U.S. patent number 3,694,618 [Application Number 05/168,686] was granted by the patent office on 1972-09-26 for high pressure thermal plasma system.
This patent grant is currently assigned to Humphreys Corporation. Invention is credited to John W. Poole, Merle L. Thorpe, Charles E. Vogel.
United States Patent |
3,694,618 |
Poole , et al. |
September 26, 1972 |
HIGH PRESSURE THERMAL PLASMA SYSTEM
Abstract
A high pressure induction plasma system of the flowing type
includes structure defining a plasma chamber, an electrical coil
surrounding the plasma chamber for creating an intense
electromagnetic field within the plasma chamber, means to supply a
gas for flow through the chamber under at least 10 atmospheres of
pressure and conversion to plasma condition under the influence of
the electromagnetic field, a flow restriction structure spaced at
least one chamber diameter downstream from the electrical coil and
structure defining a stabilizing volume between the coil and the
flow restriction. This stabilizing volume provides aerodynamic and
electrical compensation and allows flowing operation of the system
at pressures of 50 atmospheres and above.
Inventors: |
Poole; John W. (Bow, NH),
Thorpe; Merle L. (Bow, NH), Vogel; Charles E. (Bow,
NH) |
Assignee: |
Humphreys Corporation (Bow,
NH)
|
Family
ID: |
22612515 |
Appl.
No.: |
05/168,686 |
Filed: |
August 3, 1971 |
Current U.S.
Class: |
219/121.36;
219/121.52; 219/121.5 |
Current CPC
Class: |
H05H
1/46 (20130101) |
Current International
Class: |
H05H
1/46 (20060101); B23k 009/00 () |
Field of
Search: |
;219/121P,121R ;313/161
;244/74 |
References Cited
[Referenced By]
U.S. Patent Documents
Primary Examiner: Staubly; R. F.
Assistant Examiner: Peterson; Gale R.
Claims
What is claimed is:
1. An induction plasma system comprising:
structure defining a plasma chamber,
an electrical coil surrounding said chamber and adapted to be
connected to suitable power supply for creating an intense
electromagnetic field within said chamber,
means for supplying a gas under at least 10 atmospheres of pressure
for flow into said chamber and conversion to plasma condition under
the influence of the electromagnetic field produced by said
electrical coil,
flow restriction structure defining a port for flow of said gas
from said chamber, said flow restriction structure being spaced at
least one chamber diameter from the downstream end of said
electrical coil, and structure defining a stabilizing volume
between said coil and said flow restriction structure.
2. The system as claimed in claim 1 wherein said stabilizing volume
is related to the spacing of said flow restriction structure from
the downstream end of said coil, said volume being at least three
times the plasma chamber volume with said flow restriction
structure spaced one chamber diameter from said coil and being
equal to a uniform dimensional extension of said plasma chamber
when said flow restriction structure is spaced at least three
chamber diameters from the downstream end of said coil.
3. The system as claimed in claim 1 wherein said gas flow through
said chamber is a function of, approximately, the three-fourths
power of the chamber pressure in atmospheres.
4. The system as claimed in claim 1 wherein said chamber defining
structure includes a first tubular structure and further including
a second tubular structure coaxially aligned with, surrounding and
spaced from said first tubular structure such that an annular
intermediate chamber is defined and means to supply fluid under
pressure to said intermediate chamber, as to maintain the pressure
in said intermediate chamber at least one-third the pressure in
said plasma chamber.
5. The system as claimed in claim 1 and further including segmented
electrically conductive material on the inner surface of said
plasma chamber defining structure.
6. The system as claimed in claim 5 wherein said stabilizing volume
is related to the spacing of said flow restriction structure from
the downstream end of said coil, said volume being at least three
times the plasma chamber volume with said flow restriction
structure spaced one chamber diameter from said coil and being
equal to a uniform dimensional extension of said plasma chamber
when said flow restriction structure is spaced at least three
chamber diameters from the downstream end of said coil.
