U.S. patent number 3,768,726 [Application Number 05/034,949] was granted by the patent office on 1973-10-30 for method and apparatus for the removal of entrained gases from mineral slurries, pulps, liquids, and the like.
This patent grant is currently assigned to Autometrics Co.. Invention is credited to James C. Hale, Edward P. Herrick.
United States Patent |
3,768,726 |
Hale , et al. |
October 30, 1973 |
METHOD AND APPARATUS FOR THE REMOVAL OF ENTRAINED GASES FROM
MINERAL SLURRIES, PULPS, LIQUIDS, AND THE LIKE
Abstract
A deaerator comprising a rotating chamber having a nozzle
exhausting by centrifugal force the liquid of an entrained
gas/liquid feed into an outer liquid body while the entrained gases
are withdrawn from the interior of the chamber through a separate
gas outlet under a reduced pressure.
Inventors: |
Hale; James C. (Boulder,
CO), Herrick; Edward P. (Boulder, CO) |
Assignee: |
Autometrics Co. (Boulder,
CO)
|
Family
ID: |
21879655 |
Appl.
No.: |
05/034,949 |
Filed: |
May 6, 1970 |
Current U.S.
Class: |
494/10; 494/41;
494/60; 494/81; 494/900; 494/37; 494/43; 494/64; 494/85 |
Current CPC
Class: |
B01D
19/0052 (20130101); Y10S 494/90 (20130101) |
Current International
Class: |
B01D
19/00 (20060101); B04b 005/08 () |
Field of
Search: |
;233/16,1R,19R,21.1E,2R,32,47R,44,46,DIG.1,11,1A,27,28 ;416/231
;55/203 |
References Cited
[Referenced By]
U.S. Patent Documents
Foreign Patent Documents
Primary Examiner: Krizmanich; George H.
Claims
What is claimed is:
1. A deaerator comprising:
an inner gas-liquid receiving chamber having sidewalls and being of
generally circular cross section, a centrally positioned gas-liquid
inlet, a centrally positioned gas outlet and at least one liquid
outlet peripherally positioned in the sidewalls, said inner chamber
being rotatably mounted for relative rotation;
an outer liquid receiving tank surrounding said receiving chamber,
and communicating with said liquid outlet of said inner chamber, a
liquid outlet, and an overflow outlet defining a normal liquid
level therein above and completely submerging the chamber when
filled with a liquid with the liquid outlet of said chamber
communicating the interior of said tank below the normal liquid
level thereof; and,
a gas vacuum producing means connected to the gas outlet of said
chamber to exhaust gases therefrom and maintain the chamber under a
reduced pressure.
2. A deaerator according to claim 1 wherein the inner chamber is a
pair of spherical segments.
3. A deaerator according to claim 1 wherein the inner chamber is a
surface of revolution having its top and bottom surfaces converging
from a maximum dimension along the axis of rotation to a minimum
dimension at the periphery.
4. A deaerator according to claim 1 wherein the inner chamber is a
double conical section, with the axes of revolution thereof
coaligned and the bases abutting, mounted for rotation about the
axes of revolution.
5. A deaerator according to claim 1 wherein the inner chamber has a
plurality of spaced liquid outlets in the sidewalls thereof.
6. A deaerator according to claim 1 wherein the outer tank is
provided with a plurality of radially extending baffles therein
above and below the inner chamber.
7. The deaerator of claim 6 wherein the baffles are vertical.
8. The deaerator of claim 1, wherein the inner chamber is coated
both inside and out with a coating of an elastomer and is provided
with a bottom clean-out door.
9. The deaerator of claim 1 including an outlet conduit connected
to the outlet of the outer tank and an sensor chamber positioned
adjacent the normal liquid level of the tank connected to said
outlet conduit.
10. The deaerator of claim 1 including rotary prime mover means
operatively connected to said inner chamber for the rotary movement
thereof.
11. A deaerator according to claim 1 wherein the gas outlet of said
inner gas-liquid receiving chamber is located in the top thereof
concentric with said gas-liquid inlet.
12. A deaerator according to claim 1 wherein the peripherally
positioned outlet of the inner rotatable gas-liquid receiving
chamber comprises a plurality of openings spaced about the
periphery of said chamber which exhaust directly into the liquid
receiving tank and wherein the gas-liquid inlet of the gas-liquid
receiving chamber as well as the gas outlet is located at the top
thereof.
13. A deaerator according to claim 12 wherein the gas-liquid inlet
of the gas-liquid receiving chamber is positioned concentric with
the gas outlet thereof.
