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157165 1 0 165166 2 0 166167 1 0 167168 2 0 158168 1 0 159169 1 0 169170 1 0 170171 1 0 171172 2 0 155171 1 0 173174 1 0 174175 1 0 175176 1 0 176177 1 0 177178 1 0 178173 1 0 177179 1 0 179180 1 0 180181 1 0 181182 1 0 182183 2 0 183184 1 0 184185 2 0 185186 1 0 186181 2 0 183187 1 0 187188 1 0 188189 1 0 189190 1 0 187191 1 0 M ISO 1 44 2 A 42 (-^) A 43 , DIPEA M STY 1 1 SUP M SLB 1 1 1 M SAL 1 15 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 M SAL 1 3 34 35 36 M SBL 1 1 20 M SMT 1 NHFmoc M SBV 1 20 -0.5359 -0.3094 M STY 1 2 SUP M SLB 1 2 2 M SAL 2 5 37 38 39 40 41 M SMT 2 THF M STY 1 3 SUP M SLB 1 3 3 M SAL 3 3 44 45 46 M SBL 3 2 46 47 M SMT 3 DIP M SBV 3 46 -0.7487 -0.6187 M SBV 3 47 0.9797 0.6187 M SAP 3 2 44 42 Al 46 43 Br M STY 1 4 SUP M SLB 1 4 4 M SAL 4 3 66 67 68 M SMT 4 DBU M STY 1 5 SUP M SLB 1 5 5 M SAL 5 5 69 70 71 72 73 M SMT 5 THF M STY 1 6 SUP M SLB 1 6 6 M SAL 6 15 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 M SAL 6 3 107 108 109 M SBL 6 1 95 M SMT 6 NHFmoc M SBV 6 95 -0.7145 -0.4125 M STY 1 7 SUP M SLB 1 7 7 M SAL 7 15 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 M SAL 7 3 143 144 145 M SBL 7 1 135 M SMT 7 NHFmoc M SBV 7 135 -0.7145 -0.4125 M STY 1 8 SUP M SLB 1 8 8 M SAL 8 3 146 147 148 M SMT 8 MnO\s2 M STY 1 9 SUP M SLB 1 9 9 M SAL 9 3 149 150 151 M SMT 9 CH\s2\nCl\s2 M STY 1 10 SUP M SLB 1 10 10 M SAL 10 3 152 153 154 M SMT 10 CH\s2\nCl\s2 M STY 1 11 SUP M SLB 1 11 11 M SAL 11 15 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 M SAL 11 2 171 172 M SBL 11 1 181 M SMT 11 Fmo^c M SBV 11 181 0.8250 0.0000 M END