7. The system as claimed in claim 6 wherein said chamber defining
structure includes a first tubular structure and further including
a second tubular structure coaxially aligned with, surrounding and
spaced from said first tubular structure so that an annular
intermediate chamber is defined and means to supply fluid under
pressure to said intermediate chamber, to maintain the pressure in
said intermediate chamber at least one-third the pressure in said
plasma chamber.
8. The system as claimed in claim 7 wherein said gas flow through
said chamber is correlated with the three-fourths power of the
chamber pressure in atmospheres.
Description
The invention described herein was made in the performance of work
under a NASA contract and is subject to the provisions of section
305 of the National Aeronautics and Apace Act of 1958, Public Law
85-568 (72 stat. 435; 42 USC 2457).
SUMMARY OF INVENTION
This invention relates to thermal plasma systems and more
particularly to thermal plasma systems of the induction type.
Induction plasma generators create and maintain a thermal plasma by
providing an intense electromagnetic field which produces an
electrodeless discharge in an ionized gaseous medium. Such a
thermal plasma has a temperature in the range of
8,000.degree.-11,000.degree.K and is useful for many purposes such
as performing chemical reactions, the working of metallic and
refractory materials, and other processes that utilize the high
temperatures produced. A number of devices have been proposed for
generating thermal plasmas in such manner including both closed and
flowing systems in which the plasma has been stably maintained both
in reduced pressure environments and in atmospheric pressure
environments. A flowing type of system facilitates the performance
of useful work, either within the plasma chamber or by the output
from the plasma chamber. However, in such systems problems arise
concerning the stabilization of the plasma both spatially and
electrically, that is maintaining the plasma in a stable position
within the chamber so that, for example, it does not move off axis
and damage the integrity of the wall structure, and maintaining
appropriate electrical characteristics so that the thermal plasma
is not extinguished. While such spatial and electrical stability
has been achieved in systems operating at atmospheric pressure and
below, efforts to provide stable thermal plasmas in flowing systems
operating at pressures substantially above atmospheric pressure
have not been successful.
Stable operation of induction plasma generators at elevated
pressures involves a complex of interdependent consideration
including gas conductivity, temperature, pressure and electrical
coupling factors. A stable flowing thermal plasma in a high
pressure environment would be particularly useful in performing
certain chemical processing and also in simulating different types
of environments.
Accordingly it is an object of this invention to provide a novel
and improved flowing type of induction plasma generation system
which operates with improved stability at pressures substantially
above atmospheric pressures.
Another object of this invention is to provide a novel and improved
flowing type of induction plasma generation system which provides
improved yields and which produces greater radiation.
We have discovered that stable operation of a high pressure flowing
induction plasma system may be obtained if the location of the flow
restriction structure is coordinated with the size of the plasma
chamber and the position of the induction coil. A stabilizing
volume should be provided between the flow restriction structure
and the induction coil, the requisite size of this volume being in
part a function of the spacing of the flow restriction structure
from the induction coil. The flow restriction structure should be
spaced at least one chamber diameter from the downstream end of the
coil and with such spacing a volume at least three times the plasma
chamber volume should be interposed between the coil and the flow
restriction structure. The requisite size of the stabilizing volume
decreases as the flow restriction structure is spaced greater
distances from the coil. When the flow restriction structure is
spaced three chamber diameters or more from the coil, adequate
stabilizing volume is provided by a uniform dimensional extension
of the plasma chamber.
In the above description the phrase "plasma chamber volume" means
twice the volume of the chamber between the upstream and downstream
ends of the induction coil; "chamber diameter" means the linear
dimension of a plasma chamber of circular cross-section or the
average of the two dimensions of a chamber of rectangular
cross-section, for example as it will be obvious that plasma
chambers of other cross-sectional configurations may be employed
and the term "chamber diameter" is intended to describe only a
cylindrical chamber; "flow restriction structure" means a structure
which produces a pressure drop of at least 50 psi across it; and
"stabilizing volume structure" means that part of the chamber
disposed between the induction coil and the flow restriction
structure.