14. The method of deaerating a slurry of suspended solid particles
having a gas entrained therein comprising the steps of:
introducing the slurry to be deaerated into a rotating chamber
immersed in a liquid bath;
centrifugally exhausting the liquid and solids peripherally from
said chamber into the liquid bath by rotating the chamber at a rate
sufficient to provide a hollow spinning annulus of liquid
therewithin; and,
providing a reduced pressure within the chamber and the hollow
interior of the spinning liquid body to extract gases released from
the liquid body whereby a pumping action is produced therein which
is self-pumping.
Description
In the design of a liquid handling system which usually involves
the use of various pumps, agitators, beaters and other devices
which tend to entrain air or other gases in being operated, it
usually follows that a substantial amount of gas is suspended as
bubbles in the liquid. This results in both the liquid and gaseous
phase being present which may have an adverse effect on either the
process treating steps or the instrumentation or both. If
measurements are required to be taken and the instruments used are
sensitive to entrained gases, then it is a necessity for this
entrained gas to be eliminated to permit accurate measurements to
be taken.
While there are deaerating systems in the prior art that make use
of vacuum and centrifugal force or a combination thereof to remove
entrained air from liquids, they usually discharge through a pipe
or scoop which dips into the rotating fluid and picks off the
bottom layer. The pipe is subjected to severe and rapid abrasive
wear since it must be stationary relative to the fluid. The pipe
produces turbulence within the liquid body and may be the origin of
reaeration. None of the prior art devices are as free from abrasion
difficulties or turbulence reaeration as the present invention. The
patent to Rich, U.S. Pat. No. 3,371,059, is directed to apparatus
for the treatment of liquids to separate gas therefrom by combined
use of centrifugal and elastic wave energy. The liquid to be
treated is fed centrally into a rotating drum which throws the
heavier liquid to the outside of the drum leaving a center hollow
portion containing bubbles. This center portion is subjected to
elastic wave energy to break the bubbles and a pair of stationary
pipes are positioned with an inlet of each within the outer layer
of rotating gas free liquid where the liquid is withdrawn. The
patent to Humfeld et al., U.S. Pat. No. 2,542,031, is directed to a
fermentor for submerged cultures having both aeration and foam
breaking devices. The foam breaker comprises a pair of cones and a
disc located above the normal liquid level in the vessel. The
patent to Diamant et al., U.S. Pat. No. 3,249,554, is directed to
apparatus for breaking foam and comprises the drawing of foam
through a rotating impeller which serves to beat the foam and
reduce its volume. The patent to Forrester, U.S. Pat. No.
2,908,652, is directed to apparatus for defoaming liquids and
comprises a cylindrical tank under reduced pressure. An outlet for
discharge of de-aerated liquid is provided in the bottom. A
vertically positioned rotating shaft is axially positioned in the
tank and a plurality of vertically disposed horizontal paddles
mounted thereon for agitation of the liquid to be treated. The
patent to Gates, U.S. Pat. No. 2,366,513, is directed to a method
of breaking foam by separating the foam from the liquid and
subjecting it in the form of a relatively small stream to impact
against a surface and allowing the liquid and gas components to
separate. None of the prior art workers have been able to provide a
suitable dearation system to remove entrained gas from a liquid
stream.
It is an object of this invention, therefore, to provide an
improved deaeration system.
It is a further object of this invention to provide a deaeration
system for use with liquids containing abrasive solids.
A still further object of this invention is to provide a deaeration
system which has a minimum amount of reaeration after
deaeration.
A further object of the invention is to provide a deaeration system
which is easy to maintain and operate and which is readily and
economically manufactured.
In accordance with the invention there is provided a deaerator
comprising an outer liquid receiving tank and an inner
concentrically positioned rotating hollow chamber having an
enlarged portion connecting a centrally positioned inlet. The
enlarged portion is provided with one or more nozzle openings
positioned about the largest diameter thereof and means producing a
reduced pressure within the enlarged portion of the chamber. A
plurality of nozzle openings may be provided or a single annular
slot as the discharge for deaerated liquid into the outer body of
liquid below the normal operating level of the liquid.
For a better understanding of the preent invention, together with
other and further objects thereof, reference is had to the
following description taken in connection with the accompanying
drawings and its scope will be pointed out in the appended
claims.
In the drawings:
FIG. 1 is an elevational view partly in cross section of a
deaerator according to the present invention;
FIG. 2 is a cross sectional view to an enlarged scale showing the
details of the rotating vacuum seal;
FIG. 3 is a view along line 3--3 of FIG. 1; and,
FIG. 4 is a cross sectional view in elevation partly broken away to
conserve space showing another form of the rotating chamber
arrangement.
