with particles in the size range under 60 microns,
because then high conversions can be obtained and only a small
amount of unreacted methylchloride or chlorobenzene has to be
recirculated .
BRIEF DESCRIPTION OF THE DRAWINGS
The enclosed drawings show a preferred embodiment of a device for
fluidizing powders according to this invention, wherein:
FIG. 1 is a view in vertical section through a rotary gas-feed unit
independently fitted in bearings at the bottom of a vessel;
FIG. 2 is a view in plan of a non-symmetrical system of nozzles
according to the invention;
FIG. 3 is a view in vertical section through a gas-feed unit to
which a mixer is attached; and
FIG. 4 is a view in plan of the unit of FIG. 3.
DESCRIPTION OF THE PREFERRED EMBODIMENTS
In the embodiment of FIG. 1 a gas-feed unit 2 is mounted in the
bottom 1 of a vertical vessel in such a way that the axis of the
gas-feed unit is perpendicular to the bottom of the vessel. The
gas-feed unit 2 is journalled in an upper bearing 3 and a lower
bearing 3', and is provided with two parallel longitudinal passages
4, 4' for gas through-flow. At unequal distances from the bottom 1
of the vessel passages 4, 4' bend at right angles and are connected
to sources of gas under pressure by means of packings 8, 8' and 8".
In the head of the gas-feed unit 2, which extends above the bottom
1 of the vessel, the openings of the channels 4, 4' for gas
through-flow are connected at right angles to tube extensions 5, 5'
and these terminate in nozzles 6, 6'. Tube extensions 5, 5' are
unequal in length and are inclined downwardly at the ends at an
angle .alpha. of 30.degree. in a radial direction. The gas-feed
unit 2 is sealed in the bottom 1 of the vessel by a packing 9. The
gas-feed unit 2 is rotated by a prime mover such as an electric
motor (not shown) which drives a pulley at the bottom of the unit 2
through a V-belt, also not shown.
FIG. 2 shows a non-symmetrical system of two nozzles 6, 6' at the
end of tube extensions 5, 5' connected to the head of the gas-feed
unit 2. The lengths of the tube extensions 5, 5' differ, and are
deflected at the ends so that the nozzles 6, 6' at the ends of
these tube extensions 5, 5' form an angle .beta. of 45' in the
plan-view plane with the radial direction in the clockwise
direction of rotation indicated by the curved arrow.
In FIGS. 3 and 4 there is shown a gas-feed unit 2 journalled in
bearings 3, 3' in the bottom of the vessel. The gas-feed unit 2 is
provided by only one channel 4 for gas through-flow through only
one tube extension 5 and only one nozzle 6. Mixer blades 7, 7'
extending almost to the bottom of the vessel 1 are fixed to the
head of the rotating gas-feed unit 2. As indicated by the arrows in
FIGS. 3 and 4, the gas-feed unit rotates clockwise; the mixer
blades 7, 7' are inclined in such direction that they throw the
powder upwardly.
Mixer blades such as those shown in FIGS. 3 and 4 can also be
attached to the embodiments of gas-feed units shown in FIGS. 1 and
2.
Although the invention is illustrated and described with reference
to a plurality of preferred embodiments thereof, it is to be
expressly understood that it is in no way limited to the disclosure
of such a plurality of preferred embodiments, but is capable of
numerous modifications within the scope of the appended claims.
* * * * *