In particular embodiments of the invention there is provided a
plasma generator system that includes an elongated tubular plasma
defining chamber with flow restriction structure at one end. An
electrical coil surrounds a portion of this chamber and is
connected to a power supply for creating an intense electromagnetic
field within the chamber. The flow restriction is spaced downstream
from the downstream end of the electrical coil a distance of at
least three times the diameter of the plasma chamber to provide the
stabilizing volume. An injector is provided for introducing
material at the end of the chamber opposite the flow restriction
for maintaining the plasma condition. The material also may be used
as a transport medium for material to be treated within the chamber
by exposure to the high temperature environment provided by the
plasma. The material is introduced to flow in an annular flow
sheath along the inner wall of the chamber to provide stabilization
of the plasma. The requisite flow rate for adequate aerodynamic
stabilization is a function of approximately the three-fourths
power of the pressure and an inverse function of the
cross-sectional area. For example, a minimum flow of 50 SCFH is
required for operation of a particular system at atmospheric
pressure while a minimum flow of 500 SCFH is required for operation
of the same system at 500 psi. In such system the maximum flow is
in the order of about 6 times the minimum flow. The uniform
cross-sectional dimension of the chamber extends a substantial
distance downstream from the plasma so that the stabilized flow
condition is maintained downstream from the coil. Apparatus
constructed in accordance with the invention provides a simple,
reliable and relatively easy to operate stable induction plasma
system of the flowing type operable at pressures up to 50
atmospheres and above.
Other objects, features and advantages of the invention will be
seen as the following description of a particular embodiment
progresses, in conjunction with the drawings, in which:
FIG. 1 is a diagram of an induction plasma generator apparatus
constructed in accordance with the invention;
FIG. 2 is a graph indicating requisite stabilizing volume; and
FIG. 3 is a sectional view showing details of the induction plasma
generator apparatus shown in FIG. 1.
DESCRIPTION OF PARTICULAR EMBODIMENT
The induction plasma generator structure shown in FIG. 1 includes a
tubular plasma chamber defining structure 10 that is in this
embodiment 2 inches in diameter. An injector structure 12 is
disposed at one end of chamber structure 10 and a nozzle structure
14 is disposed at the opposite end. An electrical induction coil
16, six turn that has an inner diameter of 21/2 inches surrounds
chamber 10 adjacent the injector structure so that the nozzle
structure is spaced 15 inches (71/2 chamber diameters) from the
downstream end of coil 16. A nominal 4 megahertz 190-kilowatt DC
plate power power supply 18 is connected to energize coil 16. Gas
from pressurized supply 20 is introduced through injector 12 to
flow in a sheath 22 having generally laminar flow characteristics
along the inner wall of tubular member 10. The power supply 18 is
energized and plasma 24 is initiated by suitable means and stable
operation is maintainable in this system at pressures up to 50
atmospheres and above at argon gas flow rates over 1,000 SCFH.
The graph in FIG. 2 indicates the requisite size of the stabilizing
volume as a function of chamber diameter and chamber volume.
Additional details of the plasma generator may be had with
reference to FIG. 3. As shown in that figure, the chamber defining
structure 10 is a quartz cylinder that has an inner diameter of 2
inches and a length of 18 inches. Thin segments 30 of thermally
reflective material such as gold preferably extend over its inner
surface adjacent coil 16. The upstream end of 32 of cylinder 10 is
disposed within recess 34 of housing structure 36 of the injector
assembly 12 and sealed by O-ring 38.