Referring now to the drawings and in particular to FIG. 1, there is
shown a deaerator 10 which is seen to comprise generally an outer
cylindrical tank 12 having a liquid outlet 14 centrally located in
the bottom thereof and containing an inner rotatable chamber 62
with an inlet 16 communicating the interior of rotatable chamber 62
and from thence to the interior of tank 12 through ports 68. The
top of tank 12 has attached thereto a bearing support plate 18
transversely of the top and secured thereto by means of bolts 20.
Bolts 20 also secure to the support plate a cylindrical extension
22 of tank 12. The upper end of extension 22 is closed by top 23
except for a centrally positioned opening 24 therein. Also the
extension has a horizontally positioned slot 26 in the side wall
near the top to accommodate passage of drive belts 28 therethrough
as will be explained as the description progresses.
A hollow cylindrical bearing housing 30 having upper and lower
outturned mounting flanges 32 and 34 respectively has the lower
flanges 34 bolted to the support plate 18 by means of bolts 36.
Housing 30 also has at the lower extremity an inturned flange 38.
The flange 38 has a stepped portion which supports the outer race
of bearing 40. The upper extremity of housing 30 is provided with
an annular shoulder which supports the outer race of bearing 42 in
vertical spaced coaxial relation to bearing 40. The inner races of
bearings 40 and 42 receive and support tubular member 44 for
rotation. The upper end of member 44 is of a diameter greater than
the opening in the inner race of bearing 42 and provides a shoulder
which is supported vertically by bearing 42. The lower end of
member 44 and the opening in the inner race of bearing 42 is of a
smaller diameter and the larger diameter of the member above
provides a shoulder which is supported by bearing 40. A seal in the
form of an elastomer ring 46 is positioned in sealing relation
between the inturned end of flange 38 and the O.D. of member
44.
A plate 48, having a center opening 50 therein, is secured to the
top of housing 30 as by means of bolts 52. The center opening of
plate 48 is of a size to accommodate the largest diameter of
tubular member 44. The opening 50 is provided with a step forming a
shoulder and a seal in the form of an elastomer ring 54 is
positioned in sealing relation between the shoulder of opening 50
and the enlarged portion 56 of member 44. Member 44 above enlarged
portion 56 is of a reduced diameter and has mounted thereon and
secured thereto in suitable fashion a pulley 58 for rotation
therewith. The lower end of member 44 is provided with external
screw threads, shown dotted. A tubular extension 60 is threadedly
attached to the lower end of member 44 and a splash plate 61 having
a center opening receiving the lower end of member 44 is held
against a shoulder therein in close proximity to the bottom of
support 30 by the upper end of extension 60. To the lower end of
extension 60 is attached the inner rotatable chamber 62 which is
shown in the preferred form of a pair of spherical segments
positioned for rotation about its axis of revolution. The chamber
62 is secured to extension 60 in suitable fashion and the inner and
outer walls of the chamber 62 are covered by a coating 63 of
elastomer to resist abrasion wear. The bottom of chamber 62 is
provided with a clean-out opening 64 which is normally closed by a
cover 66. The walls of chamber 62 are provided with a plurality of
apertures 68 positioned in spaced relation about the largest
diameter thereof in a plane normal to the axis of rotation. The
apertures serve as nozzles to discharge deaerated liquid to the
tank 12 below the liquid level 98 as will be explained. Apertures
68 may be a number of discrete openings or a continuous slot sized
to provide an adequate flow rate of liquid therethrough.
The opening 24 in the top 23 of extension 22 is provided with a cap
70 having a central bore 72 therein and secured to the top 23 by
screws 74. The bore 72 is threaded and the inlet pipe 16 is
threadedly received in the upper end thereof. The lower end of bore
72 threadedly receives the center feed pipe 76 which passes
downwardly inside tubular member 44, extension 60 and into the
interior of vessel 62 terminating just above cover 66 of the
clean-out opening on the bottom of the vessel. The cap 70 is
provided with a downwardly directed annular slot 78 which receives
the upper tubular end of tubular member 44 within slot 78. The
inner diameter of member 44 is provided with a reduced diameter
portion to provide a shoulder 79 at a position approximating the
location of the pulley 58. The shoulder 79 supports a seal 80 which
is held in place by a keeper 82 and a spring 84 bearing against the
keeper 82 and a downwardly directed shoulder 86 on cap 70. The seal
80 provides a gas tight seal between the space 87 communicating the
interior of vessel 62 and the ambient atmosphere. Cap is provided
with a vacuum inlet 88 which is connected to a vacuum line 90.
Vacuum inlet 88 communicates the inner bore of cap 70 which is in
communication with the space 87 within tubular member 44 between
which and the outside of cap 70 seal 80 acts. Referring to FIG. 2
it will be seen that seal 80 is made up of parts 80a, 80b and 80c
which cooperate to provide the necessary sealing action.