The inner surface 40 of member 36 defines a cylindrical wall and
cooperates with injector insert structure 42. That insert 42 has a
set of six axially directed orifices 44 (each 0.028 inch in
diameter), a set of six radially directed orifices 46 (each 0.028
inch in diameter), and a set of three generally tangentially
directed swirl orifices 48 (each 0.033 inch in diameter). Conduits
50, 52 and 54 supply orifices 44, 46 and 48, respectively. A
passage through insert 42 may receive an electrode 58 which may be
used for starting purposes. End plate 60 is secured to injector
housing 36 by thumb screw 62 and has a passage 64. A sight port
structure 66 that includes a quartz sight window 68 is secured to
end plate 60 by bolts 70.
A similar end plate 72 has a recess 74 which receives the
downstream end 76 of cylinder 10 and is sealed by O-ring 78.
Secured between end plate 72 and injector retainer housing 36 is an
acrylic cylinder 80. The upstream end of cylinder 80 is secured in
recess 82 of housing 36 and sealed by O-ring 84 while the
downstream end 85 of cylinder 80 secured in recess 86 of end plate
72 and similarly sealed by O-ring 88. Coil 16 is disposed in the
space between cylinders 10 and 80 and connected to terminals 90,
92. Each terminal structure includes a flow passage for coolant,
which coolant is circulated in the space between cylinders 10 and
80 and exhausted through conduit 94. To reduce the radiant heat
load on the acrylic cylinder 80, nigrosine, a water soluble dye, is
added to the cooling water flowing in the space between cylinders
10 and 80. Four glass fiber fabric laminated epoxy rods 100 extend
between end plates 60 and 72 and are secured by nuts 102 for
clamping the assembly together.
Nozzle structure 14 is secured to end plate 72 and includes an
orifice insert 104 and housing 106. In this embodiment a
calorimeter structure 110 may be secured on nozzle structure 14 by
bolts 112. That calorimeter structure includes end plate 114 and
intermediate housing 116 that has flanges 118 which are bolted to
orifice housing 106 and end plate 114. Two arrays of 1/8 inch O.D.
copper tubes 122, 124 arranged in concentric circles extend between
end plate 114 and insert 104. Heat transfer fluid is circulated
from passage 130 through the inner array of tubes 122 to recess 132
in end plate 116 and then returned through the outer array 124 of
tubes to annulus 134 and outlet passage 136 to provide a measure of
the heat output passing through the nozzle 14. An exhaust passage
140 is provided in the side wall of the calorimeter and a
downstream needle valve of passage 140 provides a control on the
flow rate through the plasma generator assembly.
In a typical operation, the power supply 18 is energized and a
plasma is initiated by suitable means, for example by temporary
insertion of a graphite or tungsten rod 58 through either end
plate. The gas flow rate and pressure is adjusted and preferably
concurrent adjustment is made in the pressure of cooling water
flowing in the channel between chamber structure 10 and housing 80
to control the pressure differential across quartz cylinder 10 so
that that pressure differential never exceeds 300 psi. In usual
operation, the sheath gas flow is supplied solely by the radial and
swirl orifices 46, 48 with generally the same flow rates through
those two sets of orifices. The following table indicates operating
conditions in a series of operating runs of the apparatus:
HIGH PRESSURE OPERATION
DC Plate Plasma Gas Chamber Power kW SCFH Ar Pressure psia 46.0 427
215 52.2 277 215 120.0 226 270 147.7 535 317 157.5 472 370 156.0
472 433 169 472 565 128* 1040 620
__________________________________________________________________________
Comparison of visible spectra data obtained at one atmosphere and
at 14.6 atmospheres with an argon plasma indicates that
approximately 5 times as much radiation is produced when the system
is operating at 14.6 atmospheres as is produced when the system is
operating at one atmosphere.
While a particular embodiment of the invention has been shown and
described, in various modifications will be apparent to those
skilled in the art and therefore it is not intended that the
invention be limited to the disclosed embodiment or to details
thereof and departures may be made therefrom within the spirit and
scope of the invention as defined in the claims.
* * * * *