The interior of tank 12 is provided with a plurality of radially
positioned vertical baffles 92 above and 94 below vessel 62. A
horizontal baffle 96 is positioned within tank 12 above vessel 62
and below the normal liquid level 98. A motor 100 is mounted on the
side of tank 12 exterior thereof by means of suitable motor mounts
102. The rotating shaft 104 of motor is fitted with a pulley 106 in
which run belts 28 to provide transfer of rotary motion from motor
100 to vessel 62 via pulley 58.
An outlet 108 is connected to outlet 14. Pipe 108 is provided with
an upright leg 110 which includes at the upper end thereof a
chamber 112 which may conveniently contain sensors for measurement
of the parameter of the deaerated liquid. Chamber 112 is provided
with an overflow 114 the height of which establishes the normal
liquid level 98 in tank 12. The side wall of tank 12 has an opening
116 therein which will serve as an overflow port to prevent level
98 from accidentally rising too high and damaging seal 46, bearing
40, etc. Cap 70 is provided with a lubrication tube 118 whereby
lubrication may be supplied to seal 80.
In operation, a source of vacuum is connected to vacuum line 90.
This may conveniently be an aspirator type pump. A feed slurry to
be treated is introduced through pipe 16 into vessel 62 which is
rotated by motor 100 through belts 28. Pipe 16 may be provided with
a valve, not shown, to control the flow rate. The level of the
liquid 77 in vessel 62 is normally at least as high as necessary to
balance the vacuum drawn. The vacuum pump provides the reduced
pressure in the rotating vessel necessary for start-up and exhausts
gases removed from the process fluid through centrally located gas
outlet passage 87 inside of shaft 44 through passage 88 and vacuum
line 90. The incoming fluid to be deaerated is carried to the
bottom surface of the rotating vessel. The fluid flows outward and
assumes a level 77 within the vessel at which the centrifugal force
acting on the fluid is just counteracted by the pressure
differential between the interior of vessel 62 and the interior of
tank 12 which is vented to atmosphere. During the time that the
liquid is in the rotating vessel, it is acted upon by the
combination of low ambient pressure and centrifugal force which
causes the bubbles of entrained air and foam to move toward the
center and be drawn off through the vacuum line. The deaerated
liquid or slurry is exhausted through the peripheral apertures 68
in the walls of the rotating chamber, issues into the fluid body
surrounding same well below the liquid level 98 to prevent
re-aeration and is discharged from the bottom of tank 12 through
the sensing chamber 112 which may house sensors on which entrained
gas would normally have an adverse effect and finally exhausted at
114 for return to the process flow stream. Since the liquid or
slurry passing through chamber 112 has been deaerated, measurements
may be made by such sensors without the presence of entrained
gases.
Excessive turbulence in the tank 12 sufficient to result in air
entrainment is to be avoided. This is accomplished by operating the
rotating chamber a sufficient distance below the surface of the
liquid 98 and the use of baffles 92 and 94. The baffling,
particularly below the rotating chamber, also serves to eliminate
reverse pumping at the discharge 14 by impeding rotation of the
fluid body.
While the shape of the rotating chamber does not materially
influence the principle of operation, right cylindrical shapes at
the periphery are subject to accumulation of heavy solids in the
corners thereof during operation which converts same for all
practical purposes to an internal conical section. The rate of
rotation of the rotating chamber is not particularly critical, as
it only influences the fluid depth 77 in of the rotating chamber.
The rotational speed of the chamber establishes the "g" level in
the fluid, and, hence, the depth of fluid required to
counterbalance the vacuum. The vacuum is kept substantially
constant by the vacuum pump.
The deaerator according to this invention can accept a wide range
of flow rates and is adapted to being a part of a continuous
treating system. The difference between the liquid level 98 in the
tank and the level of pipe 114 is such as to provide a fluid head
to counteract some reverse pumping action.
The size of discharge apertures in the periphery of the rotating
chamber is governed in part by the flow rate desired. The aperture
size can be varied over a wide range but should be kept toward the
small end of the range, consistent with desired flow rates. It will
be understood, of course, the larger the physical size of the
deaerator, the greater the flow rate may be. On the other hand,
increasing the size of the apertures to where they are excessively
large in order to obtain the very high flow rates, might cause some
fluid to recirculate at low flow rates. In such cases, larger
equipment would preferably be used to provide the necessary flow
rates.
It will be appreciated by those skilled in the art that many other
mechanical configurations can be envisioned for supporting the
bearings, effecting the vacuum seal, and providing the necessary
rotation of the submerged inner chamber 62 with respect to the
stationary outer tank 12. The specific embodiment just described is
only intended to convey the basic principles of operation of the
invention.
* * * * *